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Contents Vol. 66b (2011)
Authors Index
 

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Graphical Abstracts: No 1, No 2, No 3, No 4, No 5, No 6, No 7, No 8, No 9, No 10, No 11 No 12

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N u m b e r  1 (Graphical Abstracts)
Original Communications
Synthesis and Crystal Structure of Nb0.84N
N. Frenzel, E. Irran, M. Lerch, and A. Buchsteiner
Key words: Niobium Nitride, Synthesis, Neutron Powder Diffraction, Close Packing 		1  Full Text
The Metal-rich Phosphide Ce4Ir13.55P9
U. Pfannenschmidt, U. Ch. Rodewald, and R. Pöttgen
Key words: Phosphide, Cerium, Crystal Chemistry 		7  Full Text
Single-crystal Structure and Solid-state NMR of Ga2-xScxO3 (x = 0.83)
H. B. Yahia, L. v. Wüllen, S. Balamurugan, U. Ch. Rodewald, H. Eckert, and R. Pöttgen
Key words: Scandium, Crystal Chemistry, Solid-state NMR 		14  Full Text
Alkaline Earth Metal-Hydride-Iodide Compounds: Syntheses and Crystal Structures of Sr2H3I and Ba5H2I3.9(2)O2
O. Reckeweg and F. J. DiSalvo
Key words: Strontium, Barium, Iodide, Hydride, Structure Elucidation, Eutax Calculations 		21  Full Text
Crystal Structure and NQR Studies of Compounds (RH)[ZnBr3(R)], (RH)2[ZnBr4] and [ZnBr2(R)2] (R = Py, n-MePy: n = 2, 3, 4); on the Dominant Stability of the Monoanionic Complexes over the Dianionic and Neutral Species
H. Ishihara, M. Nakashima, H. Nakashima, R. Tateno, Y. Shibamura, T. Makino, A. Kikuchi, D. Kii, K. Horiuchi, I. Svoboda, H. Fuess, and H. Terao
Key words: Zinc(II) Bromide Complexes, 81Br NQR, Crystal Structure, Intermolecular Interactions 		27  Full Text
A New Approach for the Synthesis of Nanostructured Polyurethane-Hydroxylapatite-based Hybrid Materials
L. M. Popescu, R. M. Piticescu, T. Buruian\ua, E. Vasile, R. Tru\csc\ua, and V. B\uadili\ct\ua
Key words: Hybrid Composites, Nanoparticles, Hydrothermal Method, Infrared Spectroscopy, Transmission Electron Microscopy 		36  Full Text
Fabrication and Characterization of Luminescent Multilayer Films Based on Polyoxometalates and Fuchsin Basic
C. Chen, J. Peng, Y. Shen, D. Chen, H. Zhang, and C. Meng
Key words: Layer-by-Layer Self-Assembly, Thin Film, Polyoxometalates, Fuchsin Basic, Fluorescence 		43  Full Text
A Three-dimensional Ferric Molybdenum(V) Phosphate Network with Tunnels: Synthesis, Structure, Magnetic and Electrochemical Properties
K. Yu, B.-b. Zhou, Y. Yu, and Z.-h. Su
Key words: Hydrothermal Synthesis, Ferric Molybdophosphate, Three-dimensional Framework, Topology, Magnetic Character 		49  Full Text
Synthesis and Structural Characterization of the Dinuclear Beryllium Species [Be2Cl2(m-Cl)2(PCy3)2]
H. Braunschweig and K. Gruß
Key words: Beryllium, Dinuclear Compound, Lewis Base, Palladium, X-Ray Diffraction 		55  Full Text
Unusual Formation of Two New Titanium(IV) Tetraphenolates
J. Knizek and H. Nöth
Key words: Tetrakis(2,4-di-tert.-butyl-phenolato)titanium(IV), Dimeric [Tris(pentafluorophenolato)(2,6-diisopropylphenolato)titanium(IV), X-Ray Structures 		58  Full Text
Synthesis, Crystal Structure and Photoluminescence of 1,2-Bis(phenylselenyl)-1,2-dicarba-closo-dodecaborane(12)
J. Miao, H. Chen, M. Xu, B. Peng, Y. Nie, and D. Sun
Key words: Diphenyldiselenide, o-Carborane, Synthesis, Crystal Structure, Photoluminescence 		65  Full Text
A DFT Analysis of the Molecular Structures and Vibrational Spectra of Diphenylsulfone and 4,4'-Sulfonyldianiline (Dapsone)
W. Förner and H. M. Badawi
Key words: Conformational Behavior, Vibrational Spectra and Assignments, Diphenylsulfone, 4,4'-Sulfonyldianiline, Dapsone 		69  Full Text
An Efficient Ultrasound-assisted Method for the Synthesis of 1,4-Disubstituted Triazoles
Y. Jiang, X. Chen, L. Qu, J. Wang, J. Yuan, S. Chen, and X. Li
Key words: Huisgen Cycloaddition, Cu(OAc)2/Cu Wire, Ultrasound, 1,4-Disubstituted Triazole 		77  Full Text
Crystal Structures of Three Di- and Tetrabenzylterephthalamides
P. G. Jones and P. Ku\'s
Key words: Terephthalamides, X-Ray Structures, Secondary Interactions 		83  Full Text
Guanidinium-tagged Organocatalysts for Direct Aldol Reactions
J. Shah and J. Liebscher
Key words: Organocatalysis, Ionic Liquids, Guanidinium Salts, Proline, Asymmetric Synthesis, Aldol Reaction 		88  Full Text
An Alternative and Efficient Route to Chlorophacinone
R. Csuk, A. Barthel, and D. Ströhl
Key words: Chlorophacinone, Anticoagulant, Friedel-Crafts Reaction 		95  Full Text
Notes
1,1-Ethylboration of Trimethyl(methoxypropargyl)- and Chloro(dimethyl)methoxypropargylsilane. A Novel 1,2,5-Oxasilaborolane
B. Wrackmeyer, E. V. Klimkina, T. Kupcik, and R. Lohwasser
Key words: Organoboration, Methoxypropargylsilanes, Heterocycles, NMR 		98  Full Text
Hydrothermal Synthesis and Crystal Structure of a Novel Pb(II) Coordination Polymer
X.-Y. Wang, S. Ma, T. Li, and N. S. Weng
Key words: Coordination Polymer, Crystal Structure, Cyclohexane-1,4-dicarboxylic Acid, 11-Fluoro-dipyrido[3,2-a:2',3'-c]phenazine 		103  Full Text
N u m b e r  2 (Graphical Abstracts)
Original Communications
Synthesis and Characterization of a Cubic Iron Hydroxy Boracite
S. C. Neumair, J. S. Knyrim, O. Oeckler, R. Kaindl, and H. Huppertz
Key words: Borate, Crystal Structure, Hydroxy Boracite, High Pressure 		107  Full Text
The New Vanadoborate-supported Hexanuclear Zinc Complex [Zn(teta)]6[(VO)12O6B18O36(OH)6](H2O) · 8H2O
X. Liu and J. Zhou
Key words: Vanadium, Hydrothermal Synthesis, Crystal Structures, Borates 		115  Full Text
Synthesis, Topological Analysis and Properties of a Coordination Polymer with Butane-1,2,3,4-tetracarboxylato-bridged (Phenanthroline)cobalt(II) Units
H.-L. Zhu and Y.-Q. Zheng
Key words: Supramolecular Architecture, Butane-1,2,3,4-tetracarboxylic Acid, Crystal Structure, Topology, Magnetic Properties 		119  Full Text
Ligand-controlled Assembly of Cd(II) Metal-Organic Coordination Polymers Based on 3,5-Dinitrobenzoate and Flexible Bis(imidazole) Derivatives
G.-C. Liu, J.-X. Zhang, X.-L. Wang, H.-Y. Lin, A.-X. Tian, and Y.-F. Wang
Key words: Coordination Polymer, Hydrothermal Synthesis, Crystal Structure, Photoluminescent Property, Bis(imidazole) Derivative 		125  Full Text
Synthesis, Crystal Structures and Properties of New Barium Thiocyanato Coordination Polymers with trans-1,2-Bis(4-pyridyl)ethylene as Ligand
S. Wöhlert, I. Jess, and C. Näther
Key words: Coordination Chemistry, Barium(II) Thiocyanates, Crystal Structures, Thermal Properties 		133  Full Text
Crystal Chemistry of Uranyl Halides Containing Mixed (UO2)(XmOn)5 Bipyramids (X = Cl, Br): Synthesis and Crystal Structure of Cs2(UO2)(NO3)Cl3
E. V. Nazarchuk, O. I. Siidra, and S. V. Krivovichev
Key words: Uranyl, Chloride, Crystal Structure, Crystal Chemistry, Nitrate 		142  Full Text
Synthesis, Characterization, and Catalytic Activity of Zirconium Oxide Nitrides Supported on High-surface SiO2 (In German)
N. Frenzel, T. Otremba, R. Schomäcker, T. Ressler, and M. Lerch
Key words: Zirconium Oxide Nitride, Ammonia Decomposition, Catalysis 		147  Full Text
HF-HNO3-H2SO4/H2O Mixtures for Etching Multicrystalline Silicon Surfaces: Formation of NO2+, Reaction Rates and Surface Morphologies
M. Lippold, S. Patzig-Klein, and E. Kroke
Key words: Acidic Etching, Multicrystalline Silicon, Nitronium Ions, Sulfuric Acid, Solar Cells 		155  Full Text
Orthoamides and Iminium Salts, LXX. Capturing of Carbon Dioxide with Organic Bases - Reactions of Diamines with Carbon Dioxide
I. Tiritiris and W. Kantlehner
Key words: Carbon Dioxide, Diaminoalkanes, Zwitterionic Carbamates, Crystal Structures 		164  Full Text
Design, Synthesis and Characterization of Some Novel 3-Coumarinyl-5-aryliden-1,3-thiazolidine-2,4-diones and Their Antioxidant Activity
M. \vCa\vci\'c and M. Molnar
Key words: 1,3-Thiazolidine-2,4-diones, 7-Hydroxy-4-bromomethyl-2-oxo-2H-chromene, Knoevenagel Reaction, N-Substitution, Antioxidant Activity 		177  Full Text
Four-component Synthesis of 1,3,4-Oxadiazole Derivatives from (N-Isocyanimino)triphenylphosphorane, (E)-Cinnamic Acids, Acetaldehyde and Secondary Amines
A. Ramazani, Y. Ahmadi, and F. Z. Nasrabadi
Key words: (N-Isocyanimino)triphenylphosphorane, (E)-Cinnamic Acid, Acetaldehyde, 1,3,4-Oxadiazole, aza-Wittig Reaction, Secondary Amine 		184  Full Text
An Efficient Procedure for the Synthesis of Polysubstituted Pyrroles in an Ionic Liquid
Y.-H. He, G.-Q. Wang, K.-L. Xu, and Z. Guan
Key words: Ionic Liquid, Paal-Knorr Reaction, Polysubstituted Pyrrole, 1,4-Diketone, Decarboxylation 		191  Full Text
New Pyridylene-bridged Bisoxazoles - Synthesis and Structural Study
M. Felsmann, J. Hübscher, F. Eißmann, W. Seichter, and E. Weber
Key words: Pyridine Derivatives, Oxazole Derivatives, Nickel, Coordination Compound, X-Ray Diffraction Analysis 		197  Full Text
Notes
ScIrP with ZrNiAl-type Structure
U. Pfannenschmidt, U. Ch. Rodewald, and R. Pöttgen
Key words: Phosphide, Scandium, Crystal Structure 		205  Full Text
A Metal-Organic Framework Constructed of 1,4-Di(pyridin-4-yl)-buta-1,3-diyne and Nickel(II) Nitrate
M. Albrecht, M. Nieger, and A. Schmidt
Key words: MOF, Pyridine, Rhombic Cavities, Coordination Polymer 		209  Full Text
N u m b e r  3 (Graphical Abstracts)
Original Communications
Oxide Fluoride Sulfides of the Lanthanoids with the Formula M3OF5S (M = Nd, Sm, Gd-Ho) (In German)
H. Grossholz, O. Janka, and T. Schleid
Key words: Lanthanides, Oxide Fluoride Sulfides, Crystal Structures 		213  Full Text
CaAl2Si2-type Arsenides RE2/3Zn2As2 (RE = La, Ce, Pr, Nd, Sm)
A. T. Nientiedt, H. Lincke, U. Ch. Rodewald, R. Pöttgen, and W. Jeitschko
Key words: Arsenides, Rare Earth Compounds, Crystal Structure 		221  Full Text
AgScO2 Revisited: Synthesis, Crystal Structure Refinement and Properties of the Single-phase 3R Polymorph
V. Dietrich and M. Jansen
Key words: Silver, Scandium, Delafossite, High Oxygen Pressure, Crystal Structure 		227  Full Text
Application of n-Dodecyltrimethylammonium Chloride for the Oxidation of Intermetallic Phases
B. Böhme, S. Hoffmann, M. Baitinger, and Y. Grin
Key words: DTAC, Ionic Liquid, Oxidation, Ge(cF136), Ge(hR8) 		230  Full Text
Mössbauer-spectroscopic Characterization of the Local Surrounding of Tin Dopant Cations in the Bulk and on the Surface of YCrO3 Crystallites
M. I. Afanasov, A. Wattiaux, C. Labrugère, P. B. Fabritchnyi, and C. Delmas
Key words: YCrO3, 119Sn Mössbauer Spectroscopy, Bulk and Surface Sites 		239  Full Text
New Mixed Tin-rich Alkaline Earth Stannides - Synthesis, Structural Chemistry and Chemical Bonding (In German)
M. Wendorff and C. Röhr
Key words: Stannides, Strontium, Crystal Structure, Band Structure Calculation 		245  Full Text
{[(PhCH2Sn)12(m3-O)14(m-OH)6](F3CSO3)2}: A New Dodecanuclear Organostannoxane
L. Plasseraud, H. Cattey, and P. Richard
Key words: Polyhydroxyorganotin(IV) Cluster, Sn-O-Sn Framework, Triflate, Cleavage Reactions, Crystal Structure 		262  Full Text
First Principles Investigation of the Stability and the Chemical Behavior of Hydrogen in ThCoH4
S. F. Matar
Key words: ThCo Intermetallic, DFT, CrB Type, Hydrides, Bader Charge, Chemical Bonding 		269  Full Text
A New 1D Coordination Polymer Constructed From a Dissymmetrical Oxamidate Ligand: Structure and Magnetic Properties
B. L. Liu, J. Dang, and R. J. Tao
Key words: Oxamidate Ligand, Crystal Structure, Magnetic Propertie 		275  Full Text
Electrochemical Behavior of Cu2+-Histidine Complexes on a Glassy Carbon Electrode
Y.-C. Weng and T.-H. Cheng
Key words: Cu2+-L-Histidine, Copper Complexes, Glassy Carbon Electrode, Electrochemistry, Histidine Complexes 		279  Full Text
A Procedure for Rapid Determination of the Silicon Content in Plant Materials
M. Neumann, R. Nöske, G. Bach, T. Glaubauf, M. Bartoszek, and P. Strauch
Key words: Silica Determination, Silicon Content, Plant Material 		289  Full Text
Separation of Different Types of Monosaccharides by Polyacrylamide Column Chromatography
S. Bystrick\'y, I. Medovarská, and E. Machová
Key words: Polyacrylamide Chromatography, Monosaccharides, Separation 		295  Full Text
Synthesis, Reactions and Antibacterial Activity of 3-Acetyl[1,2,4]triazolo[3,4-a]isoquinoline Derivatives using Chitosan as Heterogeneous Catalyst under Microwave Irradiation
H. M. Hassaneen, H. M. E. Hassaneen, Y. S. Mohammed, R. M. Pagni
Key words: [1,2,4]Triazolo[3,4-a]isoquinoline, Enaminones, Hydrazinolysis, Hydrazonoyl Chlorides, Cycloaddition Reaction, Chitosan, Hydroximoyl Chloride 		299  Full Text
A Short Synthesis of Rhaponticin and its 3''-Fluoroanalog via a Wittig/Heck-Mizoroki Route
R. Csuk and S. Albert
Key words: Rhaponticin, Heck-Mizoroki Reaction, Fluorination 		311  Full Text
First Total Synthesis of 3-Epi-calystegin B2
R. Csuk, S. Reißmann, R. Kluge, D. Ströhl, and C. Korb
Key words: Calystegin, Glucosidase Inhibitor, Ring Closure Metathesis 		317  Full Text
Syntheses and Crystal Structures of Ruthenium-Salen Complexes Containing Triphenylphosphine Ligands
Y. Li, Q. Ma, H.-T. Shi, Q. Chen, and Q.-F. Zhang
Key words: Ruthenium, Schiff Base Ligand, Salen, Synthesis, Crystal Structure 		324  Full Text
N u m b e r  4 (Graphical Abstracts)
Review
Silver-free Gold(I) Catalysts for Organic Transformations
H. Schmidbaur and A. Schier
Key words: Gold Catalysis, Silver-free Gold Catalysts, Silver Salts, Gold Complexes, Homogeneous Catalysis 		329  Full Text
Original Communications
Synthesis and Characterization of a New Infinite 1D Polyoxomolybdate Polymer Further Connected via Cu(I) Nicotinate Subunits
F. Gschwind and M. Jansen
Key words: Polyoxomolybdate, MoO Polymer, Copper Complex, Nicotinic Acid, Hydrothermal Synthesis 		351  Full Text
Structure and Magnetic Properties of a Three-dimensional Metal-organic Framework: [Co(L)(H2O)2] · H2O
M.-S. Chen, Y.-F. Deng, Z.-M. Chen, C.-H. Zhang, and D.-Z. Kuang
Key words: Cobalt(II), Metal-organic Framework, Crystal Structure, Magnetic Property 		355  Full Text
Orthoborate Halides with the Formula (M+II)5(BO3)3X: Syntheses, Crystal Structures and Raman Spectra of Eu5(BO3)3Cl and Ba5(BO3)3X (X = Cl, Br)
O. Reckeweg, A. Schulz, and F. J. DiSalvo
Key words: Incremental Volume, Barium, Europium, Chloride, Bromide, Orthoborate, Raman Spectra 		359  Full Text
Solvothermal Syntheses and Crystal Structures of Two Thioarsenate Metal Complexes [Co(dien)2]3[As3S6]2 and [Mn(teta)]2As2S5
X. Liu and J. Zhou
Key words: Solvothermal Synthesis, Crystal Structure, Thioarsenates, Metal Complexes 		366  Full Text
Sulfur and Selenium Activation by Frustrated NHC/B(C6F5)3 Lewis Pairs; Conformational Flexibility of Products
D. Holschumacher, C. G. Daniliuc, P. G. Jones, and M. Tamm
Key words: N-Heterocyclic Carbenes, Frustrated Lewis Pairs, Sulfur, Selenium 		371  Full Text
Metal-Fluorocarbon Pyrolants. XII: Calcium Salts of 5-Perfluoroalkylated Tetrazoles - Synthesis, Characterization and Performance Evaluation as Oxidizers in Ternary Mixtures with Magnesium and VitonTM (In German)
E.-C. Koch, T. M. Klapötke, H. Radies, K. Lux, and A. Hahma
Key words: Calcium-bis(5H-perfluoroalkyltetrazolates), Magnesium, Pyrolant, NMR, Crystal Structure 		378  Full Text
Synthesis and Characterization of the nido-Platinaborane 7,7-(PPh3)2-7-PtB10H11-11-OC(O)Me
J. Miao, Y. Nie, H. Chen, D. Wang, M. Enders, W. Siebert, G. Sun, and J. Dou
Key words: Boron Cluster, Metallaborane, Platinaborane, Hydrogen Bond, Supramolecular Chemistry 		387  Full Text
Synthesis, Structures and Reactions of Trimethyltantalum(V) Bis[tri(tert.-butyl)silanolate]
J. Knizek and H. Nöth
Key words: Trimethyl-bis(tri-tert.-butylsilanolato)tantalum, Reaction with Borane Derivatives, Molecular Structure 		392  Full Text
Weak Hydrogen Bonds in the Molecular Packing of N-Tetraalkyl Terephthalamides
P. G. Jones and P. Ku\'s
Key words: Terephthalamides, X-Ray Structures, Secondary Interactions 		397  Full Text
Orthoamides and Iminium Salts, LXXI. Capturing of Carbon Dioxide with Organic Bases (Part 2) - Reactions of Guanidines and w-Aminoalkyl-guanidines with Carbon Dioxide (In German)
I. Tiritiris, J. Mezger, E. V. Stoyanov, and W. Kantlehner
Key words: Carbon Dioxide, Guanidines, w-Aminoalkylguanidines, Guanidinium Hydrogen Carbonates, Carbamic Acid, X-Ray Structures 		407  Full Text
Synthesis and X-Ray Crystal Structure Analysis of 1,4-Epoxy-4-methyl-1H,4H-2,3-benzodioxepin
D. S. Giera, L. Hennig, T. Gelbrich, and C. Schneider
Key words: Ozonolysis, Stable Secondary Ozonide, X-Ray Crystal Structure Analysis 		419  Full Text
Dendrophen, a Novel Glycyrrhetyl Amino Acid from Dendronephthya hemprichi
M. Shaaban, K. A. Shaaban, H. I. Abd-Alla, A. G. Hanna, and H. Laatsch
Key words: Dendrophen, Dendrotriol, Dendronephthya hemprichi, Biological Activity 		425  Full Text
Notes
New Quaternary Indides RE7Ni5-xGe3+xIn6 (RE = La, Nd, Sm)
N. Dominyuk, V. I. Zaremba, and R. Pöttgen
Key words: Indide, Rare Earth Compounds, Crystal Structure 		433  Full Text
Synthesis and Structure of the Ternary Vanadate NaMn4(VO4)3
H. B. Yahia, E. Gaudin, U. Ch. Rodewald, and R. Pöttgen
Key words: Vanadates, Crystal Structure, MnO-V2O5-Na2O Ternary System 		437  Full Text
N u m b e r  5 (Graphical Abstracts)
Original Communications
Mössbauer Spectroscopic Investigation of the Cesium Suboxoferrate(III) Cs9FeO4
C. Hoch, I. Schellenberg, and R. Pöttgen
Key words: Suboxometallates, Cesium, Ferrates, Mössbauer Spectroscopy 		441  Full Text
Hydrothermal Synthesis, Crystal Structure and Properties of a 1D Metal-organic Coordination Polymer [Cd(pztmb)2(H2O)2]n
Y. Zhou, X.-M. Sun, S.-Q. Zang, and H.-W. Hou
Key words: 4-(2-Pyrazinylthiomethyl)benzoic Acid, Metal-organic Chain, Hydrogen Bond, p-p Interactions, Supramolecular Structure 		444  Full Text
Amine Complexes of Silver(I) Disulfonylamides, Part I: Secondary Amines (In German)
E.-M. Zerbe, C. Wölper, and P. G. Jones
Key words: Silver, Amine, Disulfonylamine, Hydrogen Bonds 		449  Full Text
Syntheses, Structures and Photoluminescent Properties of the Two Novel Coordination Polymers [Cd(pydc)2(tu)]n and [Cd2(SO4)(nic)2(tu)1.5(H2O)2]n (pydc = Pyridine-2,3-dicarboxylate, nic = Nicotinate, tu = Thiourea)
C. Xu, S.-B. Liu, T. Duan, Q. Chen, and Q.-F. Zhang
Key words: Cadmium, Pyridine-dicarboxylate, Synthesis, Crystal Structure, Coordination Polymer 		459  Full Text
Synthesis, Crystal Structure and Magnetic Properties of an Iron(III) Pyridine-2,3,5,6-tetracarboxylate Complex
W. Xu, J.-L. Lin, H.-L. Zhu, F.-H. Hu, and Y.-Q. Zheng
Key words: Fe(III) Complex, Pyridine-2,3,5,6-tetracarboxylic Acid, Supramolecular Assembly, Magnetic Properties 		465  Full Text
Three New Coordination Compounds with Complex Cations [M(X)6]n+ (M = Co: X = H2O, NH3 and n = 3; N = Ni: X = H2O and n = 2) and Hydrogenacetylenedicarboxylate Anions (In German)
I. Stein and U. Ruschewitz
Key words: Cobalt, Crystal Structure Analysis, Hydrogenacetylenedicarboxylates, Hydrogen Bonds, Nickel 		471  Full Text
Synthesis of Substituted Benzoxazolinones by the Curtius Rearrangement: Crystal Structures of Intermediates and By-Products
G. Laus, V. Kahlenberg, K. Wurst, S. Nerdinger, and H. Schottenberger
Key words: Acyl Azide, Benzoxazolinone, Crystal Structure, Curtius Rearrangement 		479  Full Text
An Efficient Synthesis of 1-Thia-5-azaspiro[5.5]undec-2-ene and its Recyclization to 1,5-Diazaspiro[5.5]undec-2-ene and/or Spiro-Thieno[2,3-d]pyrimidin-4(1H)-one Derivatives
R. M. Shaker, A. Hamoda, Y. R. Ibrahim, K. M. El-Shaieb, and F. F. Abdel-Latif
Key words: 4-Oxo-1-phenylcyclohexanecarbonitrile, 1-Thia-5-azaspiro[5.5]undec-2-ene, Spiro-1,3-thiazine, Spiropyrimidine, Spiro-thieno[2,3-d]pyrimidine 		487  Full Text
Reactions of Nitroxides. Part XII. - 2,2,6,6-Tetramethyl-1-oxyl-4-piperidyl Chloroformate - A New Reactive Nitroxyl Radical. One-pot Synthesis of 2,2,6,6-Tetramethyl-1-oxyl-4-piperidyl N,N-Dialkyl-carbamates
J. Zakrzewski and M. Krawczyk
Key words: Diphosgene, Thiophosgene, Nitroxyl Radicals 		493  Full Text
A Quantum Chemistry Approach to the Force Fields of the Asymmetrical Thionyl Halides FS(O)Cl, CF3S(O)F and CF3S(O)Cl
A. d. C. Coronel, M. E. Gargiulo, E. L. Varetti, and L. E. Fernández
Key words: Thionyl Halides, Force Constants, Structure, DFT Calculations 		499  Full Text
Synthesis, Experimental and Theoretical Study on the Structure of Some Semicarbazides with Potential Antibacterial Activity
M. Pitucha, Z. Karczmarzyk, U. Kosikowska, and A. Malm
Key words: Semicarbazides, Keto-Enol Tautomerism, Gas Phase, Antibacterial Activity, RHF/SCF/6-31G** Calculations 		505  Full Text
New Substituted Thiazol-2-ylidene-benzamides and Their Reaction with 1-Aza-2-azoniaallene Salts. Synthesis and anti-HIV Activity (Erratum)
A. Saeed, N. A. Al-Masoudi, A. A. Ahmed, and C. Pannecouque
Key words: Anti-HIV Activity, Benzamides, Thiazolidones, Pyrazoles 		512  Full Text
Synthesis and Antitumor Activity of Ring A-modified Glycyrrhetinic Acid Derivatives
R. Csuk, S. Schwarz, B. Siewert, R. Kluge, and D. Ströhl
Key words: Glycyrrhetinic Acid, Antitumor Activity, Apoptosis 		521  Full Text
Assembly of 1,2,3,4-Benzenetetracarboxylic Acid and Zinc(II) Metal Centers to a Chiral 3D Metal-organic Framework: Syntheses, Structure and Properties
C. Ji, S.-Q. Zang, J.-Y. Liu, J.-B. Li, and H.-W. Hou
Key words: Homochiral, Helical, Metal-organic Framework, Topology, SHG, Photoluminescence 		533  Full Text
Notes
Synthesis and Crystal Structure of a New Cd(II) Coordination Polymer Based on a 1,10-Phenanthroline Derivative
Z.-L. Xu, S. Ma, Y. He, and Z.-G. Kong
Key words: Coordination Polymer, Crystal Structure, Octanedioic Acid, 2-(4-Fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline 		538  Full Text
NQR Study of AlBr3 Complexes with Dimethylsulfide
H. Ishihara, T. Sirahama, S. Nakashima, H. Terao, and K. Yamada
Key words: 81Br and 27Al NQR, Polymorphism, AlBr3 Complexes with (CH3)2S 		541  Full Text
Imidazolium Dicyanoargentates
E. Mallah, Q. Abu-Salem, K. Sweidan, N. Kuhn, C. Maichle-Mößmer, M. Steimann, M. Ströbele, and M. Walker
Key words: Imidazoles, Heterocycles, Dicyanoargentate, Crystal Structure 		545  Full Text
Synthesis, Crystal Structure and Luminescence Properties of the Inorganic-Organic Hybrid Compound [FTMA]2[CdI4] (FTMA = Ferrocenylmethyltrimethylammonium Cation)
Y. Bai, G. Q. Zhang, D. B. Dang, Z. Y. Qi, and L. Zhang
Key words: Inorganic-Organic Hybrid, Crystal Structure, Luminescence Properties 		549  Full Text
N u m b e r  6 (Graphical Abstracts)
Original Communications
Synthesis and Crystal Structure of a Meso-Meso Directly Linked Bisporphyrin
M. O. Senge, M. Pintea, and A. A. Ryan
Key words: Porphyrins, Conformational Analysis, Bisporphyrins, Tetrapyrroles, Crystal Structure 		553  Full Text
Cd4 Tetrahedra and Condensed RE6Rh Trigonal Prisms as Building Units in the Rare Earth-rich Compounds RE15Rh5Cd2 (RE = La, Ce, Pr, Nd)
F. Tappe, U. Ch. Rodewald, R.-D. Hoffmann, and R. Pöttgen
Key words: Intermetallics, Metal-rich Compounds, Crystal Structure 		559  Full Text
Chains of Condensed RuSm6/2 Octahedra in Sm3RuMg7 - A Ternary Ordered Version of the Ti6Sn5 Type
S. Linsinger and R. Pöttgen
Key words: Magnesium, Rare Earth Compounds, Crystal Structure 		565  Full Text
Synthesis, Crystal Structure and Properties of a New Lanthanide Pyridine-2,4,6-tricarboxylato Coordination Polymer
J.-L. Lin, W. Xu, L. Zhao, and Y.-Q. Zheng
Key words: Lanthanide, Pyridine-2,4,6-tricarboxylic Acid, Coordination Polymer, Crystal Structure, Properties 		570  Full Text
Mannich Bases as Synthetic Intermediates: Convenient Synthesis of Functionalized 1,2,4-Triazepines, 1,4-Diazepines and 1,5-Diazocines
E. M. Afsah, E. M. Keshk, A.-R. H. Abdel-Rahman, and N. F. Jomah
Key words: Mannich Bases, 1,2,4-Triazepines, 1,4-Diazepines, 1,5-Diazocines 		577  Full Text
Novel Phenylazo Derivatives of Condensed and Uncondensed Thiophene. Synthesis, Characterization, and Antimicrobial Studies
H. M. Gaber, M. C. Bagley, S. M. Sherif, and M. A. Sayed
Key words: Thienopyrimidinones, Hydrazinolysis, Cyclocondensation, Cyclodesulfurization, Antibacterial Activity 		585  Full Text
Enamines in Heterocyclic Synthesis: A Novel Simple and Efficient Route to Condensed Pyridazines
E. S. Darwish, M. A. Abdelrahman, and A. M. Salaheldin
Key words: Enamines, Pyridazinones, Amidoacetal, Pyridazinylenamine 		597  Full Text
Photocatalytic Ring Opening of a-Epoxyketones in Cyclopentanone
H. R. Memarian, G. Shokuhimehr, and M. Soleymani
Key words: Dioxolanes, Electron Transfer, a-Epoxyketones, Photocatalyst, Ring Opening, Spiro Compounds 		603  Full Text
Heterogeneously Catalyzed Diastereoselective Synthesis of 2-Nitro-1,3-di(pyridin-2-yl)propane-1,3-diols
M. Schulz, K. Wimmer, H. Görls, and M. Westerhausen
Key words: Heterogeneous Catalysis, Nitroaldol Reaction, N,O Ligands, Configuration Determination, Solid-state Structures 		611  Full Text
Dialiumoside, an Olean-18-ene Triterpenoid from Dialium excelsum
A. F. Awantu, B. N. Lenta, T. Bogner, Y. F. Fongang, S. Ngouela, J. D. Wansi, E. Tsamo, and N. Sewald
Key words: Dialium excelsum, Dialiumoside, Triterpenoids, Cytotoxicity, KB-3-1 and KB-V1 Cells 		624  Full Text
2-Hydroxy-luisol A, a New Quinone-derived Tetraol from a Marine Streptomyces sp. and Oxidation Products of Luisol A
S. Fotso, C. B. Fotso-Fondja Yao, E. Helmke, and H. Laatsch
Key words: Luisol, Marine Streptomycetes 		629  Full Text
Steroids from the South China Sea Gorgonian Coral Muricella flexuosa
P. Wang, S.-H. Qi, K.-S. Liu, L.-S. Huang, F. He, and Y.-F. Wang
Key words: Muricella flexuosa, Steroid, Steroidal Glycoside, Cytotoxicity 		635  Full Text
Chemical Constituents of Pedicularis densispica Franch
H. B. Chu, G. Z. Zeng, M. J. Zhu, W. J. He, Y. M. Zhang, and N. H. Tan
Key words: Scrophulariaceae, Pedicularis densispica, Densispicoside, Densispicnin C and D 		641  Full Text
Synthesis and Crystal Structure of a New Pb(II) Coordination Polymer Constructed by a 1,10-Phenanthroline Derivative and a Flexible Dicarboxylate
X.-Y. Wang, J. Guo, H.-L. Wang, and Q.-W. Wang
Key words: Coordination Polymer, Crystal Structure, trans-1,4-Cyclohexanedicarboxylic Acid,1-(1H-Imidazo[4,5-f][1,10]phenanthrolin-2-yl)naphthalen-2-ol 		647  Full Text
Intermetallic Compounds RETMg2 (RE = La, Pr, Nd; T = Ni, Pd, Pt) with MgCuAl2-type Structure
M. Kersting and R. Pöttgen
Key words: Magnesium, Intermetallics, Crystal Chemistry 		651  Full Text
Hydrothermal Synthesis and Crystal Structure of a Nickel(II) Coordination Polymer with 1,1'-Biphenyl-2,2'-dicarboxylato-6,6'-dicarboxylic Acid and 2,2':6,2"-Terpyridine Ligands
C.-Z. Mei, W.-W. Shan, and B.-T. Liu
Key words: Nickel(II), 1,1'-Biphenyl-2,2',6,6'-tetracarboxylic Acid, 2,2':6,2"-Terpyridine, Coordination Polymer, Thermal Analysis 		654  Full Text
N u m b e r  7 (Graphical Abstracts)
Original Communications
Two Organic Hybrid Thiogermanates [Ni(dien)2]2(H2dien)Ge2S6 and [Ni(teta)2]2Ge4S10
X. Liu, J. Zhou, J. He, and Z.-w. Huang
Key words: Thiogermanates, Solvothermal Syntheses, Crystal Structures, Complex Cation, Nickel 		659  Full Text
Ternary Stannides RE3Ru4Sn13 (RE = La, Ce, Pr, Nd) - Structure, Magnetic Properties, and 119Sn Mössbauer Spectroscopy
T. Mishra, C. Schwickert, T. Langer, and R. Pöttgen
Key words: Intermetallics, Rare Earth Compounds, Stannide, Crystal Structure 		664  Full Text
Intermetallic REPtZn Compounds with TiNiSi-type Structure
T. Mishra and R. Pöttgen
Key words: Intermetallics, Rare Earth Compounds, Crystal Structure 		671  Full Text
Synthesis, Characterization and Structure of Tribromo(2-phenyl-1,8-naphthyridine)gold(III)
R. Schmidt, S. A. Moya, P. Aguirre, M. Fuentealba, M. Leboschka, M. Sieger, M. Niemeyer, and W. Kaim
Key words: Crystal Structure, Gold Complexes, Naphthyridine Ligands, Intermolecular Interactions 		677  Full Text
Characterization and Crystal Structure of a Novel Two-dimensional Coordination Polymer: [Ni(bpdc)(bix)1.5 · H2O]n
L. H. Wei, Z.-L. Wang, and M.-X. Li
Key words: Crystal Structure, Coordination Polymer, Carboxylate, Topology 		681  Full Text
Two New Chromium(III) Complexes with the Pincer-type Pyridine-2,6-dicarboxylate Ligand
N. M. Halim, V. Abramov, I. Pantenburg, and G. Meyer
Key words: Chromium, Picolinic Acid, Complexes, Crystal Structure 		685  Full Text
Synthesis, Crystal Structure and Properties of a Cobalt(II) Coordination Polymer with Cyclohexane-1,2,3,4,5,6-hexacarboxylic Acid
W. Xu and Y.-Q. Zheng
Key words: Co(II) Complex, Cyclohexane-1,2,3,4,5,6-hexacarboxylic Acid, Coordination Polymer, Crystal Structure, Properties 		689  Full Text
Investigations of the Reactivity of the Lithiumphosphanide Li[PtBu2] towards GaCl3 (In German)
H.-W. Lerner, I. Sänger, F. Schödel, M. Bolte, and M. Wagner
Key words: Gallium, Phosphorus, Addition Compounds, X-Ray Structure Analysis 		695  Full Text
Triphenylphosphine-promoted C-Vinylation of 4-Hydroxyquinolines
B. Mohtat, S. Nahavandian, Z. N. Azar, H. Djahaniani, and Z. Hossaini
Key words: Acetylenic Ester, C-Vinylation, 4-Hydroxyquinoline, 2-Methyl-4-hydroxyquinoline, Triphenylphosphine 		700  Full Text
Isomers of Diformyl[2.2]paracyclophane; X-Ray Structure Determinations of the Pseudo-ortho Isomer and Two Polymorphs of the Pseudo-meta Isomer
P. G. Jones, I. Dix, M. Negru, and D. Schollmeyer
Key words: Paracyclophanes, X-Ray Structures, Secondary Interactions, Polymorphs 		705  Full Text
A Simple Route to Benz[a]acridinium Salts
H. Hartmann
Key words: Vilsmeier Reaction, 		711  Full Text
Concise Synthesis and Displacement Reactions of Model 3-(Alkylthio)-6-chloro- and 2,6-Dichlorothieno[2,3-e][1,4,2]dithiazine 1,1-Dioxides
R. Abu-El-Halawa, M. Masad, Y. Bathich, M. Al-Refai, M. M. Ibrahim, M. M. El-Abadelah, and W. Voelter
Key words: 2,5-Dichlorothiophene-3-sulfonamide, Cyclization with Carbon Disulfide, Thieno[2,3-e][1,4,2]dithiazine 1,1-Dioxides, SN-Ar Reactions 		715  Full Text
Imidazole-containing Bispidine Ligands: Synthesis, Structure and Cu(II) Complexation
M. Walther, M. Matterna, S. Juran, S. Fähnemann, H. Stephan, W. Kraus, and Franziska Emmerling
Key words: Piperidone, Bispidine, Copper(II), Configuration Isomerism 		721  Full Text
Sesquiterpene Lactones from Cichorium intybus
S. Shah, Z. Ali, A. Malik, I. A. Khan, and S. Saied
Key words: Cichorium intybus, Asteraceae, Sesquiterpene Lactones, 15-Hydroxytaraxacin, 6,8,11-epi-Desacetylmatricarin 		729  Full Text
Benzoic Acid Allopyranosides and Lignan Glycosides from the Twigs of Keteleeria evelyniana
W. J. He, Z. H. Fu, H. J. Han, H. Yan, G. Z. Zeng, C. J. Ji, H. B. Chu, Y. M. Zhang, and N. H. Tan
Key words: Keteleeria evelyniana, Pinaceae, Benzoic Acid Allopyranosides, Lignan Glycosides 		733  Full Text
Gingerol Derivatives from the Rhizomes of Zingiber Officinale
Z. Wang, K.-J. Wang, C.-S. Cheng, N. Li, T.-M. Wang, and L. Di
Key words: Zingiber officinale, Zingiberaceae, Gingerol Derivatives, [8]-Gingesulfonic Acid, [10]-Gingesulfonic Acid 		740  Full Text
Haliclocyclin C, a New Monomeric 3-Alkyl Pyridinium Alkaloid from the Arctic Marine Sponge Haliclona viscosa
G. Schmidt, C. Timm, and M. Köck
Key words: 3-Alkyl Pyridinium Alkaloid, Cyclic Monomer, HPLC-MS, High-resolution MS 		745  Full Text
Enicostemins A and B, New Secoiridoids from Enicostemma verticillatum
E. Jahan, I. Fatima, and A. Malik
Key words: Enicostemma verticillatum, Secoiridoids, Enicostemins A and B 		749  Full Text
Notes
Crystal and Molecular Structure of a New Hydroxylamido/Amino Acid Oxovanadium(V) Complex, [VO(NH2O)2(DL-methioninato)] · H2O
O. E. Piro, G. A. Echeverría, G. Arrambide, D. Gambino, and E. J. Baran
Key words: Oxovanadium(V) Complex, Amino Acid Complex, Hydroxylamido Complex, Crystal Structure 		752  Full Text
Synthesis and Structural Characterization of N,N'-Dipropyl-N,N,N',N'-tetramethyl-1,2-ethylenediammonium Dichloride and Dibromide
S. M. Närhi, J. Asikkala, J. Kostamo, M. K. Lajunen, R. Oilunkaniemi, and R. S. Laitinen
Key words: N,N'-Dipropyl-N,N,N',N'-tetramethyl-1,2-ethylenediammonium Dichloride/Dibromide, X-Ray Crystallography 		755  Full Text
A Novel Taxatetraene Framework Formed From a New Natural Taxane from Taxus cuspidata
Y. Li, Y.-L. Wang, Z.-Y. Ni, M. Dong, B. Cong, F. Sauriol, M.-L. Zhang, Y.-F. Wang, C.-H. Huo, Y.-C. Gu, Q.-W. Shi, and H. Kiyota
Key words: Taxus cuspidata, Taxanes, Taxatetraene, Structure Elucidation 		759  Full Text
N u m b e r  8 (Graphical Abstracts)
Original Communications
Ce2[MoO5][MoO4] and Ce5[MoO4]8: Two New Cerium Oxomolybdates, Each Exhibiting a Special Structural Feature
T. Schustereit, T. Schleid, and I. Hartenbach
Key words: Cerium, Oxomolybdates, Crystal Structure, Mixed Valency 		763  Full Text
Structure Refinement and Magnetic Properties of Ce2RuAl3 and a Group-Subgroup Scheme for Ce5Ru3Al2
T. Mishra, R.-D. Hoffmann, C. Schwickert, and R. Pöttgen
Key words: Cerium, Intermetallics, Crystal Structure, Magnetic Properties 		771  Full Text
Ternary Antimonides RE2Ir3Sb4 (RE = La, Ce, Pr, Nd)
K. Schäfer, W. Hermes, U. Ch. Rodewald, R.-D. Hoffmann, and R. Pöttgen
Key words: Rare Earth, Intermetallics, Crystal Structure, Magnetic Properties 		777  Full Text
m-Oxido-bis(pentammine iron(III))-chloride-ammonia(1/8), [Fe2(m-O)(NH3){10]Cl4 · 8NH3 (In German)
M. B. Fichtl, L. M. Scherf, S. A. Baer, and F. Kraus
Key words: Iron, Liquid Ammonia, X-Ray Structure, Quantumchemical Calculations 		784  Full Text
Aluminum Germanides of the Divalent Lanthanoides Eu and Yb: Synthesis, Structural Chemistry and Chemical Bonding (In German)
B. Bauer and C. Röhr
Key words: Aluminum, Ytterbium, Europium, Germanides, Crystal Structure, Band Structure Calculation 		793  Full Text
A Rare Example of a Dinuclear Cobalt(II) Complex with Dipicolinate and Bridging 2-Aminopyrazine Ligands. Preparation, Structural, Spectroscopic and Thermal Characterization
M. Tabatabaee, B.-M. Kukovec, and V. Razavimahmoudabadi
Key words: Cobalt, Dipicolinic Acid, 2-Aminopyrazine, Dinuclear Complex, X-Ray Diffraction 		813  Full Text
Synthesis, Crystal Structures, and Spectroscopic and Thermal Properties of New Cobalt Thiocyanato Coordination Compounds Based on 3-Methylpyridine as a Neutral Coligand
J. Boeckmann, B. Reimer, and C. Näther
Key words: Coordination Chemistry, Cobalt(II) Thiocyanate, Crystal Structures, Thermochemistry 		819  Full Text
Electronic Spectra and Photochemistry of Coordinated Astaxanthin
H. Kunkely and A. Vogler
Key words: Electronic Spectra, Luminescence, Photochemistry, Rhodium Complexes, Astaxanthin, Carotenoid 		828  Full Text
One-pot Synthesis of Dibenzofurans via SNAr and Subsequent Ligand-free Palladium-catalyzed Intramolecular Aryl-aryl Cross-coupling Reactions under Microwave Irradiation
Z. Che and H. Xu
Key words: Dibenzofurans, Ligand-free, Microwave, SNAr Reaction, Cross-coupling 		833  Full Text
An Efficient Synthesis of the Glycosidase Inhibitor 1,6-Dideoxy-6,6-difluoronojirimycin
R. Csuk, E. Prell, and Claudia Korb
Key words: Deoxynojirimycin, Fluorination, Reductive Amination, Glycosidase Inhibitor 		837  Full Text
5-Aminouracil as a Building Block in Heterocyclic Synthesis: Part IV. One-pot Synthesis of 1{H}-Pyrrolo[2,3-d]pyrimidine-2,4(3H,7H)-dione Derivatives Using Controlled Microwave Heating
R. M. Shaker, K. U. Sadek, E. A. Hafez, and M. A. Elrady
Key words: 5-Aminouracil, Dimedone, Barbituric Acid, Thiobarbituric Acid, Controlled Microwave Heating, One-pot Synthesis, Pyrrolo[2,3-d]pyrimidine-2,4-dione 		843  Full Text
Ab initio Computational Insight into the Interaction of Alkyl-substituted Ethene and Sulfenyl Halide
A. Vektariene and G. Vektaris
Key words: Quantum Chemical Calculations, Gibbs Free Energy Profile, Addition Reaction 		850  Full Text
New Secondary Metabolites from Croton sparsiflorus
R. Mehmood and A. Malik
Key words: Croton sparsiflorus, Euphorbiaceae, Inositol, Proaporphine Alkaloid 		857  Full Text
Notes
Addition of Organometallic Nucleophiles (Carbonylmetallates) to the Allyl Ligand of [(h3-C3H5)Pd(m-Cl)]2. Synthesis and Structure of (h3-C3H5)Mn(CO)3PEt3
T. Kerscher, S. Mihan, and W. Beck
Key words: Allyl, Carbonyl, Palladium, Manganese, X-Ray Structure Determination 		861  Full Text
mer-Triammine Trifluorido Iron(III), mer-[FeF3(NH3)3]
F. Kraus and S. A. Baer
Key words: Iron, Fluoride, Ammine, Crystal Structure, Liquid Ammonia 		865  Full Text
Tetraammine Tetrafluorido Cerium(IV) Ammonia (1/1), [CeF4(NH3)4] · NH3
F. Kraus and S. A. Baer
Key words: Cerium, Fluoride, Ammine, Crystal Structure, Liquid Ammonia 		868  Full Text
Caesium Tetrachlorido Aurate(III), CsAuCl4
F. Kraus
Key words: Caesium, Gold, Chloride 		871  Full Text
N u m b e r  9 (Graphical Abstracts)
Original Communications
The Mixed Lanthanum Dichalcogenide b-LaS1.86(1)Se0.14(1). Synthesis, Crystal Structure, Raman Spectrum and Optical Band Gap
C. Bartsch and T. Doert
Key words: Polychalcogenides, Rare Earth Metal, Crystal Structure, Raman Spectra 		873  Full Text
Solvothermal Syntheses and Crystal Structures of New One-dimensional Selenogallates [bappH2][Ga2Se4] (bapp = 1,4-Bis-(3-aminopropyl)piperazine) and [Mn(en)3][Ga2Se5] (en = Ethylenediamine)
C. Xu, J.-J. Zhang, T. Duan, Q. Chen, and Q.-F. Zhang
Key words: Selenogallate, Organic Amine, Polyselenide, Solvothermal Synthesis, Crystal Structure 		877  Full Text
Synthesis and Characterization of the Manganese Borate a-MnB2O4
S. C. Neumair, L. Perfler, and H. Huppertz
Key words: High Pressure, Borate, Crystal Structure 		882  Full Text
Synthesis and Crystal Structure of a Green Photoluminescent 1D Cobalt(II) Coordination Polymer Constructed from 2,2' Bibenzimidazole
Y. Yang, L.-T. Yan, X. Li, X.-M. Chen, R.-H. Qin, and W.-G. Duan
Key words: Cobalt(II) Complex, Crystal Structure, Fluorescence 		889  Full Text
Structure, Electrochemical and Magnetic Properties of a New Dinuclear Copper(II) Complex: [Cu2(C12H6O4N2)2(2,2'-bipy)2] · CH3OH
Y.-Q. Yang, M.-S. Chen, W. Li, and Z.-M. Chen
Key words: Copper(II) Complex, Crystal Structure, Magnetic Properties 		894  Full Text
Syntheses, Crystal Structures and Characterization of Two New Pb(II) and Cu(II) Coordination Polymers Based on 2-(4-Fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline and Benzenedicarboxylate Ligands
Z.-L. Xu, Y. He, and H.-L. Wang
Key words: Coordination Polymer, Crystal Structure, 1,3-Benzenedicarboxylate, 2-(4-Fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline 		899  Full Text
Preparation of Silver Nanoparticles Suitable for Textile Finishing Processes to Produce Textiles with Strong Antibacterial Properties against Different Bacteria Types
B. Mahltig, M. Reibold, E. Gutmann, T. Textor, J. Gutmann, H. Haufe, and H. Haase
Key words: Silver, Coatings, Textile, Antimicrobial, Nanoparticles 		905  Full Text
CO2 as an Oxygen Source for Polysiloxanes - Preparation, Crystal Structure and Thermal Decomposition of Two Novel Silylcarbamates
C. Wiltzsch, K. Kraushaar, A. Schwarzer, and E. Kroke
Key words: Polysiloxane, Silylamine, CO2 Insertion, Silylcarbamates, Crystal Structure 		917  Full Text
Preparation, Photophysical, Electrochemical, and Ion-Binding Properties of Ru(II) Polypyridyl Complexes Containing a Crown Ether Unit
F. Cheng, N. Tang, J. Chen, F. Wang, and L. Chen
Key words: Ru(II) Complex, Crown Ether, Photophysics, Electrochemistry, Ion Binding 		923  Full Text
Synthesis and Characterization of Three Novel Nitrogen-containing Macrolides
X. Leng, B. Yang, Y. Liu, Y. Xie, and J. Tong
Key words: Macrocycles, Macrolides, Synthesis, X-Ray Crystal Structure, Hydrogen Bonds 		930  Full Text
An Efficient Synthesis of Rubin's Aldehyde and its Precursor 1,3,5-Tribromo-2,4,6-tris(dichloromethyl)benzene
C. Holst, D. Schollmeyer, and H. Meier
Key words: Polyfunctional Aromatics, Hexasubstituted Benzenes, Hindered Rotation 		935  Full Text
Synthesis and Structures of Three- and Hexa-armed Benzene Derivatives Featuring Lateral Benzoic Ester and Benzoic Acid Functions
S. Förster, W. Seichter, and E. Weber
Key words: Tri- and Hexa-substituted Benzene Derivatives, Benzoic Acid, Benzoic Ester, X-Ray Diffraction Analysis 		939  Full Text
Synthesis and Characterization of o-Carboranylthioether Derivatives
M. Xu, Y. Nie, J. Miao, Z. Zhang, B. Peng, and G. Sun
Key words: o-Carborane, Thioether, Synthesis, Crystal Structure, Photoluminescence 		947  Full Text
Synthesis and anti-HIV Activity of New Benzimidazole, Benzothiazole and Carbohyrazide Derivatives of the anti-Inflammatory Drug Indomethacin
N. A. Al-Masoudi, N. N. A. Jafar, L. J. Abbas, S. J. Baqir, and C. Pannecouque
Key words: Anti-HIV Activity, Benzimidazole, Indomethacin, Non-nucleoside Reverse Transcriptase Inhibitors 		953  Full Text
Phenylisobenzofuranones from Fungicolous Nodulisporium sp. SH-1
S. Hayasaka, T. Koseki, T. Murayama, E. Kwon, and Y. Shiono
Key words: Phenylisobenzofuranone, Nodulisporones A and B, Fungicolous Fungus, Nodulisporium sp. SH-1, Antimicrobial Activity 		961  Full Text
An Efficient and Simple Route to Prospective Biologically Active Isoindoloquinazoline, Pyrimidine and Thiazine Derivatives Using 2-Amino-N'-Arylbenzamidine and Related Compounds as Starting Materials
F. F. Abdel-Latif, K. M. El-Shaieb, and A. G. El-Deen
Key words: Amidines, Aldehydes, Quinazolines, Thienopyrimidines, Thiazines 		965  Full Text
Notes
Crystal and Molecular Structure of Palladium(II) and Silver(I) Complexes with Oxotetrazolinate Ligands [1-Me-N4C(O)]-
H. Nöth, K. Burger, and W. Beck
Key words: Oxotetrazolinate, Palladium, Silver, Phosphines, X-Ray Crystallography 		972  Full Text
Synthesis and Crystal Structure Determination of a Guanidine Adduct of Sodium Guanidinate, NaCN3H4(CN3H5)2
V. Hoepfner, U. Englert, and R. Dronskowski
Key words: Guanidinate, Guanidine Adduct, Sodium, Crystal Structure, Hydrogen Bonds 		975  Full Text
Erratum
Z. Naturforsch. 2011, 66b, 512 - 520
A. Saeed, N. A. Al-Masoudi, A. A. Ahmed, and C. Pannecouque 		979  Full Text
N u m b e r  10 (Graphical Abstracts)
Original Communications
A Dodecanuclear Copper(I) Complex Containing a Cubic (CuS)4 Core Stabilized by a Tripodal (N,N,P)-Chelating Ligand
M. M. Meinholz and D. Stalke
Key words: Copper, Sulfur, Phosphorus, Sulfur Diimide, Ligand Design 		981  Full Text
Magnetic Properties of RE3Pd6Sb5 (RE = Pr, Nd, Gd) and a Group-Subgroup Scheme for Ce3Pd6Sb5 and Yb5Cu11Sn8
I. Schellenberg, R.-D. Hoffmann, S. Seidel, C. Schwickert, and R. Pöttgen
Key words: Antimony, Intermetallics, Magnetic Properties, Group-Subgroup Schemes 		985  Full Text
SrAu4.76In1.24 with YbMo2Al4-type Structure
I. Muts, S. F. Matar, U. Ch. Rodewald, V. I. Zaremba, and R. Pöttgen
Key words: Strontium, Indium, Crystal Structure, Intermetallic Compound 		993  Full Text
Syntheses and Crystal Structures of the Solid Solution Sr4OBr2.89(2)Cl3.11(2) and the Elusive Ba2OBr2
O. Reckeweg and Francis J. DiSalvo
Key words: Alkaline Earth Metal, Strontium, Barium, Oxide, Chloride, Bromide, Solid Solution, Structure Elucidation 		1000  Full Text
The Influence of d10-d10 Interactions in Ag5Te1.8Se0.2Cl and Ag5Te1.6Se0.4Cl on Structural and Thermoelectric Properties
N. Eckstein, J.-L. Bobet, B. Chevalier, and T. Nilges
Key words: Silver, Tellurium, Polytelluride, Thermoelectrics, d10-\d10 Interactions 		1005  Full Text
New Lanthanum Stannide/Germanides: La3Sn4.4Ge0.6, La3Sn3.1Ge0.9 and La9Sn6.7Ge3.3 (In German)
I. Dürr and C. Röhr
Key words: Lanthanum, Tetrelides, Stannides, Germanides, Band Structure Calculation 		1015  Full Text
Synthesis, Structure, and Spectral and Magnetic Properties of a Three-dimensional Cobalt(II)-Neodymium(III) Heterometal-Organic Framework Based on Oxydiacetic Acid
J.-X. Li, Z.-X. Du, and W.-P. Huang
Key words: Oxydiacetic Acid, Cobalt-Neodymium Complex, Fluorescence, EPR, Magnetic Properties 		1029  Full Text
Halogen Bonds in Two Silver(I) Mixed-ligand Supramolecular Frameworks: Synthesis, Structure and Photoluminescence
D. Sun, R.-B. Huang, and L.-S. Zheng
Key words: Silver(I), 2-Aminopyrimidine, Tetrachlorophthalic Acid, Halogen Bonds, Photoluminescence 		1035  Full Text
Preparation, Characterization, X-Ray Structure Determination and Solution Properties of some Novel Copper(I) Bisulfate and Sulfate Salts and Their Stable Derivatives
D. S. Gill, R. Singh, D. S. Rana, J. Wagler, and E. Kroke
Key words: Acetonitrile, Copper(I) Salts, Copper(I) Bisulfate, Copper(I) Sulfate, UV/Vis Spectra, Molar Conductance, 63Cu NMR 		1042  Full Text
Synthesis, Crystal Structure and DNA-Binding Properties of a Cadmium(II) Complex with 2,6-Bis(N-methylbenzimidazol-2-yl)pyridine
H. Wu, X. Huang, J. Yuan, F. Kou, F. Jia, B. Liu, and Y. Bai
Key words: 2,6-Bis(N-methylbenzimidazol-2-yl)pyridine, Cd(II) Complex, Crystal Structure, DNA-Binding Properties 		1049  Full Text
Synthesis of New Bisphosphonate and Bisphosphonic Acid Derivatives and Heterocyclic and Dialkylcarbamoyl Oxazolone Derivatives with Anticancer and Antischistosomal Activity
L. S. Boulos, E. F. Ewies, and A. F. M. Fahmy
Key words: 1,1-Bisphosphonate, 1,1-Bisphosphonic Acid, Wittig Reagents, Oxazolones, Anticancer Activity, Antischistosomal Activity 		1056  Full Text
Locking Out Ants - Synthesis and Biological Evaluation of Some Fluorinated Repellents
R. Csuk, M. G. Tamba, and R. Kluge
Key words: Fluorination, Trifluoromethyl Ketones, Repellents, Ants 		1069  Full Text
A New Triterpenoid Alkaloid from Buxus sempervirens
Y.-X. Yan, Y. Sun, J.-C. Chen, J. Su, Y. Li, and M.-H. Qiu
Key words: Buxus sempervirens, Triterpenoid Alkaloid, 16-Deacetoxy-hyrcamine, Cytotoxicity 		1076  Full Text
Notes
Calculation of 15N NMR Parameters of Azides and Some Related Compounds. Revisiting the Methylation of Nitrous Oxide N2O
B. Wrackmeyer
Key words: 15N NMR, Chemical Shifts, Nitrous Oxide, Methylation 		1079  Full Text
Diabietane Ether, a New Dimeric Abietane with an Ether Linkage from Taxus cuspidata Needles
Z.-Y. Ni, Y.-B. Wu, M. Dong, M.-L. Zhang, Y.-F. Wang, F. Sauriol, C.-H. Huo, Q.-W. Shi, Y.-C. Gu, H. Kiyota, and B. Cong
Key words: Taxus cuspidata, Abietanes, Diterpenes, Dimer, Structure Elucidation 		1083  Full Text
N u m b e r  11 (Graphical Abstracts)
Original Communications
Filling up another Gap: Synthesis and Crystal Structure of Ba2H3I
O. Reckeweg and F. J. DiSalvo
Key words: Barium, Iodide, Hydride, Structure Elucidation 		1087  Full Text
Syntheses, Single-crystal Structure and Vibrational Spectra of Ca15(CBN)6(C2)2H2
O. Reckeweg, A. Schulz, and F. J. DiSalvo
Key words: Acetylide, Calcium, CBN4- Anion, Hydride, Structure Elucidation, Vibrational Spectra 		1092  Full Text
Crystal Structure and Magnetic Properties of the Novel Hollandite Ba1.3Co1.3Ti6.7O16
L. Shlyk and R. Niewa
Key words: Hollandite, Cobaltate, Titanate 		1097  Full Text
The Gold-rich Indide Sr5Au13.5In8.5
I. Muts, U. Ch. Rodewald, V. I. Zaremba, and R. Pöttgen
Key words: Crystal Structure, Indide, Intergrowth Structure, Gold, Strontium 		1101  Full Text
Lanthanum Triel/Tetrel-ides La(Al,Ga)x}(Si,Ge)<1-x. Experimental and Theoretical Studies on the Stability of Intermetallic 1:1 Phases (In German)
I. Dürr, B. Bauer, and C. Röhr
Key words: Lanthanum, Gallium, Aluminum, Tetrelides, Band Structure Calculation 		1107  Full Text
Synthesis, Characterization and Crystal Structure of a Binuclear Cadmium Iodide Complex with a Multi-N-donor Oxazolidine Ligand
M. Hakimi, Z. Mardani, K. Moeini, M. Minoura, and H. Raissi
Key words: X-Ray Crystal Structure, Cadmium, Oxazolidine Ligand, Bridging Iodide 		1122  Full Text
Hydrothermal Synthesis and Structure of Two 1-D Organic Hybrid Metal Sulfates
X. Liu, J. Zhou, F. Hu, W. Yuan, and Z. Huang
Key words: Metal Sulfates, Crystal Structure, Hydrothermal Synthesis, Complex Cations 		1127  Full Text
Basic Beryllium ortho-Fluorobenzoate and its Mono-hydroxo Derivative
R. J. F. Berger, S. Jana, R. Fröhlich, and N. W. Mitzel
Key words: Beryllium, Cluster, Aryl-carboxylate, Crystal Structure 		1131  Full Text
Synthesis of Some 1,3-Dimethyl-6-substituted-1H-pyrazolo[3,4-b]pyrazin-5(4H)-ones
K. A. A. Safieh, F. S. Al-Masri, M. T. Ayoub, M. M. El-Abadelah, and W. Voelter
Key words: 5-Chloro-1,3-dimethyl-4-nitropyrazole, D,L-a-Amino Acids, SN-Ar Reactions, Pyrazolo[3,4-b]pyrazin-5-ones, Pyrazolo[4,3-e]pyrrolo[1,2-a]pyrazin-5-one 		1136  Full Text
Reaction Prediction using Density Functional Theory Calculations: A Study into the Synthesis of Safranal via Diels-Alder Reactions
G. Wagner, N. Vahdati, A. Howkins, and L. Cubitt
Key words: Cycloaddition, Diels-Alder Reaction, hetero-Diels-Alder Reaction, DFT Calculations, Safranal 		1141  Full Text
Synthesis, Structure, and Optoelectronic Properties of para- and meta-Bismethylborylbenzene Complexes of 5-Fluoro-2-(2'-pyridyl)indole (In German)
J. Heilmann-Brohl, F. Schödel, M. Bolte, M. Wagner, and H.-W. Lerner
Key words: BN Addition Compounds, 2-(2'-Pyridyl)indole Derivatives, Luminescence, X-Ray Structure Analysis 		1151  Full Text
Polysulfonylamines, CXCII. Polynary Compounds Based upon Di(4-fluorobenzenesulfonyl)amine (FAH), 1,1,3-Trimethylurea (TrMU) and Dimethylamine (Me2NH): Formation and Structures of the Cocrystal FAH · TrMU (Z' = 1), the Salt Me2NH2+ · FA$- (Z' = 6) and the Salt Cocrystal FAH · TrMU$· Me2NH2+ · FA- (Z' = 1). Comments on the Oxophobia of C-F Groups in Crystal Structures (In German)
C. Wölper, A. Rodríguez-Gimeno, K. C. Iborra, I. Dix, M. Freytag, P. G. Jones, and A. Blaschette
Key words: Cocrystals, Catemers via Hydrogen Bonding, Halogen Bonding, Oxophobia of C-F Groups, Sulfonamides 		1161  Full Text
Notes
Structure and Magnetic Properties of a Three-dimensional Cobalt Metal-Organic Framework
M.-S. Chen, W. Li, M.-B. Zhang, R.-Xi. Hu, C.-H. Zhang, and Z.-M. Chen
Key words: Metal-Organic Framework, Crystal Structure, Magnetic Properties 		1175  Full Text
Magnetic and Mössbauer Spectroscopic Characterization of EuNi2Sb2
I. Schellenberg, M. Eul, and R. Pöttgen
Key words: Europium, Antimonide, Mössbauer Spectroscopy 		1179  Full Text
The Solid Solution Lu2-xScxSiO5
H. B. Yahia, U. Ch. Rodewald, B. Heying, S. Balamurugan, and R. Pöttgen
Key words: Crystal Structure, Solid Solution, Silicate 		1183  Full Text
N u m b e r  12 (Graphical Abstracts)
Review
Barbituric Acid Utility in Multi-Component Reactions
R. M. Shaker and E. A. Ishak
Key words: Barbituric Acid Derivatives, Multi-Component Reactions, Pharmacological Activities 		1189  Full Text
Original Communications
2-Thiophenecarbohydrazides: A Novel Efficient Method for the Synthesis of 2-Thiophenecarbohydrazide
R. F. M. Elshaarawy and C. Janiak
Key words: Carbohydrazides, Thiophenecarbohydrazide, 2-Thiophenecarboxylic Hydrazide, 2-Thenoyl-hydrazine, Hydrogen Bonding 		1202  Full Text
Investigations into the Regioselectivity of Fischer Indole and Friedländer Quinoline Syntheses with Octahydroisobenzofuran and Octahydroisoindole Derivatives
M. Bender and J. Christoffers
Key words: Indoles, Quinolines, Isoindoles, Isobenzofurans, Carbazoles, Acridines, N-Heterocycles 		1209  Full Text
Intermetallic Cadmium Compounds M5T2Cd (M = Ca, Yb, Eu; T = Cu, Ag, Au) with Mo5B2Si-type Structure
F. Tappe, C. Schwickert, M. Eul, and R. Pöttgen
Key words: Cadmium, Intermetallics, Magnetic Properties 		1219  Full Text
Pyridine-promoted Cyclization of Functionalized N-Silylated Boron-Nitrogen Compounds
F. Schurz M. Jansen
Key words: Silazane Cleavage, Decomposition, Cyclization, Diazadiboretidine Derivatives, Crystal Structures 		1225  Full Text
Crystal Structure and Catalytic Properties of (C6H8N)3[PMo12O40]
T.-J. Cai, S.-Z. Lü, C.-L. Zhang, Y.-l. Huang, R.-y. Liu, and Q. Deng
Key words: Heteropolyoxoanion, 4-Picoline, Hydrothermal Method, Crystal Structure, Oxidative Elimination 		1231  Full Text
A Rare Two-dimensional Network Based on 2,2'-Biimidazole Bridged Double [PW11O39Ni]5- Polyanions
L.-H. Wei, Z.-L. Wang, and M.-X. Li
Key words: Polyoxometalate, Crystal Structure, Keggin, Topology 		1237  Full Text
Synthesis, Crystal Chemistry and Magnetism of the Metal-rich Borides MxRh7-xB3 (M = Cr, Mn, Ni; x = 0.39 - 1) with Th7Fe3-type Structure
P. R. N. Misse, R. Dronskowski, and B. P. T. Fokwa
Key words: Boron, Rhodium, Transition Metal Borides, Site Preference, Crystal Structure, Th7Fe3 Type, Paramagnetism 		1241  Full Text
The New Oxometallates Cs4[FeO3], Cs4[ZnO3] and Cs3[BO3] with Trigonal-planar Anions - Decomposition Products of Alkali Metal Suboxometallates
C. Hoch
Key words: Oxometallates, Cesium, Ferrates, Zincates, Borates, Crystal Structure, Topology 		1248  Full Text
Synthesis, Characterization and Luminescence of Silver(I) and Gold(I) Complexes Bearing a Diethyl Acetal Functionalized N-Heterocyclic Carbene
S. Leitner, M. List, and U. Monkowius
Key words: Silver(I), Gold(I), N-Heterocyclic Carbenes, Crystal Structure, Luminescence 		1255  Full Text
NQR, DSC, and X-Ray Structure Studies of Pyridinium Tetrabromozincate and Pyridinium Tetrabromocadmate (C5H5NH)2MBr4 · nH2O (M = Zn and Cd; n = 0, 1); Phase Transitions and Weak Hydrogen Bond Interactions
H. Ishihara, N. Hatano, K. Horiuchi, H. Terao, I. Svoboda, and H. Fuess
Key words: 81Br NQR, DSC, Phase Transition, Pyridinium Tetrabromometalates, Crystal Structure, Weak Hydrogen Bonds 		1261  Full Text
Salacetal, an Oleanane-type Triterpene from Salacia longipes var. camerunensis
B. M. Mba'ning, B. N. Lenta, S. Ngouela, D. T. Noungoué, F. Tantangmo, F. M. Talontsi, E. Tsamo, and H. Laatsch
Key words: Salacia longipes var. camerunensis, Celastraceae, Oleanane-type Triterpene, Salacetal 		1270  Full Text
Note
Cyclization of Unsaturated Alcohols. Mild and Efficient Selenocyclization of Pent-4-en-1-ol
M. D. Rvovi\'c, V. M. Divac, N. Radenkovi\'c, and Z. M. Bugar\vci\'c
Key words: Alcohol, Cyclization, Catalyst 		1275  Full Text