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Contents Vol. 65b (2010)

Headings and Complete Articles in PDF

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Graphical Abstracts: No 1, No 2

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N u m b e r  1 (Graphical Abstracts)
Original Communications
A First Experimental Electron Density Study on a C70 Fullerene: (C70C2F5)10
Key words: Fullerenes, Electron Density, Topological Analysis, Synchrotron Radiation
R. Kalinowski, M. Weber, S. I. Troyanov, C. Paulmann, and P. Luger 		1  Full Text
Crystal Structure of Silver Chromate Silicate, Ag6(CrO4)(SiO4)
Key words: Silver, Chromium, Silver Chromate Silicate, High Oxygen Pressure, Crystal Structure
W. Klein and M. Jansen 		8  Full Text
Sc2(MoO4)3 and Sc2(WO4)3: Halide Flux Growth of Single Crystals and 45Sc Solid-state NMR
Key words: Scandium, Crystal Chemistry, Solid-state NMR
S. Balamurugan, U. Ch. Rodewald, T. Harmening, L. v. Wüllen, D. Mohr, H. Eckert, and R. Pöttgen 		13  Full Text
On the Magnetic and Mössbauer Spectroscopic Characterization of EuPd2Sb2
Key words: Europium, Antimonides, Mössbauer Spectroscopy
I. Schellenberg, M. Eul, and R. Pöttgen 		18  Full Text
Mechano-thermally Activated Solid-state Synthesis of Li4Ti5O12 Spinel from Li2CO3-TiO2 Mixtures
Key words: Li4Ti5O12, Solid-state Synthesis, High-energy Milling, Molar Heat Capacity
V. Berbenni, C. Milanese, G. Bruni, and A. Marini 		23  Full Text
A Two-dimensional Rare Earth Metal-Organic Polymer {[Pr2(csph)2(H2O)4]· 6H2O}n with 3-Carboxylate-4-sulfonatophenolate (csph) Ligands
Key words: Praseodymium, Sulfosalicylic Acid, Fluorescence, Thermogravimetry
G. Wu, Z.-M. Wang, X.-T. Ge, X.-L. Wang, and Q.-F. Zhang 		27  Full Text
Syntheses and Structures of Silver(I) and Palladium(II) Complexes with Ferrocenyl-phosphonodithiolate Ligands
Key words: Synthesis, Crystal Structure, Ferrocenyl-dithiophosphonate, Heterobimetallic Complex
X.-Y. Wang, H.-T. Shi, Q. Ma, and Q.-F. Zhang 		32  Full Text
New Guanidinium-based Room-temperature Ionic Liquids. Substituent and Anion Effect on Density and Solubility in Water
Key words: Ionic Liquids, Guanidinium Salts, Density, Quaternization Reaction, DMF
M. G. Bogdanov, D. Petkova, S. Hristeva, I. Svinyarov, and W. Kantlehner 		37  Full Text
Structure and Properties of Non-classical Polymers. XV. 1D Polymers Possessing Two Bands with Ferromagnetically Coupled Electrons
Key words: Non-classical 1D Polymers, Molecular Magnets, Polymers with Two Half-filled Bands
N. Tyutyulkov, N. Drebov, K. Müllen, and F. Dietz 		49  Full Text
Copper-catalyzed Synthesis and Antimicrobial Activity of Disubstituted 1,2,3-Triazoles Starting from 1-Propargyluracils and Ethyl (4-Azido-1,2,3-trihydroxybutyl)furan-3-carboxylate
Key words: 1,3-Dipolar Cycloaddition, 1,2,3-Triazoles, 1,3,4-Oxadiazoles, Antimicrobial Activity
W. A. El-Sayed and A. A.-H. Abdel-Rahman 		57  Full Text
Effect of the Analytic Regions on the Quality Trend of Diamond-like/Graphitic Carbon Ratios in Raman Spectra
Key words: Raman Spectroscopy, Analytic Regions, Diamond-like Carbon, D Peak, G Peak, Peak Position, Deposition Time
A.-L. Shen, Y.-C. Weng, and T.-C. Chou 		67  Full Text
Thermolysis Reactions of Donor-free Silanimines tBu2Si=N-SiRtBu2 (R = tBu, Ph) (In German)
Key words: SiN Double Bond, Silanimine, Ene Reaction, X-Ray Structure Analysis
H.-W. Lerner, I. Sänger, M. Bolte, and M. Wagner 		72  Full Text
Two Novel Norlignan Derivatives from Curculigo breviscapa
Key words: Curculigo breviscapa, Hypoxidaceae, Norlignan Derivatives, Breviscaside A, Breviscapin B
N. Li, C.-C. Zhu, K.-J. Wang, and J.-M. Hu 		79  Full Text
Two New Clerodane Diterpenes from Dodonaea viscosa
Key words: Clerodane Diterpene, Dodonaea viscosa
Z. Huang, M.-Y. Jiang, Z.-Y. Zhou, and D. Xu 		83  Full Text
Brominated Metabolites from the Marine Red Alga Laurencia similis
Key words: Sesquiterpenoid, Indole Alkaloid, Laurencia similis
C.-S. Li, X.-M. Li, C.-M. Cui, and B.-G. Wang 		87  Full Text
Notes
151Eu Mössbauer Spectroscopic Characterization of EuRu4B4 and the New Boride EuRuB4
Key words: Europium, Borides, Mössbauer Spectroscopy
T. Harmening and R. Pöttgen 		90  Full Text
TaRhGe with TiNiSi-type Structure
Key words: Tantalum, Germanide, Crystal Structure, Pauli Paramagnetism
T. Dinges, M. Eul, and R. Pöttgen 		95  Full Text
Reaction of a Zwitterionic Pyridinium Ylide with N,N-Dimethylaniline
Key words: Heterocycles, Barbituric Acid, Crystal Structure
K. Sweidan, N. Kuhn, C. Maichle-Mößmer, and M. Steimann 		99  Full Text
N u m b e r  2 (Graphical Abstracts)
Original Communications
Formation of the Complexes [Fe(H2BDI)3]X2 and [CpCr(H2BDI)2]X2 (X = OTf) from the Unusual Reactions of Benzil-bis(trimethylsilyl)diimine with CpML2Cl (M = Fe, L = CO; M = Cr, L = NO)
Key words: Benzil-bis(trimethylsilyl)diimine, Benzildiimine, Crystal Structures, Iron, Chromium
N. Haque, B. Neumann, and I.-P. Lorenz 		101  Full Text
Thermal Isomerisation of a Sileneketazine to a Diazasilacyclopentene: Experimental and Theoretical Studies (In German)
Key words: Sileneketazine, Diazasilacyclopentene, Reaction Mechanism, Transition States, Density Functional Calculations
M. Görth, S. Abraham, S. Schmatz, H. Ott, D. Stalke, and U. Klingebiel 		107  Full Text
Tetra(alkynyl)silanes, a 3,6-Disila-triyne, a 3,6,9-Trisila-tetrayne, a 1,3,4,6-Tetrasiladiyne, and Bis(trimethylstannyl)ethyne. Molecular Structures and Solid-state NMR Studies
Key words: Alkynes, Silanes, Organotin Compounds, NMR, X-Ray
B. Wrackmeyer, E. Khan, A. Badshah, E. Molla, P. Thoma, O. L. Tok, W. Milius, R. Kempe, and J. Senker 		119  Full Text
Synthesis and Crystal Structure of Lead(II) Thenoyltrifluoroacetonate Complexes with Substituted 2,2'-Bipyridines: Interplay of Intermolecular Interactions in Crystals
Key words: Lead(II), Thenoyltrifluoroacetonate, Intermolecular Interactions
F. Marandi, Z. Nikpey, J. H. Goh, and H.-K. Fun 		128  Full Text
Supramolecular Assembly through the Highest Connectivity of a Keggin Polyoxometalate
Key words: Hydrothermal Synthesis, Supramolecular Chemistry, Keggin Polyoxometalate, Highest Connectivity, Electrochemistry
J.-Q. Sha, H.-Y. Liu, J. Peng, C. Wang, Y.-G. Lv, and P.-P. Zhang 		135  Full Text
Fabrication and Characterization of Antibacterial-active Multilayer Films Based on Keggin Polyoxometalates and Methylene Blue
Key words: Thin Films, Polyoxometalates, Methylene Blue, Atomic Force Microscopy, Antibacterial-activity
D. Chen, J. Peng, H. Pang, P. Zhang, Y. Chen, Y. Shen, C. Chen, and H. Ma 		140  Full Text
Synthesis and Structural Characterisation of a Hexanuclear TiIV Compound Ti6(m2-O)2(m3-O)2(m2-OC4H9)2(OC4H9)6(OOCCHCl2)8
Key words: Titanium, Butoxy, Oxo, Dichloroacetate, Crystal Structure
A. Pandey, A. Pandey, S. Singh, P. Mayer, and W. J. Parak 		147  Full Text
Self-assembly of a Novel Three-dimensional Silver(I) Supramolecular Framework from Cationic Chains and Anionic Sheets
Key words: Silver, 4,4'-Bipyridine, Hydrogen Bond, p···p Interactions, Photoluminescence Properties
D. Sun, C.-F. Yang, Z.-H. Wei, G.-G. Luo, N. Zhang, Q.-J. Xu, R.-B. Huang, and L.-S. Zheng 		152  Full Text
Synthesis and Crystal Structure of the Novel Three-dimensional Vanadium Coordination Compound Potassium Oxo-bis(hydroxylamido)malonatovanadate(V)
Key words: Vanadium Compounds, Hydroxylamine, Insulin Mimics, Malonic Acid
Q.-Y. Zhang, H.-Q. Zhang, A.-G. Kong, Q. Yang, and Y.-K. Shan 		157  Full Text
Synthesis and Structural Characterization of a New Two-dimensional Organic-Inorganic Hybrid Molybdoarsenate: [Cu(en)2]2[(CuO6)Mo6O18(As3O3)2]
Key words: Polyoxometalate, Hydrothermal Synthesis, Crystal Structure, Anderson-type Unit
Q. Wu, Q. Han, L. Chen, P. Ma, and J. Niu 		163  Full Text
Microwave-assisted Conversion of Carbohydrates into 5-Hydroxymethylfurfural Catalyzed by ZnCl2
Key words: Microwave-assisted Reaction, Degradation of Carbohydrate, 5-Hydroxymethylfurfural (HMF), Zinc Chloride
B. Zheng, Z. Fang, J. Cheng, and Y. Jiang 		168  Full Text
Reactions of 3,5-Dimethyl-1,2,4,3,5-trithiadiborolane with Secondary Amines: Formation of Diorganylamino(sulfhydryl)boranes
Key words: Diorganylamino(sulfhydryl)methylboranes, Dimeric Dimethylamino(sulfhydryl)methylborane
H. Nöth and T. Taeger 		173  Full Text
Synthesis, Crystal Structure and Antiproliferative Activity of 6-Adamantyl-3-aryl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazoles
Key words: Antiproliferative Activity, [1,2,4]Triazolo[3,4-b][1,3,4]thiadiazoles, Adamantyl Derivatives
M.-u.-H. Khan, T. Akhtar, K. A. Yasin, N. A. Al-Masoudi, P. G. Jones, and S. Hameed 		178  Full Text
Syntheses, Structures and Second-order Nonlinear Optical Behavior of (E)-N-(4-Nitrobenzylidene)-3,4-dimethylaniline and (E)-N-(3-Nitrobenzylidene)-3,4-dimethylaniline
Key words: X-Ray Diffraction, UV/Vis Spectroscopy, Electric Dipole Moment, First Hyperpolarizability, Configuration Interaction
H. Ünver, A. Karaka\cs, and T. N. Durlu 		185  Full Text
Enantioselective Synthesis of a 2,2-Disubstituted Tetrahydro-3-benzazepine as Novel NMDA Receptor Antagonist
Key words: NMDA Antagonists, X-Ray Crystal Structure Analysis, Isomerization, Asymmetric Synthesis, 2,2-Disubstituted Tetrahydro-3-benzazepines
S. M. Husain, R. Fröhlich, D. Schepmann, and B. Wünsch 		191  Full Text
Ring-opening Addition Reactions of 1-tert-Butoxycarbonyl-3,4-epoxypiperidine with Amine Nucleophiles
Key words: Epoxypiperidine, trans-b-Aminoalcohols, 4-Methoxyphenylpiperazine, 3-Methoxyaniline, Microwave Irradiation, Regioselectivity
B. Poojary and L. Hee-Jong 		197  Full Text
Phytochemical Studies on Alstonia scholaris
Key words: Alstonia scholaris, Apocynaceae, Triterpene, Flowers, Spectroscopic Studies
N. Sultana and M. Saleem 		203  Full Text
New Dibenzocyclooctadiene Lignans from Schisandra sphenanthera and Their Pro-inflammatory Cytokine Inhibitory Activities
Key words: Schisandra sphenanthera, Dibenzocyclooctadiene Lignans, Methylgomisin O, Chloromethyl Schisantherin B, Anti-inflammatory Activity
R. Ren, X.-X. Ci, H.-Z. Li, H.-M. Li, G.-J. Luo, R.-T. Li, and X.-M. Deng 		211  Full Text
N u m b e r  3 or later (in preparation)
Original Communications
304: Acridone Alkaloids and Coumarins from the Stem Bark of Citropsis articulata (Rutaceae)
Key words: Citropsis articulata, Rutaceae, Acridone Alkaloids, Coumarins
L. M. Meva'a, J. L. Songue, J. D. Wansi, A. F. K. Waffo, E. Dongo, T. N. Mpondo, and N. Sewald
312: Fluorescent Nano pH Indicators Based on Supramolecular Interactions
Key words: pH Indicators, Nano Particles, Fluorescence, Supramolecular Chemistry
H. Langhals and T. Pust
315 Vibrational Spectra of Phenylphosphonic and Phenylthiophosphonic Acid and their Complete Assignment
Key words: DFT and MP2 Calculations, Vibrational Spectra and Assignments, Torsional Potentials, Phenylphosphonic Acid, Phenythiolphosphonic Acid
W. Förner and H. M. Badawi
330: Isolation and X-Ray Characterization of {[Phthalazinium](CuCl2)}¥: A New Example of a Dichlorocuprate(I) Presenting a Rare Staircase Chain Structure
Key words: Copper(I), Phthalazine Ligand, Organic-Inorganic Hybride Compound, Non-coordinating Interactions, Crystal Structure
L. Plasseraud, H. Cattey, and P. Richard
333: Five-coordinate Zinc(II) Complexes Containing Sterically Demanding Bio-mimetic N3S2 Ligands. Syntheses, Characterization and DFT Calculations
Key words: Zinc Complexes, Amine Sulfur Ligands, Template Synthesis, Steric Hindrance, NMR, DFT Calculations
S. Y. Shaban, R. Puchta, and R. v. Eldik