Contents Vol. 65b (2010)
Authors Index

Headings and Complete Articles in PDF

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Graphical Abstracts: No 1, No 2, No 3, No 4, No 5, No 6, No 7, No 8, No 9, No 10, No 11, No 12

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N u m b e r  1 (Graphical Abstracts)
Original Communications
A First Experimental Electron Density Study on a C70 Fullerene: (C70C2F5)10
Key words: Fullerenes, Electron Density, Topological Analysis, Synchrotron Radiation
R. Kalinowski, M. Weber, S. I. Troyanov, C. Paulmann, and P. Luger
1  Full Text
Crystal Structure of Silver Chromate Silicate, Ag6(CrO4)(SiO4)
Key words: Silver, Chromium, Silver Chromate Silicate, High Oxygen Pressure, Crystal Structure
W. Klein and M. Jansen
8  Full Text
Sc2(MoO4)3 and Sc2(WO4)3: Halide Flux Growth of Single Crystals and 45Sc Solid-state NMR
Key words: Scandium, Crystal Chemistry, Solid-state NMR
S. Balamurugan, U. Ch. Rodewald, T. Harmening, L. v. Wüllen, D. Mohr, H. Eckert, and R. Pöttgen
13  Full Text
On the Magnetic and Mössbauer Spectroscopic Characterization of EuPd2Sb2
Key words: Europium, Antimonides, Mössbauer Spectroscopy
I. Schellenberg, M. Eul, and R. Pöttgen
18  Full Text
Mechano-thermally Activated Solid-state Synthesis of Li4Ti5O12 Spinel from Li2CO3-TiO2 Mixtures
Key words: Li4Ti5O12, Solid-state Synthesis, High-energy Milling, Molar Heat Capacity
V. Berbenni, C. Milanese, G. Bruni, and A. Marini
23  Full Text
A Two-dimensional Rare Earth Metal-Organic Polymer {[Pr2(csph)2(H2O)4]· 6H2O}n with 3-Carboxylate-4-sulfonatophenolate (csph) Ligands
Key words: Praseodymium, Sulfosalicylic Acid, Fluorescence, Thermogravimetry
G. Wu, Z.-M. Wang, X.-T. Ge, X.-L. Wang, and Q.-F. Zhang
27  Full Text
Syntheses and Structures of Silver(I) and Palladium(II) Complexes with Ferrocenyl-phosphonodithiolate Ligands
Key words: Synthesis, Crystal Structure, Ferrocenyl-dithiophosphonate, Heterobimetallic Complex
X.-Y. Wang, H.-T. Shi, Q. Ma, and Q.-F. Zhang
32  Full Text
New Guanidinium-based Room-temperature Ionic Liquids. Substituent and Anion Effect on Density and Solubility in Water
Key words: Ionic Liquids, Guanidinium Salts, Density, Quaternization Reaction, DMF
M. G. Bogdanov, D. Petkova, S. Hristeva, I. Svinyarov, and W. Kantlehner
37  Full Text
Structure and Properties of Non-classical Polymers. XV. 1D Polymers Possessing Two Bands with Ferromagnetically Coupled Electrons
Key words: Non-classical 1D Polymers, Molecular Magnets, Polymers with Two Half-filled Bands
N. Tyutyulkov, N. Drebov, K. Müllen, and F. Dietz
49  Full Text
Copper-catalyzed Synthesis and Antimicrobial Activity of Disubstituted 1,2,3-Triazoles Starting from 1-Propargyluracils and Ethyl (4-Azido-1,2,3-trihydroxybutyl)furan-3-carboxylate
Key words: 1,3-Dipolar Cycloaddition, 1,2,3-Triazoles, 1,3,4-Oxadiazoles, Antimicrobial Activity
W. A. El-Sayed and A. A.-H. Abdel-Rahman
57  Full Text
Effect of the Analytic Regions on the Quality Trend of Diamond-like/Graphitic Carbon Ratios in Raman Spectra
Key words: Raman Spectroscopy, Analytic Regions, Diamond-like Carbon, D Peak, G Peak, Peak Position, Deposition Time
A.-L. Shen, Y.-C. Weng, and T.-C. Chou
67  Full Text
Thermolysis Reactions of Donor-free Silanimines tBu2Si=N-SiRtBu2 (R = tBu, Ph) (In German)
Key words: SiN Double Bond, Silanimine, Ene Reaction, X-Ray Structure Analysis
H.-W. Lerner, I. Sänger, M. Bolte, and M. Wagner
72  Full Text
Two Novel Norlignan Derivatives from Curculigo breviscapa
Key words: Curculigo breviscapa, Hypoxidaceae, Norlignan Derivatives, Breviscaside A, Breviscapin B
N. Li, C.-C. Zhu, K.-J. Wang, and J.-M. Hu
79  Full Text
Two New Clerodane Diterpenes from Dodonaea viscosa
Key words: Clerodane Diterpene, Dodonaea viscosa
Z. Huang, M.-Y. Jiang, Z.-Y. Zhou, and D. Xu
83  Full Text
Brominated Metabolites from the Marine Red Alga Laurencia similis
Key words: Sesquiterpenoid, Indole Alkaloid, Laurencia similis
C.-S. Li, X.-M. Li, C.-M. Cui, and B.-G. Wang
87  Full Text
151Eu Mössbauer Spectroscopic Characterization of EuRu4B4 and the New Boride EuRuB4
Key words: Europium, Borides, Mössbauer Spectroscopy
T. Harmening and R. Pöttgen
90  Full Text
TaRhGe with TiNiSi-type Structure
Key words: Tantalum, Germanide, Crystal Structure, Pauli Paramagnetism
T. Dinges, M. Eul, and R. Pöttgen
95  Full Text
Reaction of a Zwitterionic Pyridinium Ylide with N,N-Dimethylaniline
Key words: Heterocycles, Barbituric Acid, Crystal Structure
K. Sweidan, N. Kuhn, C. Maichle-Mößmer, and M. Steimann
99  Full Text
N u m b e r  2 (Graphical Abstracts)
Original Communications
Formation of the Complexes [Fe(H2BDI)3]X2 and [CpCr(H2BDI)2]X2 (X = OTf) from the Unusual Reactions of Benzil-bis(trimethylsilyl)diimine with CpML2Cl (M = Fe, L = CO; M = Cr, L = NO)
Key words: Benzil-bis(trimethylsilyl)diimine, Benzildiimine, Crystal Structures, Iron, Chromium
N. Haque, B. Neumann, and I.-P. Lorenz
101  Full Text
Thermal Isomerisation of a Sileneketazine to a Diazasilacyclopentene: Experimental and Theoretical Studies (In German)
Key words: Sileneketazine, Diazasilacyclopentene, Reaction Mechanism, Transition States, Density Functional Calculations
M. Görth, S. Abraham, S. Schmatz, H. Ott, D. Stalke, and U. Klingebiel
107  Full Text
Tetra(alkynyl)silanes, a 3,6-Disila-triyne, a 3,6,9-Trisila-tetrayne, a 1,3,4,6-Tetrasiladiyne, and Bis(trimethylstannyl)ethyne. Molecular Structures and Solid-state NMR Studies
Key words: Alkynes, Silanes, Organotin Compounds, NMR, X-Ray
B. Wrackmeyer, E. Khan, A. Badshah, E. Molla, P. Thoma, O. L. Tok, W. Milius, R. Kempe, and J. Senker
119  Full Text
Synthesis and Crystal Structure of Lead(II) Thenoyltrifluoroacetonate Complexes with Substituted 2,2'-Bipyridines: Interplay of Intermolecular Interactions in Crystals
Key words: Lead(II), Thenoyltrifluoroacetonate, Intermolecular Interactions
F. Marandi, Z. Nikpey, J. H. Goh, and H.-K. Fun
128  Full Text
Supramolecular Assembly through the Highest Connectivity of a Keggin Polyoxometalate
Key words: Hydrothermal Synthesis, Supramolecular Chemistry, Keggin Polyoxometalate, Highest Connectivity, Electrochemistry
J.-Q. Sha, H.-Y. Liu, J. Peng, C. Wang, Y.-G. Lv, and P.-P. Zhang
135  Full Text
Fabrication and Characterization of Antibacterial-active Multilayer Films Based on Keggin Polyoxometalates and Methylene Blue
Key words: Thin Films, Polyoxometalates, Methylene Blue, Atomic Force Microscopy, Antibacterial-activity
D. Chen, J. Peng, H. Pang, P. Zhang, Y. Chen, Y. Shen, C. Chen, and H. Ma
140  Full Text
Synthesis and Structural Characterisation of a Hexanuclear TiIV Compound Ti6(m2-O)2(m3-O)2(m2-OC4H9)2(OC4H9)6(OOCCHCl2)8
Key words: Titanium, Butoxy, Oxo, Dichloroacetate, Crystal Structure
A. Pandey, A. Pandey, S. Singh, P. Mayer, and W. J. Parak
147  Full Text
Self-assembly of a Novel Three-dimensional Silver(I) Supramolecular Framework from Cationic Chains and Anionic Sheets
Key words: Silver, 4,4'-Bipyridine, Hydrogen Bond, p···p Interactions, Photoluminescence Properties
D. Sun, C.-F. Yang, Z.-H. Wei, G.-G. Luo, N. Zhang, Q.-J. Xu, R.-B. Huang, and L.-S. Zheng
152  Full Text
Synthesis and Crystal Structure of the Novel Three-dimensional Vanadium Coordination Compound Potassium Oxo-bis(hydroxylamido)malonatovanadate(V)
Key words: Vanadium Compounds, Hydroxylamine, Insulin Mimics, Malonic Acid
Q.-Y. Zhang, H.-Q. Zhang, A.-G. Kong, Q. Yang, and Y.-K. Shan
157  Full Text
Synthesis and Structural Characterization of a New Two-dimensional Organic-Inorganic Hybrid Molybdoarsenate: [Cu(en)2]2[(CuO6)Mo6O18(As3O3)2]
Key words: Polyoxometalate, Hydrothermal Synthesis, Crystal Structure, Anderson-type Unit
Q. Wu, Q. Han, L. Chen, P. Ma, and J. Niu
163  Full Text
Microwave-assisted Conversion of Carbohydrates into 5-Hydroxymethylfurfural Catalyzed by ZnCl2
Key words: Microwave-assisted Reaction, Degradation of Carbohydrate, 5-Hydroxymethylfurfural (HMF), Zinc Chloride
B. Zheng, Z. Fang, J. Cheng, and Y. Jiang
168  Full Text
Reactions of 3,5-Dimethyl-1,2,4,3,5-trithiadiborolane with Secondary Amines: Formation of Diorganylamino(sulfhydryl)boranes
Key words: Diorganylamino(sulfhydryl)methylboranes, Dimeric Dimethylamino(sulfhydryl)methylborane
H. Nöth and T. Taeger
173  Full Text
Synthesis, Crystal Structure and Antiproliferative Activity of 6-Adamantyl-3-aryl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazoles
Key words: Antiproliferative Activity, [1,2,4]Triazolo[3,4-b][1,3,4]thiadiazoles, Adamantyl Derivatives
M.-u.-H. Khan, T. Akhtar, K. A. Yasin, N. A. Al-Masoudi, P. G. Jones, and S. Hameed
178  Full Text
Syntheses, Structures and Second-order Nonlinear Optical Behavior of (E)-N-(4-Nitrobenzylidene)-3,4-dimethylaniline and (E)-N-(3-Nitrobenzylidene)-3,4-dimethylaniline
Key words: X-Ray Diffraction, UV/Vis Spectroscopy, Electric Dipole Moment, First Hyperpolarizability, Configuration Interaction
H. Ünver, A. Karaka\cs, and T. N. Durlu
185  Full Text
Enantioselective Synthesis of a 2,2-Disubstituted Tetrahydro-3-benzazepine as Novel NMDA Receptor Antagonist
Key words: NMDA Antagonists, X-Ray Crystal Structure Analysis, Isomerization, Asymmetric Synthesis, 2,2-Disubstituted Tetrahydro-3-benzazepines
S. M. Husain, R. Fröhlich, D. Schepmann, and B. Wünsch
191  Full Text
Ring-opening Addition Reactions of 1-tert-Butoxycarbonyl-3,4-epoxypiperidine with Amine Nucleophiles
Key words: Epoxypiperidine, trans-b-Aminoalcohols, 4-Methoxyphenylpiperazine, 3-Methoxyaniline, Microwave Irradiation, Regioselectivity
B. Poojary and L. Hee-Jong
197  Full Text
Phytochemical Studies on Alstonia scholaris
Key words: Alstonia scholaris, Apocynaceae, Triterpene, Flowers, Spectroscopic Studies
N. Sultana and M. Saleem
203  Full Text
New Dibenzocyclooctadiene Lignans from Schisandra sphenanthera and Their Pro-inflammatory Cytokine Inhibitory Activities
Key words: Schisandra sphenanthera, Dibenzocyclooctadiene Lignans, Methylgomisin O, Chloromethyl Schisantherin B, Anti-inflammatory Activity
R. Ren, X.-X. Ci, H.-Z. Li, H.-M. Li, G.-J. Luo, R.-T. Li, and X.-M. Deng
211  Full Text
N u m b e r  3 (Graphical Abstracts)
Preface to the 70th Birthday Celebration Issue for Professor Rolf W. Saalfrank (In German)
R. Puchta and A. Scheurer
219  Full Text
Original Communications
High-Pressure Study of Oxo-bridged Mixed-Valent MnIII/MnIV Dimers
Key words: High Pressure, Coordination Chemistry, Clusters, X-Ray Crystallography, SQUID Magnetometry
A. Prescimone, J. Sanchez-Benitez, K. V. Kamenev, J. E. Warren, A. R. Lennie, M. Murrie, S. Parsons, and E. K. Brechin
221  Full Text
Can Metallocryptands act as Proton Cages? - DFT Study of Proton Affinity in [2.2.2]-analogous Metallocryptands (In German)
Key words: Metallocryptand, Cryptand, Proton Sponge, Proton Affinity, DFT Calculations
R. Puchta and A. Scheurer
231  Full Text
Bond Activation in Iron(II) and Nickel(II) Complexes of Polypodal Phosphanes
Key words: Bond Activation, N/P Ligands, Polypodal Ligands, Agostic Interaction, Iron, Nickel
S.-A. Gentschow, S. W. Kohl, W. Bauer, F. W. Heinemann, D. Wiedemann, and A. Grohmann
238  Full Text
Five-coordinate Zinc(II) Complexes Containing Sterically Demanding Bio-mimetic N3S2 Ligands. Syntheses, Characterization and DFT Calculations
Key words: Zinc Complexes, Amine Sulfur Ligands, Template Synthesis, Steric Hindrance, NMR, DFT Calculations
S. Y. Shaban, R. Puchta, and R. v. Eldik
251  Full Text
A Novel Five-coordinate Mn Complex with a Redox-active SNNNS Ligand System
Key words: Manganese, Five-coordinate Complexes, SNNNS Ligation, Superoxide
K. Dürr, D. A. Yalalov, F. W. Heinemann, S. B. Tsogoeva, and I. Ivanovi\'c-Burmazovi\'c
258  Full Text
Disruption of the La(III)[15-Metallacrown-5] Cavity through Bithiophene Dicarboxylate Inclusion
Key words: Metallacrown, Molecular Recognition, Host-Guest Chemistry, Bithiophene, Metallamacrocycle
J. Jankolovits, C.-S. Lim, J. W. Kampf, and V. L. Pecoraro
263  Full Text
Binuclear Cofacial Metallocycles of Copper and Nickel: Synthesis and Structure (In German)
Key words: N,O-Ligand, Metallocycle, Cage Compound, Self-assembly, Supramolecular Chemistry
W. Bauer, F. Hampel, and H. Maid
273  Full Text
Structural Properties of Ruthenium Biimidazole Complexes Determining the Stability of their Supramolecular Aggregates
Key words: Ruthenium, Biimidazole, Bibenzimidazole, Supramolecular Chemistry, Hydrogen Bonds
N. Rockstroh, K. Peuntinger, H. Görls, D. M. Guldi, F. W. Heinemann, B. Schäfer, and S. Rau
281  Full Text
Fluorescent Nano pH Indicators Based on Supramolecular Interactions
Key words: pH Indicators, Nano Particles, Fluorescence, Supramolecular Chemistry
H. Langhals and T. Pust
291  Full Text
Synthesis and Characterization of the Heptanuclear [MnIII6CoIII]3+ Triplesalen Complex: Evidence for Exchange Pathways Involving Low-spin CoIII
Key words: Magnetic Properties, Heteronuclear Complexes, Exchange Pathways
E. Krickemeyer, V. Hoeke, A. Stammler, H. Bögge, J. Schnack, and T. Glaser
295  Full Text
Supramolecular Architectures of Copper(II) Perchlorate Complexes of cis,trans-1,3,5-Triaminocyclohexane Assembled Exploiting the Delicate Balance Between Weak and Strong Interactions
Key words: Self-assembly, Stoichiometry Control, Coordination Complexes, Supramolecular Chemistry, Hydrogen Bonding Networks
M. N. Corella Ochoa, G. J. T. Cooper, G. N. Newton, D.-L. Long, G. Seeber, and L. Cronin
304  Full Text
Changing the Overall Shape of Heterodinuclear Helicates via Substitution of Acylhydrazones by Tosylhydrazones
Key words: Self-assembly, Helicates, Heteronuclear, Catechol, Hydrazone
M. Albrecht, I. Latorre, Y. Liu, and R. Fröhlich
311  Full Text
Isolation and X-Ray Characterization of {[Phthalazinium](CuCl2)}¥: A New Example of a Dichlorocuprate(I) Presenting a Rare Staircase Chain Structure
Key words: Copper(I), Phthalazine Ligand, Organic-Inorganic Hybride Compound, Non-coordinating Interactions, Crystal Structure
L. Plasseraud, H. Cattey, and P. Richard
317  Full Text
A Promising New Schiff Base-like Ligand for the Synthesis of Octahedral Iron(II) Spin Crossover Complexes
Key words: Schiff Base-like Ligand, Iron Complexes, Magnetic Properties
W. Bauer, T. Ossiander, and B. Weber
323  Full Text
Enantiomerically Pure {C}2-symmetric Dinuclear Silver(I) and Copper(I) Complexes from a Bis(2,2'-bipyridine)-substituted 9,9'-Spirobifluorene Ligand
Key words: Self-assembly, Helicates, 2,2'-Bipyridines, 9,9'-Spirobifluorene, Diastereoselectivity
T. Piehler and A. Lützen
329  Full Text
Enantioselective Biocatalytic Reduction of Non-protected Hydroxyacetophenones
Key words: Alcohols, Asymmetric Synthesis, Biocatalysis, Enzymes, Reduction
A. Neupert, T. Ress, J. Wittmann, W. Hummel, and H. Gröger
337  Full Text
Platinum Complexes with Picoline-functionalized Benzimidazolin-2-ylidene Ligands
Key words: Heterocyclic Carbene Complexes, Platinum(II) Complexes
M. C. Jahnke, T. Pape, and F. E. Hahn
341  Full Text
Catalysis of the Quadricyclane to Norbornadiene Rearrangement by SnCl2 and CuSO4
Key words: Ab initio Calculations, Density Functional Calculations, Electron Transfer, Catalysis, Rearrangement
T. E. Shubina and T. Clark
347  Full Text
Vibrational Spectra of Phenylphosphonic and Phenylthiophosphonic Acid and their Complete Assignment
Key words: DFT and MP2 Calculations, Vibrational Spectra and Assignments, Torsional Potentials, Phenylphosphonic Acid, Phenythiolphosphonic Acid
W. Förner and H. M. Badawi
357  Full Text
Understanding Selectivities in Ligand-free Oxidative Cyclizations of 1,5- and 1,6-Dienes with RuO4 from Density Functional Theory
Key words: Oxidative Cyclization, DFT, Cycloaddition
P. J. d. Dio, S. Zahn, C. B. W. Stark, and B. Kirchner
367  Full Text
Ligand vs. Metal Basicity: Reactions of 2-(Diphenylphosphanyl)anilido and 2-(Diphenylphosphanyl)phenolato Complexes of Rhodium(I) and Iridium(I) with HBF4
Key words: P,O Ligands, P,N Ligands, Rhodium Complexes, Iridium Complexes, Protonation
L. Dahlenburg and K. Herbst
376  Full Text
Mono- and Di-Lanthanide Derivatives of 19-Tungsto-2-Arsenate(III)
Key words: Arsenic, Lanthanides, Polyoxometalates, Tungsten, X-Ray Crystal Structure
A. H. Ismail, B. S. Bassil, I. Römer, N. C. Redeker, and U. Kortz
383  Full Text
Microspectroscopic Analysis of the X-Ray-induced Photoreduction in Fe- and Mn-containing SMMs
Key words: Single-molecule Magnet (SMM), X-Ray Absorption, X-Ray Microspectroscopy, STXM, Photoreduction
N. Schmidt, A. Scheurer, S. Sperner, and R. H. Fink
390  Full Text
Mineralization of Phenol and 4-Chlorophenol Induced by Visible Light and Assisted by Semiconducting b-Bi2O3
Key words: Bismuth Oxide, Fermi Level, Photocatalysis, Semiconductor, Visible Light
J. Eberl and H. Kisch
399  Full Text
Ligand Exchange Processes on Solvated Lithium Cations. VI. Determination of Coordination Numbers by Ligand Substitution and 7Li NMR
Key words: Lithium Complex Formation, 7Li NMR, N Chelates, DFT Calculations
M. Schmeisser, A. Zahl, A. Scheurer, R. Puchta, and R. v. Eldik
405  Full Text
Syntheses and Palladium, Platinum, and Borane Adducts of Symmetrical Trialkylphosphines with Three Terminal Vinyl Groups, P((CH2)mCH=CH2)3
Key words: Phosphine, Phosphine Borane, Palladium, Platinum, a,w-Diene
A. J. Nawara-Hultzsch, K. Skopek, T. Shima, M. Barbasiewicz, G. D. Hess, D. Skaper, and J. A. Gladysz
414  Full Text
Push-Pull-Allenes: The Influences of Substituents on the Activation of Allenes by Biomimetic Zinc Complexes
Key words: Allenes, Substitution Effects, Carbonic Anhydrase, Cumulene Activation
B. O. Jahn, W. A. Eger, and E. Anders
425  Full Text
N u m b e r  4 (Graphical Abstracts)
Original Communications
Secondary Interactions in Crystals of all Ten Isomers of Di(bromomethyl)naphthalene
Key words: Di(bromomethyl)naphthalenes, Solid-state Structure, Weak Hydrogen Bonds, Bromine-Bromine Contacts
P. G. Jones and P. Ku\'s
433  Full Text
First Total Synthesis of a Fluorinated Calystegin
Key words: Calystegin, Ring Closure Metathesis, Glucosidase Inhibitor
R. Csuk, E. Prell, S. Reißmann, and C. Korb
445  Full Text
Electron Density of Corannulene from Synchrotron Data at 12 K, Comparison with Fullerenes
Key words: Electron Density, Topological Analysis, Synchrotron Radiation, Corannulene
S. Grabowsky, M. Weber, Y.-S. Chen, D. Lentz, B. M. Schmidt, M. Hesse, and P. Luger
452  Full Text
H3PW12O40: An Efficient and Recyclable Heterogeneous Catalyst for the Selective Synthesis of 2-Aryl-5,6-dihydro-4H-1,3-oxazines and 2-Aryl-1,4,5,6-tetrahydropyrimidines
Key words: Oxazines, Tetrahydropyrimidines, Microwave Irradiation, Solid Acid Catalyst, Tungstophosphoric Acid
I. Mohammadpoor-Baltork, M. Moghadam, S. Tangestaninejad, V. Mirkhani, and Z. Eskandari
461  Full Text
Synthesis and Site-selective Metalation of a Benzene-o-dithiol/Pyridylimine Ligand
Key words: Heterodonor Ligands, S-S Ligands, N-N Ligands, Titanium, Schiff Bases
J. Dömer, T. Pape, and F. E. Hahn
470  Full Text
Crystal and Molecular Structure of 3-(N-Methoxy-N-methylcarbamoyl)-2,2,5,5-tetramethyl-1-oxy-pyrroline
Key words: Crystal Structure, Nitroxide, Radical
G. D. Frey and E. Herdtweck
475  Full Text
Synthesis and Structural Characterization of Diisopropylammonium Trifluoroacetate and Diisoproplyammonium Pentafluoropropionate
Key words: Diisopropylammonium Cation, Hydrogen Bonding, Crystal Engineering, Carboxylates
G. J. Reiß and M. K. Meyer
479  Full Text
Synthesis of 3,4-Dihydropyrimidin-2(1H)-one-5-carboxamides
Key words: Biginelli Reaction, 3,4-Dihydropyrimidine-5-carboxamides, Microwave, ZrCl4, Zirconium Salts
M. Soleymani and H. R. Memarian
485  Full Text
New Calcium Hydride Halides with Familiar Structures. Syntheses and Crystal Structures of Ca7H12Cl2 and Ca2H3Br
Key words: Calcium, Halide, Hydride, Structure Elucidation, EUTAX Calculations
O. Reckeweg and F. J. DiSalvo
493  Full Text
1H NMR Studies on the Cation Motions in Crystalline Cadmium Bromide Complexes [C(NH2)3]Cd2Br5, [(CH3)3NH]3Cd2Br7, and [i-C3H7NH3]CdBr3
Key words: 1H NMR, T1, DSC, Phase Transition, Cationic Motion
H. Ishihara, K. Horiuchi, and Y. Furukawa
499  Full Text
Metal Complexes of Biologically Important Ligands, CLXXIV. Palladium(II) and Platinum(II) Complexes with Schiff Bases from 2-(Diphenylphosphino)benzaldehyde and a-Amino Acid Esters
Key words: 2-(Diphenylphosphino)benzaldehyde, 2-Formylphenyldiphenylphosphine, Palladium, Platinum, a-Amino Acid Esters, Schiff Bases
B. Schreiner, C. Robl, B. Wagner-Schuh, and W. Beck
503  Full Text
Synthesis, Crystal Structure and Luminescence Properties of a Cyclometalated Ir(III) Complex of 3,4-Diphenylcinnoline
Key words: Iridium(III) Complex, 3-Phenylcinnoline, Crystal Structure, Photoluminescence
B.-H. Tong, F.-H. Wu, Q.-B. Mei, and Q.-F. Zhang
511  Full Text
Organic-Inorganic Hybrid Compounds Based on Lead Halide Units: Preparation from Melts and through Grinding Effects
Key words: Organic-Inorganic Hybrids, Optical Properties
G. C. Papavassiliou, G. A. Mousdis, and G. C. Anyfantis
516  Full Text
Terpenoids from Clerodendrum formicarum Gürke (Lamiaceae) of Cameroon
Key words: Formidiol, abeo-Abietane, Leaves, Clerodendrum formicarum, Lamiaceae, Characterization, Spectroscopy
M. S. Ali, Z. Ahmed, J. Ngoupayo, and M. I. Ali
521  Full Text
Acridone Alkaloids and Coumarins from the Stem Bark of Citropsis articulata (Rutaceae)
Key words: Citropsis articulata, Rutaceae, Acridone Alkaloids, Coumarins
L. M. Meva'a, J. L. Songue, J. D. Wansi, A. F. K. Waffo, E. Dongo, T. N. Mpondo, and N. Sewald
525  Full Text
Original Notes
Single-Crystal X-Ray Diffraction Study of Na[OCN] at 170 K and its Vibrational Spectra
Key words: Sodium, Cyanate, Disordered Anion, Structure Elucidation, Vibrational Spectroscopy
O. Reckeweg, A. Schulz, B. Leonard, and F. J. DiSalvo
528  Full Text
1,3-Dialkyl-5-hydroxy-2-thioxoimidazolidin-4-ones (In German)
Key words: Heterocycles, Imidazolidines, Silylation, Crystal Structure
N. Kuhn, C. Maichle-Mößmer, M. Steimann, I. Walker, and K.-P. Zeller
533  Full Text
N u m b e r  5 (Graphical Abstracts)
Original Communications
Li13.7Rh8Si18.3 - A Non-Centrosymmetric Variant of the R-Phase Structure
Key words: Lithium, Silicide, Group-Subgroup, Crystal Structure
T. Dinges, R.-D. Hoffmann, and R. Pöttgen
537  Full Text
The New Niobium Cluster Azides (NH4)4[Nb6Cl12(N3)6](H2O)2 and Na1.15(3)La0.85(3)[Nb6Cl12(N3)6](H2O)13(1). Syntheses and Crystal Structure Determination
Key words: Azide, Cluster, Niobium, Alkaline Earth Metal, Rare Earth Metal
O. Reckeweg and A. Simon
543  Full Text
Condensed [OPr4]10+ and Discrete [AsO3]3-- Y1-Tetrahedra in Pr5O4Cl[AsO3]2
Key words: Oxide Chlorides, Oxoarsenites, Rare-earth Compounds, Crystal Structures
H. B. Yahia, A. Villesuzanne, U. Ch. Rodewald, T. Schleid, and R. Pöttgen
549  Full Text
N-Dimethylphosphinoyl-substituted Aminomethanephosphonic Acids
Key words: Phosphinoyl-substituted Aminomethanephosphonic Acids, Moedritzer-Irani Reaction, Aminophosphonic Acids, X-Ray Diffraction, Electrospray Ionization Mass Spectrometry
V. Lachkova, S. Varbanov, W. Frank, and H. Keck
556  Full Text
Ab initio Molecular and Solid-state Studies of the Spin Crossover System [Fe(phen)2(NCS)2]
Key words: Spin Crossover, DFT, Inorganic Complexes, Raman, IR, Equation of State
S. F. Matar and J.-F. Létard
565  Full Text
Synthesis and Properties of 3,6-Diamino-substituted 1,2,4-Triazin-5(2H)-ones (In German)
Key words: 3,6-Diamino-1,2,4-triazin-5(2H)-ones, Ethyl 2-Amino-2-thioxoacetate, Acylation, N-2-Acyl-1,2,4-triazin-5(2H)-ones, Ultrasound Synthesis
D. Geffken and M. A. Köllner
571  Full Text
Structural and Computational Studies of 1-Methyl-2-thiocytosine and its Coordination Mode in a Dinuclear Platinum(IV) Complex [(PtMe3)2(m-1-MeSCy-1kN3,1:2k2S)2][BF4]2
Key words: Thionucleobases, Platinum Complexes, Hydrogen Bonding, Single-crystal X-Ray Diffraction Analysis, DFT Calculations
C. Vetter, C. Wagner, R. Kluge, and D. Steinborn
578  Full Text
Synthesis and Cyclisation of Boryl- and Silylhydrazones (In German)
Key words: Borylhydrazone, Silylhydrazone, Diazasilacyclopentene, Diazaboracyclopentene, Diazasilacyclopentadiene, One-electron Oxidation
M. Görth, U. Schneider, H. Ott, C. Schulzke, D. Stalke, and U. Klingebiel
587  Full Text
Synthesis and Characterization of Fluorescent Polyoxometalate Nano-/Microrods
Key words: Nano-/Microrods, Polyoxometalates, Photoluminescence Properties
Y. Shen, J. Peng, C. Chen, D. Chen, H. Zhang, and C. Meng
603  Full Text
Synthesis and Crystal Structure of a New 1D Oxamidato-bridged Heterobimetallic Polymer
Key words: Copper, Zinc, Oxamidato Bridging, Coordination Polymer, Crystal Structure
W. J. Lou, Y. Zhang, H. Cui, B. L. Liu, and R. J. Tao
607  Full Text
Crystal Structures of Some N-substituted 2,5-Dimethylpyrrole Derivatives
Key words: N-Pyrrole Derivatives, 2,5-Dimethylpyrrole, Solid-state Structure
P. G. Jones, P. Ku\'s, M. \Lannik, and V. Kozik
611  Full Text
Synthesis and Antimicrobial Evaluation of Some New 2-(6-Oxo-5,6-dihydro[1,3]thiazolo[3,2-b]-2-aryloxymethyl-1,2,4-triazol-5-yl)-N-arylacetamides
Key words: 1,2,4-Triazole-3-thiol, N-Aryl-maleimides, Antibacterial, Antifungal
P. L. Lobo, B. Poojary, K. Manjunatha, and N. S. Kumari
617  Full Text
Sesterterpenes from the Sponge Dysidea sp.
Key words: Sesterterpene, Sponge, Dysidea sp., Scalarane
X. Yang, Z. Shao, and X. Zhang
625  Full Text
Polystachyasaponin with Adjuvant Activity from Entada polystachya
Key words: Entada polystachya, Leguminosae, Polystachyasaponin, Complex Triterpenoid Saponin, Ovalbumin, Adjuvant Activity
B. P. d. Silva and J. P. Parente
628  Full Text
A New Taxane from the Hard Wood of Taxus cuspidata
Key words: Taxus cuspidata, Yew, Taxaceae, Hard Wood, Taxanes
S.-H. Yu, M.-l. Zhang, Y.-F. Wang, C.-H. Huo, Y.-C. Gu, and Q.-W. Shi
635  Full Text
Crystal Structure of the Arsenate(V) NaTi2[AsO4]3
Key words: Crystal Structure, Nasicon, Arsenate(V), Single Crystal Diffraction, Salt Flux Synthesis
H. B. Yahia, U. Ch. Rodewald, and R. Pöttgen
639  Full Text
Synthesis and Crystal Structure of Barium Indide Ba9In4
Key words: Indium, Barium, Binary Indides, Crystal Structure
V. Smetana and A. Simon
643  Full Text
N u m b e r  6 (Graphical Abstracts)
Original Communications
A Simple System with many Structural Variants: A Reexamination of (Amine)halogenidosilver(I) Complexes (In German)
Key words: Silver, Halides, Hydrogen Bonds, Amines
C. Wölper, M. D. P. Bastardés, I. Dix, D. Kratzert, and P. G. Jones
647  Full Text
Hydrothermal Synthesis, Crystal Structure and Properties of a 1D Metal-Organic Coordination Polymer {[Zn2(2,2',3,3'-odpa)(py)3(H2O)]·H2O}n
Key words: 2,2',3,3'-Oxydiphthalic Acid, Coordination Polymer, Crystal Structure, Photoluminescence
Q.-Y. Li, S.-Q. Zang, J.-B. Li, and H.-W. Hou
674  Full Text
Metal Complexes of Biologically Important Ligands, CLXXV. Pentamethylcyclopentadienyl Halfsandwich Complexes of Rhodium(III) and Iridium(III) with Schiff Bases from 2-(Diphenylphosphino)benzaldehyde and a-Amino Acid Esters
Key words: Pentamethylcyclopentadienyl, Rhodium, Iridium, Schiff Bases, 2-(Diphenylphosphino)benzaldehyde, a-Amino Acid Esters
B. Schreiner, B. Wagner-Schuh, and W. Beck
679  Full Text
Treatment of Tetramethylpyrazole and 3,5-Diphenylpyrazole with Dialkylaluminum Hydrides - Hydroalumination versus Deprotonation
Key words: Organoelement Compounds, Aluminum, Hydrazides, Heterocycles, Hydroalumination
W. Uhl and A. Vogelpohl
687  Full Text
Synthesis, Crystal Structure, Magnetic, Thermal and Fluorescent Properties of [Co(H2O)4(nia)2](suc)·(H2suc)
Key words: Succinate Complexes, Nicotinamide, Crystal Structure, Thermal Analysis, Magnetic Interaction
S. Demir, V. T. Yilmaz, J. Mrozi\'nski, T. Lis, and M. Ho\ly\'nska
695  Full Text
Lithium and Aluminum Anthracenyldiimidosulfinates
Key words: Sulfur, Imide, Anthracene, Lithium, Aluminum
T. Schulz and D. Stalke
701  Full Text
p-Spacer-coupled Diimidosulfinates
Key words: Sulfur, Imide, Aromatic Spacers, Lithium, Aluminum
T. Schulz, D.-R. Dauer, and D. Stalke
711  Full Text
Polymorphism of Dibromo-tetrakis(tetrahydrofuran-kO)magnesium(II)
Key words: Polymorphism, Crystal Structure, Magnesium Halides, Schlenk Equilibrium, Grignard Reaction
D. Stern, M. Granitzka, T. Schulz, and D. Stalke
719  Full Text
Alkynylsilanes and Alkynyl(vinyl)silanes. Synthesis, Molecular Structures and Multinuclear Magnetic Resonance Study
Key words: Alkynes, Silanes, NMR, X-Ray
B. Wrackmeyer, E. Khan, S. Bayer, O. L. Tok, E. V. Klimkina, W. Milius, and R. Kempe
725  Full Text
Unusual Behaviour During the Route of a Japp-Klingemann Reaction
Key words: Pentane-2,4-dione, Anilines, Diazotation, Japp-Klingemann Reaction, X-Ray Diffraction Analysis
J. Marten, W. Seichter, J. Wagler, and E. Weber
745  Full Text
A Cleistanthane Diterpene From a Marine-derived Fusarium Species Under Submerged Fermentation
Key words: Cleistanthane, Diterpenoid, Antimicrobial Activity, Cytotoxicity, Fusarium sp.
Y. Shiono, K. Ogata, T. Koseki, T. Murayama, and T. Funakoshi
753  Full Text
Antimicrobial Alkaloids from the Tubers of Stephania succifera
Key words: Stephania succifera, Alkaloid, Cepharanone D, N-Formyl-asimilobine, Antimicrobial Activity
D.-L. Yang, W.-L. Mei, H. Wang, and H.-F. Dai
757  Full Text
A New Limonoid from Trichilia connaroides
Key words: Trichilia connaroides, Limonoid, Trichiliton B
Z.-L. Geng, X. Fang, Y.-T. Di, Q. Zhang, Y.-M. Shen, and X.-J. Hao
762  Full Text
Abietane Diterpenoids and a Lignan from Pinus yunnanensis
Key words: Pinus yunnanensis, Pinaceae, Diterpenoids, Lignan, Anti-inflammatory Activity, Cytotoxicity
T. Feng, X.-H. Cai, Q.-G. Tan, and X.-D. Luo
765  Full Text
Triniobiumoctabromide, Nb3Br8, Revisited
Key words: Niobium, Bromide, Cluster, Crystal Structure
K. Habermehl and G. Meyer
770  Full Text
N u m b e r  7 (Graphical Abstracts)
Foreword: Chemistry of Iminium Salts and Related Compounds, ImSaT-9
G. Maas
773  Full Text
Original Communications
N-Heterocyclic Carbene (NHC) Derivatives of 1,3-Di(benzyloxy)imidazolium Salts
Key words: Carbene, Gold, Imidazolium Salt, Ionic Liquid, NHC, Rhodium, Silver
G. Laus, K. Wurst, V. Kahlenberg, H. Kopacka, C. Kreutz, and H. Schottenberger
776  Full Text
Metal-doped Zeolites as Green Catalysts for Organic Synthesis
Key words: Heterogeneous Catalysis, Zeolite, Copper, Scandium, Click Chemistry
S. Chassaing, A. Alix, A. Olmos, M. Keller, J. Sommer, and P. Pale
783  Full Text
Empirical Polarity Parameters for Hexaalkylguanidinium-based Room-temperature Ionic Liquids
Key words: Ionic Liquids, Polarity, Hexaalkylguanidinium Salts, Reichardt's Dye, 5-Dimethylamino-5'-nitro-2,2'-bithiophene
M. G. Bogdanov, I. Svinyarov, H. Kunkel, C. Steinle, M. Arkhipova, W. Kantlehner, and G. Maas
791  Full Text
New Bisguanidine-Copper Complexes and their Application in ATRP (In German)
Key words: Bisguanidine Ligands, Copper Complexes, X-Ray, Low Polymerisation Temperatures, ATRP
O. Bienemann, R. Haase, U. Flörke, A. Döring, D. Kuckling, and S. Herres-Pawlis
798  Full Text
The Structure of the Product Formed by Condensation of Malononitrile with Dialkyl Acetone-1,3-dicarboxylates
Key words: Enamino Esters, Malononitrile, Dialkyl Acetone-1,3-dicarboxylates, X-Ray Structures
P. Šimunek, J. Baškov\vc, U. Grošelj, A. Meden, J. Svete, and B. Stanovnik
807  Full Text
Parallel Solution-phase Synthesis of (2S,4E)-4-(Arylaminomethylidene)pyroglutamic Acids
Key words: Pyroglutamic Acid, Enaminones, Amines, Combinatorial Synthesis, Pyrrolidinone
J. Svete, U. Grošelj, J. Baškov\vc, G. Dahmann, and B. Stanovnik
811  Full Text
2-Isoxazolinium Salts and 3-Isoxazolines: Exploratory Chemistry and Uses for the Synthesis of Branched Amino Polyols and Amino Acids
Key words: 2-Isoxazolines, 2-Isoxazolinium Salts, 3-Isoxazolines, Nucleophilic Additions, Electrophilic Additions
V. Jäger, W. Frey, Y. Bathich, S. Shiva, M. Ibrahim, M. Henneböhle, P.-Y. LeRoy, and M. Imerhasan
821  Full Text
Synthesis and Modification of Substituted 2-Azaanthraquinones
Key words: Azaanthraquinones, Ring Transformation, Cycloaddition, Functional Dyes
T. Welzel, D. Weiß, R. Beckert, and H. Görls
833  Full Text
Chemistry of Polyhalogenated Nitrobutadienes, Part 9: Acyclic and Heterocyclic Nitroenamines and Nitroimines from 2-Nitroperchlorobuta-1,3-diene
Key words: Nitro Compounds, Nucleophilic Substitution, Pyrimidines, Pyrazoles, Betaines, Click Chemistry
V. A. Zapol'skii, J. C. Namyslo, M. Gjikaj, and D. E. Kaufmann
843  Full Text
Reduction of Dipyrido Ureas via 6-Alkyloxydipyrido[1,2-c;2',1'-e]imidazolium Salts
Key words: Urea, Imidazolinone, Uronium Salts, Imidazolium Salts, Reduction
D. Kunz, C. Deißler, V. Gierz, F. Rominger, and T. Oeser
861  Full Text
Orthoamides, LXIX. Contributions to the Synthesis of N,N,N',N',N''-peralkylated Guanidines and N,N,N',N',N'',N''-persubstituted Guanidinium Salts (In German)
Key words: N,N,N',N'-Tetraalkyl-chloroformamidinium Salts, Alkylation, N,N,N',N',N''-Pentasubstituted Guanidines, N,N,N',N',N'',N''-Persubstituted Guanidinium Salts, Crystal Structures, Zwitterionic Guanidinium Salts
W. Kantlehner, J. Mezger, R. Kreß, H. Hartmann, T. Moschny, I. Tiritiris, B. Iliev, O. Scherr, G. Ziegler, B. Souley, W. Frey, I. C. Ivanov, M. G. Bogdanov, U. Jäger, G. Dospil, and T. Viefhaus
873  Full Text
Synthesis and Crystal Structures of N-[w-(Dimethylammonio)alkyl]-N',N',N'',N''-tetramethylguanidinium Chloride Tetraphenylborates (In German)
Key words: N',N',N'',N''-Pentasubstituted Guanidinium Salts, Mixed Chloride Tetraphenylborate Salts, Thermal Analysis, Phase Transition, X-Ray Crystal Structures
I. Tiritiris, F. Lissner, T. Schleid, and W. Kantlehner
907  Full Text
N u m b e r  8 (Graphical Abstracts)
Preface: Solvothermal Processes
G. Demazeau, W. Bensch, and R. Pöttgen
917  Full Text
Solvothermal Synthesis and Structure of Chalcogenidoarsenate Anions
Key words: Arsenic, Sulfur, Selenium, Tellurium, Solvothermal Synthesis, Chalcogenidoarsenates
A. Kromm, T. v. Almsick, and W. S. Sheldrick
918  Full Text
Synthesis of Inorganic-Organic Hybrid Thiometallate Materials with a Special Focus on Thioantimonates and Thiostannates and in situ X-Ray Scattering Studies of their Formation
Key words: Thiometallates, Inorganic-Organic Hybrid Compounds, Solvothermal Synthesis, in situ X-Ray Scattering
B. Seidlhofer, N. Pienack, and W. Bensch
937  Full Text
Solvothermal Synthesis of Multifunctional Coordination Polymers
Key words: Solvothermal Synthesis, Coordination Polymer, Metal-Organic Framework, Porosity, Multifunctionality
Y. Zhao, K. Li, and J. Li
976  Full Text
Solvothermal Processes: Definition, Key Factors Governing the Involved Chemical Reactions and New Trends
Key words: Hydrothermal Processes, Aqueous Solvents, Solvothermal Processes, Non-aqueous Solvents, Key Factors
G. Demazeau
999  Full Text
New Trends in Solvothermal Crystal Growth at the Macro- and Nanoscale
Key words: Solvothermal Crystal Growth, Large Single Crystals, Density of Defects, Nanoscale Crystal Growth, 1D Nanomorphology
G. Demazeau, A. Largeteau, and S. Darracq
1007  Full Text
Non-aqueous Sol-Gel Routes to Metal Oxide Nanocrystals under Solvothermal Conditions: Review and Case Study on Doped Group IV Metal Oxides
Key words: Metal Oxides, Nanocrystals, Sol-Gel Process, Solvothermal Synthesis
A. Pucci and N. Pinna
1015  Full Text
Original Communications
The Influence of Synthesis Parameters on FeO(OH) / Fe2O3 Formation by Hydrothermal Techniques
Key words: Fe2O3, High Pressure, Hydrothermal Synthesis, Correlation Analysis
M. Popescu, R. Piticescu, E. Vasile, D. Taloi, M. Petriceanu, M. Stoiciu, and V. Badilita
1024  Full Text
Solvothermal/Hydrothermal Synthesis of Metal Oxides and Metal Powders with and without Microwaves
Key words: Nanoparticles, Anatase, Apatites, Copper, Gold, Microwave-Hydrothermal Technique
S. Komarneni, Y. D. Noh, J. Y. Kim, S. H. Kim, and H. Katsuki
1033  Full Text
Hydrothermal Sintering under Mild Temperature Conditions: Preparation of Calcium-deficient Hydroxyapatite Compacts
Key words: Calcium-deficient Hydroxyapatite, Hydrothermal Hot-Pressing, Hydrothermal Sintering, Low-temperature Densification, Ca/P Ratio
K. Yanagisawa, J.-H. Kim, C. Sakata, A. Onda, E. Sasabe, T. Yamamoto, Z. Matamoros-Veloza, and J. C. Rendón-Angeles
1038  Full Text
Hybridisation of Sebacic Acid on the Surface of g-Alumina Nanoparticles in Sub- and Supercritical Water
Key words: Surface Modification, Nano Alumina, Supercritical and Subcritical Water
V. Singh, S. Takami, K. Minami, D. Hojo, T. Arita, and T. Adschiri
1045  Full Text
Solvothermal Synthesis of Gallium and Indium Nitrides Using Lithium Amide
Key words: Gallium Nitride, Indium Nitride, Nanocrystal, Solvothermal Synthesis
P. Chirico and A. L. Hector
1051  Full Text
N u m b e r  9 (Graphical Abstracts)
Original Communications
Dissolving Silicides: Syntheses and Crystal Structures of New Ammoniates Containing Si52- and Si94- Polyanions and the Role of Ammonia of Crystallisation
Key words: Silicides, Zintl Anions, Liquid Ammonia, Crystal Structure Determination
S. Joseph, C. Suchentrunk, and N. Korber
1059  Full Text
Cyanoplatinate Halides - Synthesis, Crystal Structure Analyses and Vibrational Spectroscopy of Compounds A2[Pt(CN)4X2] (A = Rb, Cs; X = Cl, Br, I)
Key words: Platinum, Cyanides, Crystal Structures, X-Ray Scattering, Vibrational Spectroscopy
C. Mühle, J. Nuss, R. E. Dinnebier, and M. Jansen
1066  Full Text
Molybdenum-Boron Bonds in the Crystal - Structural Characterization of K[(h5-C5H5)Mo(CO)3] and [(h5-C5H5) (OC)3Mo-{B(NMe2)-B(NMe2)Br}]
Key words: Half-sandwich Molybdenum Complexes, Boranes, Diboranes(4), Boryl Complexes, X-Ray Diffraction
H. Braunschweig, K. Radacki, K. Kraft, and S. Stellwag
1073  Full Text
Penta-, Hepta-, and Octaiodide Anions in Salts with Alkaline Earth Metal Crown Ether Cations (In German)
Key words: Pentaiodide, Heptaiodide, Octaiodide, Crown Ether, Crystal Structure
C. Walbaum, I. Pantenburg, and G. Meyer
1077  Full Text
Two New Hemidirected Lead(II) Complexes: [Pb(pcih)(bha)] and [Pb(pcih)(NO3)]
Key words: Lead(II) Complex, Crystal Structure, Solvothermal Synthesis, Hemidirected
D.-Q. Li, X. Liu, and J. Zhou
1084  Full Text
Gold Nanoparticles Bearing an a-Lipoic Acid-based Ligand Shell: Synthesis, Model Complexes and Studies Concerning Phosphorescent Platinum(II)-Functionalisation
Key words: Gold, Luminescence, Nanoparticles, Platinum, Self-assembly
U. Siemeling, F. Bretthauer, C. Bruhn, T.-P. Fellinger, W.-L. Tong, and M. C. W. Chan
1089  Full Text
A Seven-coordinate Manganese(II) Complex Formed with the Tripodal Tetradentate Ligand Tris(N-methylbenzimidazol-2-ylmethyl)amine
Key words: Manganese(II) Complex, Crystal Structure, Cylovoltammetry, EPR, Tris(N-methylbenzimidazol-2-ylmethyl)amine
H. Wu, J. Yuan, B. Qi, J. Kong, F. Kou, F. Jia, X. Fan, and Y. Wang
1097  Full Text
Hydrothermal Synthesis, Crystal Structure and Catalytic Properties of a Novel Polyoxometalate: (C5H7N2)3(AsMo12O40) · 2C5H6N2 · 1.5H2O
Key words: Polyoxometalate, Hydrothermal Synthesis, Keggin Structure, Crystal Structure, Catalytic Elimination
T.-J. Cai, X.-M. Shen, Z.-S. Peng, S.-Z. Lü, and Q. Deng
1101  Full Text
Synthesis and Structural Aspects of Two Trinuclear Cyano-bridged Heterometallic Complexes with Monodentate Coordination of Perchlorate and Acetate Anions
Key words: CaII/FeIII Complex, Cyano Bridge, Trinuclear, Thermal Analysis
A. Datta, S. Pillet, N.-T. Chuang, H. M. Lee, and J.-H. Huang
1106  Full Text
Morphology and Structure of Biomorphous Silica Isolated from Equisetum hyemale and Equisetum telmateia
Key words: Equisetum hyemale, Equisetum telmateia, Horsetail, Biomorphous Silica, Silicon Dioxide
M. Neumann, S. Wagner, R. Nöske, B. Tiersch, and P. Strauch
1113  Full Text
2,2'-Bipyridine-1,2-dithiolate Mixed Ligand Complexes. Synthesis, Characterisation and EPR Spectroscopy (In German)
Key words: 1,2-Dithiosquarate, 1,2-Dithiooxalate, 2,2'-Bipyridine, EPR Spectroscopy, Copper(II)
D. J. Awad, F. Conrad, A. Koch, A. Friedrich, A. Pöppl, and P. Strauch
1121  Full Text
Synthesis and Radiofluorination of Iodophenyl Esters as Tool for the Traceless Staudinger Ligation
Key words: Staudinger Ligation, Traceless, Bioorthogonal, Radiofluorination, PET, X-Ray Structure
M. Pretze, A. Flemming, M. Köckerling, and C. Mamat
1128  Full Text
The Rotationally Disordered Crystal Structure of Tropylium Bromide C7H7+Br- (In German)
Key words: Crystal Structure, Molybdenum, Rotational Disorder, Tropylium Bromide, Tropylium Complexes
F. Hoffmann, G. W. Fester, and J. Wagler
1137  Full Text
Catalytic Effect of Basic Alumina in the Dehydrogenation of 1,4-Dihydropyridines with Tetrabutylammonium Peroxydisulfate
Key words: 1,4-Dihydropyridines, Heterocycles, Oxidation, Peroxydisulfates, Pyridines
H. R. Memarian and B. Barati
1143  Full Text
2,2'-(1,4-Phenylene)bis-3,4-dihydro-2H-1,3-thiazin-4-ones and their Facile Recyclization to 2,2'-(1,4-Phenylene)bis(pyrimidin-4-one) and/or 2,2'-(1,4-Phenylene)-bis-(thieno[2,3-d]pyrimidin-4(1H)-one) Derivatives
Key words: Terephthalaldehyde, Cyanoacetamide, Phenyl (Phenethyl) Isothiocyanate, Bis-1,3-thiazin-4-one, Bis-pyrimidin-4-one, Bis-thieno[2,3-d]pyrimidin-4-one
R. M. Shaker, Y. R. Ibrahim, F. F. Abdel-Latif, and A. Hamoda
1148  Full Text
Cyclic Oxalylation of Primary N-Substituted Anthranilamides: 1H-Benzo[e][1,4]diazepine-2,3,5(4H)-triones and 11a-Chloro-benzo[e]oxazolo[3,2-a][1,4]diazepine-2,3,5,11(10H,11aH)-tetraones
Key words: Anthranilamides, Cyclization, Fused Heterocycles, Oxalyl Chloride, Acylation
M. A. Köllner and D. Geffken
1155  Full Text
Two New Compounds from the Bark of Dysoxylum hainanense
Key words: Dysoxylum hainanense, ent-8(9)-Pimarene-20-hydroxy-16-nor-15-oic acid, 20S,24-Epoxy-25,26,27-trisnor-24-oxo-3,4-seco-dammar-4(28),22-dien-3-oic acid
X.-Y. Zhang, R.-T. Zhang, X.-H. Cai, Y.-P. Liu, and X.-D. Luo
1161  Full Text
Novel Alkaloids from Alstonia scholaris
Key words: Alstonia scholaris, Scholarisines I and II, COX, 5-LOX
X.-H. Cai, J.-H. Shang, T. Feng, and X.-D. Luo
1164  Full Text
Hydrothermal Synthesis, Crystal Structure and Properties of a 2D Network of Cd(II) Coordination Polymers with Helical Chains
Key words: Cadmium(II), Biphenyl-2,3',3,4'-tetracarboxylic Acid, Helical Chain, Coordination Polymer, Crystal Structure
C.-Z. Mei, N. Ma, and K.-H. Li
1169  Full Text
Synthesis, Structure and Characterization of a Novel Two-Dimensional Supramolecular Mn(II) Coordination Polymer Constructed from a 1,10-Phenanthroline Derivative and a Flexible Dicarboxylate
Key words: Coordination Polymer, Crystal Structure, Glutaric Acid, 1,10-Phenanthroline Derivative
Z.-G. Kong, X.-Y. Ma, and Z.-L. Xu
1173  Full Text
N u m b e r  10 (Graphical Abstracts)
Original Communications
The First Ammoniates of Alkali Metal Fluorides: Cesium Fluoride Ammonia (3/4) [Cs3F3(NH3)4] and Ammonium Cesium Difluoride\\[1mm] [NH4CsF2]
Key words: Cesium, Fluoride, Liquid Ammonia, Crystal Structure, Hydrogen Bond
S. A. Baer and F. Kraus
1177  Full Text
Intermediate-valent Cerium in CeRu2Mg5
Key words: Intermetallics, Cerium, Magnesium, Intermediate Valence
S. Linsinger, M. Eul, U. Ch. Rodewald, and R. Pöttgen
1185  Full Text
Optical and Magnetic Properties of some RE}ZnPnO (1{Pn} = P, As, Sb) Phases
Key words: Arsenide Oxide, Antimonide Oxide, Rare Earth, Optical Properties, Mössbauer Spectroscopy, Magnetism
I. Schellenberg, H. Lincke, W. Hermes, V. Dittrich, R. Glaum, M. H. Möller, and R. Pöttgen
1191  Full Text
PbO / PbF2 Flux Growth of YScO3 and LaScO3 Single Crystals - Structure and Solid-State NMR Spectroscopy
Key words: Scandium, Crystal Chemistry, Solid-State NMR
S. Balamurugan, U. Ch. Rodewald, T. Harmening, L. v. Wüllen, D. Mohr, H. Deters, H. Eckert, and R. Pöttgen
1199  Full Text
Synthesis and Crystal Structure of the Praseodymium Orthoborate l-PrBO3
Key words: High Pressure, Crystal Structure, Multianvil, Orthoborate, Aragonite
A. Haberer, R. Kaindl, and H. Huppertz
1206  Full Text
High-pressure Synthesis and Characterization of the Fluoride Borate Tm5(BO3)2F9
Key words: Rare Earth, Fluoride, Borate, High Pressure, Crystal Structure
A. Haberer, M. Enders, R. Kaindl, and H. Huppertz
1213  Full Text
Synthesis, Crystal Structures and Spectroscopic Properties of RbBaTaS4 and K2BaTa2S11
Key words: Alkali Polysulfide Flux, Barium, Tantalum Thiophosphates, Crystal Structure, Spectroscopic Properties
Y. Wu and W. Bensch
1219  Full Text
Two Supramolecular Architectures Containing Dinuclear Thiostannate [Sn2S6] Units
Key words: Solvothermal Synthesis, Crystal Structures, Thiostannates, Transition Metal Complex
J. Zhou, X. Liu, G.-Q. Chen, F. Zhang, and L.-R. Li
1229  Full Text
Synthesis, High-resolution Crystal Structure Refinement and Magnetic Properties of the Manganese-rich Cementite-type Mn1.8Fe1.2C
Key words: Cementite, Synthesis, Manganese, X-Ray Diffraction, Magnetic Susceptibility
L. Stork, P. Müller, M. Speldrich, P. Kögerler, J. v. Appen, and R. Dronskowski
1235  Full Text
From a Dissymmetrical Oxamidate Ligand to a 2D Coordination Polymer: Synthesis, Crystal Structure and Magnetic Properties
Key words: Oxamidate Ligand, Crystal Structure, Magnetic Properties
B. L. Liu, J. Dang, S. Q. Zang, Q. L. Wang, and R. J. Tao
1240  Full Text
Syntheses and Structures of [nBu4N][nBu2SbCl4] and [Et3SbMe]2[(MeSbCl3)2]
Key words: Antimony, Nitrogen, Chlorine, X-Ray Crystallography
H. J. Breunig, T. Koehne, E. Lork, O. Moldovan, J. Poveleit, and C. I. Ra\ct
1245  Full Text
Amine-rich Silver Complexes of rac-trans-1,2-Diaminocyclohexane
Key words: Silver, Hydrogen Bonds, Chiral Ligands, Amines
C. Wölper, S. D. Ibáñez, and P. G. Jones
1249  Full Text
Polysulfonylamines, CLXXXVIII. Crystal Structures of Three Dimethylammonium Di(4-halobenzenesulfonyl)amides (Halogen = Cl, Br, I) and of Dimethylammonium\\ Di(4-methylbenzenesulfonyl)amide: An Isotypical Series Featuring Strong Structure-determining Hydrogen Bonds and Incidental Halogen Bonds (In German)
Key words: Hydrogen Bonding, Halogen Bonding, Halogen-Methyl Exchange, Isotypical Structures, Sulfonamides
C. Wölper, A. Rodríguez-Gimeno, M. Freytag, P. G. Jones, and A. Blaschette
1258  Full Text
An Air-induced Synthesis of a Salt [AuCl2(DDDT)](MET-TTF) (DDDT = 5,6-Dihydro-1,4-dithiin-2,3-dithiolate, MET-TTF = Bis(methylthio)ethylenedithiotetrathiafulvalene)
Key words: Tetrathiafulvalene, Charge Transfer, Gold Complex, Crystal Structure
W. Yang, Z.-G. Ren, G.-Q. Bian, Q.-Y. Zhu, and J. Dai
1267  Full Text
Synthesis and Characterization of New Palladium(II) Complexes with Ligands Derived from Furan-2-carbaldehyde and Benzaldehyde Thiosemicarbazone and their {\twlbi{}in vitro} Cytotoxic Activities against Various Human Tumor Cell Lines
Key words: Thiosemicarbazone, Palladium(II) Complexes, Crystal Structures, Antitumor/Cytotoxic Activity
W. Hernández, J. Paz, F. Carrasco, A. Vaisberg, J. Manzur, E. Spodine, L. Hennig, J Sieler, and L. Beyer
1271  Full Text
Molecular Neodymium and Yttrium Cations with the N,N-Bis[2-(pyrid-2-yl)ethyl]hydroxylaminato Ligand
Key words: Lanthanides, Hydroxylamines, N-O Ligands, X-Ray Diffraction
B. J. Hellmann, B. Neumann, H.-G. Stammler, and N. W. Mitzel
1279  Full Text
Study on Chemical Constituents and Cytotoxic Activities of Salacia chinensis Growing in Vietnam
Key words: Salacia chinensis, Triterpenes, Cytotoxic Activities
T. T. Minh, N. T. H. Anh, V. D. Thang, and T. V. Sung
1284  Full Text
Crystal Structure of La3OBr[AsO3]2
Key words: Oxoarsenite, Rare Earth Compound, Crystal Structure
H. B. Yahia, U. Ch. Rodewald, and R. Pöttgen
1289  Full Text
N u m b e r  11 (Graphical Abstracts)
Original Communications
Unprecedented Hexa- and Undecanuclear Frameworks of Two New Tin(IV) Oxo Clusters Resulting from Partial Debenzylation Reactions
Key words: Organotin(IV), Sn-O-Sn Framework, Triflate, Cleavage Reactions, Crystal Structures
L. Plasseraud, H. Cattey, and P. Richard
1293  Full Text
Synthesis and Crystal Structure of AgTl3(Cr2O7)2
Key words: Silver, Thallium, Hydrothermal Synthesis, Crystal Structure
V. Dietrich, D. Pitzschke, and M. Jansen
1301  Full Text
Intermetallic Magnesium Compounds RE2Ni2Mg3 (RE = Gd, Dy - Tm, Lu) with Tb2Ni2Mg3-type Structure
Key words: Intermetallics, Magnesium, Crystal Chemistry
S. Linsinger, M. Eul, H. B. Yahia, M. H. Möller, and R. Pöttgen
1305  Full Text
Synthesis and Crystal Structure of the High-pressure Cobalt Borate HP-CoB2O4
Key words: Borate, High Pressure, Crystal Structure, Multianvil
S. C. Neumair, R. Kaindl, and H. Huppertz
1311  Full Text
Photophysics of [Pt{4-(o-tolyl)isqbipy}Cl]SbF6, where 4-(o-Tolyl)isqbipy is the New 4-(o-Tolyl)-6-(3"-isoquinolyl)-2,2'-bipyridyl Ligand
Key words: Isoquinolyl-bipyridyl Ligand, Crystal Structure, Platinum Complex, Photophysics
J. S. Field, J.-A. Gertenbach, D. Jaganyi, D. R. McMillin, A. Shaira, and D. J. Stewart
1318  Full Text
Reactivity of Tetramethylphosphonium Fluoride in Acetonitrile Solutions
Key words: Iminophosphorane, Vibrational Spectroscopy, NMR Spectroscopy, Crystal Structure
C. Hohenstein, F. Neumann, and A. Kornath
1327  Full Text
Synthesis, Crystal Structure and DNA-binding Properties of a Nickel(II) Complex with 2,6-Bis(2-benzimidazolyl)pyridine
Key words: 2,6-Bis(2-benzimidazolyl)pyridine, Nickel(II) Complex, Crystal Structure, DNA-binding Properties
H. Wu, X. Huang, J. Yuan, F. Kou, G. Chen, B. Jia, Y. Yang, and Y. Lai
1334  Full Text
Synthesis, Crystal Structure, and DNA-Binding Studies of a Ni(II) Complex with the Tris(N-methylbenzimidazol-2-ylmethyl)amine Ligand
Key words: Tris(N-methylbenzimidazol-2-ylmethyl)amine, Ni(II) Picrate Complex, Crystal Structure DNA Binding
H. Wu, K. Li, T. Sun, B. Liu, F. Kou, F. Jia, J. Yuan, and G. Chen
1341  Full Text
Metal Benzenesulfonates/Acetic Acid Mixtures as Novel Catalytic Systems: Application to the Protection of a Hydroxyl Group
Key words: Tetrahydropyranylation, Metal Benzenesulfonate, Alcohol, Phenol, Protection
M. Wang, J. Gao, and Z. Song
1349  Full Text
Synthesis of Some Fused Triazole Derivatives Containing 4-Isobutylphenylethyl and 4-Methylthiophenyl Moieties
Key words: 1,2,4-Triazole-5-thiol, N-Aryl-maleimides, [1,3]Thiazolo[3,2-b][1,2,4]triazoles
M. Kumsi, B. Poojary, P. L. Lobo, J. Fernandes, and C. Chikkanna
1353  Full Text
Cyclotrimerization of 3-R-1,2,4-Triazin-5(4H)-ones with Cyclic Ketones
Key words: Cycloaddition, Cyclic Ketones, Pyridines, 1,2,4-Triazines
I. N. Egorov, I. S. Kovalev, V. L. Rusinov, and O. N. Chupakhin
1359  Full Text
Polysulfonylamines, CLXXXIX. Additional Examples of the O-Protonation of Ureas by Di(organosulfonyl)amines: Formation and Crystal Structures of 1,1-Dimethyluronium Di(4-fluorobenzenesulfonyl)amide and Di(1-methylurea)hydrogen(I) Di(4-fluorobenzenesulfonyl)amide
Key words: Hydrogen Bonding, [O-H···O]+ Homoconjugate, N-Methyl Ureas, N-Methyl Uronium Cations, Sulfonamides
C. Wölper, A. Rodríguez-Gimeno, K. C. Iborra, P. G. Jones, and A. Blaschette
1363  Full Text
Synthesis, in vitro Antiproliferative and Anti-HIV Activity of New Derivatives of 2-Piperazino-1,3-benzo[d]thiazoles
Key words: Antiproliferative Activity, Anti-HIV Activity, Benzothiazole, Aryl Isothiocyanate, Amide, Thiourea Derivatives
Y. A. Al-Soud, H. H. Al-Sa'doni, S. O. W. Saber, R. H. M. Al-Shaneek, N. A. Al-Masoudi, R. Loddo, and P. La Colla
1372  Full Text
Synthesis of (R)-(-)-Carvone Derivatives
Key words: Terpenes, Essential Oils, p-Menthanes, Structure-Activity Relationship
D. P. d. Sousa, E. Raphael, and T. J. Brocksom
1381  Full Text
Glycosides from Cephalaria Species
Key words: Dipsacaceae, Cephalaria, Oleanane and Hederagenin Glycosides, Lycicoside I and II, Cilicicoside I
E. Halay and S. K\irm\iz\igül
1384  Full Text
Three New Antiviral Triterpenes from Aster tataricus
Key words: Aster tataricus, Triterpene, Antiviral, Shionane-type Triterpenes
W. B. Zhou, J. Y. Tao, H. M. Xu, K. L: Chen, G. Z. Zeng, C. J. Ji, Y. M. Zhang, and N. H. Tan
1393  Full Text
Ziziphorins A and B. New Flavonoids from Ziziphora tenuior
Key words: Ziziphora tenuior, Labiatae, Falvonoids, Ziziphorin A, Zizphorin B
R. Mehmood, M. Imran, A. Malik, and R. B. Tareen
1397  Full Text
Two New Phytoecdysteroids from the Needles of Taxus canadensis
Key words: Taxus canadensis, Taxaceae, Ponasterone 20,22-p-Hydroxybenzylidene Acetal, Ponasterone 20,22-Acetonide, Structure Elucidation
Y. Fang, Z.-Y. Ni, T. Yamada, Y.-F. Wang, M.-L. Zhang, M. Dong, B. Cong, F. Sauriol, C.-H. Huo, Q.-W. Shi, and H. Kiyota
1401  Full Text
Daphlongamines I and J. New Yuzurine-type Alkaloids from Daphniphyllum longeracemosum
Key words: Daphniphyllum Alkaloids, Yuzurine, Daphlongamine, Daphniphyllum longeracemosum
C.-S. Li, Y.-T. Di, J. Guo, Q. Zhang, X. Fang, and X.-J. Hao
1406  Full Text
N u m b e r  12 (Graphical Abstracts)
Original Communications
One more Compound Containing the CBN4- Ion - Synthesis, Single-crystal Structure and Vibrational Spectra of Ca15(CBN)6(C2)2F2
Key words: Acetylide, Calcium, CBN4- Anion, Structure Elucidation, Vibrational Spectra
O. Reckeweg, A. Schulz, and F. J. DiSalvo
1409  Full Text
Crystal Structures of New Alkali Metal-rich Oxometallates: Rubidium Aluminate Tetrahydroxide, Rb9(AlO4)(OH)4, Rubidium Orthogallate, Rb5GaO4, Cesium {\twlbi{bis}}-Chromate(IV) Oxide, Cs10(CrO4)2O, and Cesium Diindate, Cs8In2O7
Key words: Oxometallates, Rubidium, Cesium, Aluminates, Gallates, Indates, Chromates, Dimetallates, TLS Analysis, Crystal Structure
J. Bender, A. Wohlfarth, and C. Hoch
1416  Full Text
The Transition Metal-rich Orthophosphate Arrojadite with Special Structural Features
Key words: Arrojadite, Defect Structure, Crystal Structure
C. Kallfaß, C. Hoch, H. Schier, A. Simon, and H. Schubert
1427  Full Text
Mechanothermal Solid-state Synthesis of Cobalt(II) Ferrite and Determination of its Heat Capacity by MTDSC
Key words: Cobalt Ferrite, Modulated Temperature Differential Scanning Calorimetry (MTDSC), Heat Capacity, Mechanochemistry
V. Berbenni, C. Milanese, G. Bruni, A. Girella, and A. Marini
1434  Full Text
RE4B4O11F2 (RE = Eu, Dy): New Phases Isotypic to the Fluoride Borate Gd4B4O11F2
Key words: Rare Earth, Fluoride, Borate, High Pressure, Crystal Structure
A. Pitscheider, M. Enders, and H. Huppertz
1439  Full Text
A Novel Keggin Tungstocobaltate Framework Supported by Copperbipyridyl Complexes: [Cu(I)(2,2'-bipy)2]{[Cu(II)(2,2'-bipy)2]2[HCoW12O40]} · 4H2O
Key words: Polyoxometalates, Tungstocobaltate, Copper Coordination Group, Electrochemistry
J. Sha, L. Xin, B. Zhou, D. Yu, Y. Qu, S. Li, and F. Liu
1445  Full Text
Hydrothermal Syntheses and Crystal Structures of Two New Mixed-valence Vanadium Oxides [Ni(en)2(H2O)2][Ni(en)3]2[V16O38Cl] · 3(H2O)] and H3O)2V3O8
Key words: Hydrothermal Syntheses, Vanadium Oxides, Polyoxovanadates, Crystal Structure
X. Liu, X.-H. Yin, and F. Zhang
1451  Full Text
A Vanadyl(V) Complex with a Pincer-type Thiobis(phenolate) and an Acetylacetonate Co-ligand, VO(tbp)(acac)
Key words: Oxovanadium(V), Thiobis(phenolate), Complex, Molecular Structure, Cyclic Voltammetry
R. Bikas, H. H. Monfared, S. Alami, I. Pantenburg, and G. Meyer
1457  Full Text
Dimeric, or not Dimeric, that is the Question: Two Neighboring I3- Ions Enclosed in Cavities of a Complex Host Structure (In German)
Key words: Polyiodide, Phosphinic Acid, Crystal Structure, Hydrogen Bonding
M. K. Meyer, J. Graf, and G. J. Reiß
1462  Full Text
Synthesis and Crystal Structures of Copper(II), Zinc(II), Lead(II) and Cadmium(II) Tetrazole-5-carboxylate Complexes Generated via in situ Hydrolysis Reaction
Key words: Tetrazole-5-carboxylate, Complex, in situ Synthesis, Structure
J.-F. Kou, M. Su, Y.-H. Zhang, Z.-D. Huang, S. W. Ng, and G. Yang
1467  Full Text
Key words: Porphyrins, Conformational Analysis, Anthracenylporphyrins, Tetrapyrroles, Suzuki Coupling
M. Davis, M. O. Senge, and O. B. Locos
1472  Full Text
5-Aminouracil as a Building Block in Heterocyclic Synthesis: Part III. One-pot Synthesis of Novel Pyrimido[5,4-b]quinoline-2,4,9-triones and Pyrimido[5,4-c]isoquinolines
Key words: 5-Aminouracil, Dimedone, One-pot Synthesis, Pyrimido[5,4-b]quinoline-2,4,9-trione, Pyrimido[5,4-c]isoquinoline
R. M. Shaker, K. U. Sadek, E. A. Hafez, and M. A. Elrady
1485  Full Text
Synthesis of New 3-Substituted Indole Derivatives
Key words: 3-Cyanoacetyl-2-methylindole, Thioacetanilide, Hydrazonoyl Halides, Thiadiazole, Thiazole
H. M. E. Hassaneen and R. M. Pagni
1491  Full Text
Electroreduction of Organic Compounds, 37. Electroreduction of 1,4-Dichlorobicyclo[2.2.2]octane-2-carboxamides
Key words: Bicyclo[2.2.2]octanes, [2.2.2]Propellanes, Elimination, Electroreduction, X-Ray Structure, MO Calculations
J. Voss, W. Baum, G. Adiwidjaja, and U. Behrens
1498  Full Text
Synthesis, Characterization and Biological Studies of Some Bioactive Thiazolotriazole Derivatives
Key words: Ibuprofen, 1,2,4-Triazole-5-thione, Thiazolo[3,2-$b$][1,2,4]triazole, Antimicrobial Activity
M. Kumsi, B. Poojary, P. L. Lobo, N. S. Kumari, and A. Chullikana
1509  Full Text
The Solid Solutions Gd2Cu2In1-xMgx - Drastic Increase of the Curie Temperature upon In/Mg Substitution
Key words: Intermetallics, Gadolinium, Solid Solution, Ferromagnetism
W. Hermes, F. M. Schappacher, and R. Pöttgen
1516  Full Text