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| Contents Vol. 53b (1998)
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| N u m b e r 1 | ||
| Original Communications | ||
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On CuDy2[B8O16] and CuHo2[B8O16]:
Two New "Metaborates" with a Key words: Copper, Lanthanoids, Borate, Synthesis, Crystal Structure A. Wiesch, H. Timm, K. Bluhm | 1 | |
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CuHo2[B2O5]2: An Unexpected Structure Type in the
Series of Copper Lanthanoid Borates
(In German)
Key words: Copper, Holmium, Borate, Synthesis, Crystal Structure A. Wiesch, K. Bluhm | 5 | |
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The Reaction of Bis[bis(trimethylsilyl)amino]germylene with
Bromocyanogen and the Crystal Structure of
Bis[bis(trimethylsilyl)amino]bromocyanogermane
Key words: Germanium, Germylene, Germyl Cyanide, X-Ray Data S. N. Nikolaeva, E. V. Antomonov, J. Lorberth, V. S. Petrosyan | 9 | |
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Vibrational Spectra and Normal Coordinate Analysis of
Hexathiocyanatoplatinate(IV),
Crystal Structure of [Py2CH2][Pt(SCN)6]
(In German)
Key words: Hexathiocyanatoplatinate(IV), IR Spectra, Raman Spectra, Normal Coordinate Analysis, Crystal Structure J. Seemann, W. Preetz | 13 | |
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Crystal Structures of Diphenylphosphinic Acid Amide, Ph2P(O)NH2,
and of its Cesium Salt [Cs{Ph2P(O)NH}]
(In German)
Key words: Phosphinic Acid Amide, Cesium, Crystal Structure S. Schlecht, S. Chitsaz, B. Neumüller, K. Dehnicke | 17 | |
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Synthesis and Structure of Li4GeS4
Key words: Lithium, Germanium, X-Ray Data, Crystal Structure, Raman Spectra Y. Matsushita, M. G. Kanatzidis | 23 | |
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The Crystal Structure of the Potential Ferroelectric Calcium
Rhenate(VI, VII) Ca11Re4O24 and its Relation to the
Structure of Sr11Os4O24
Key words: Crystal Structure, Ferroelectrics, Mixed Valence, Rhenates, Perrhenates W. Jeitschko, H. A. Mons, U. C. Rodewald, M. H. Möller | 31 | |
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The Reactivity of Nitrophenyl Substituted Cyclic Amines with
Dehydrogenations
(In German)
Key words: Lactam, Iminium Salt, Aminoketone, N,O-Acetal, Neighbour Group H. Möhrle, J. Mehrens | 37 | |
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On the Crystal Chemistry of Tellurates Containing Mn2+ in the
Cationic and Anionic Part
of the Crystal Structure:
(Mn2.4Cu0,6)TeO6, Ba2MnTeO6 and
Pb(Mn0.5Te0.5)O3
(In German)
Key words: Manganese, Copper, Lead, Barium, Tellurates L. Wulff, B. Wedel, Hk. Müller-Buschbaum | 49 | |
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On the Crystal Chemistry of the Copper(II) Zinc Tellurates
Cu5Zn4Te3O18
and Cu1.5Zn1.5TeO6 with a
Note on Cu1.5Co1.5TeO6
(In German)
Key words: Copper, Zinc, Cobalt, Tellurate, Crystal Structure L. Wulff, Hk. Müller-Buschbaum | 53 | |
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Magnetic Properties of
[Cu{OCH2CH2N(C4H9)2}NCO]4 in the
Temperature Range
from 10 to 240 K
(In German)
Key words: Copper Complexes, Magnetic Properties, Theoretical Calculations W. Münch, L. Walz, M. König | 58 | |
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Unusual Bonding in Ternary Nitrides:
Preparation, Structure and Properties of Ce2MnN3
Key words: Ternary Nitride, Crystal Structure, Magnetic Susceptibility, Electrical Resistivity, Extended Hückel Method R. Niewa, G. V. Vajenine, F. J. DiSalvo, H. Luo, W. B. Yelon | 63 | |
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RbAsF6, CsAsF6 and RbSbF6:
Crystal Structures, Thermal Phase Transitions,
and Vibrational
Spectra
(In German)
Key words: Alkaline Hexafluoropnictates, Crystal Structure, Thermal Phase Transitions, Vibrational Spectra S. Loss, C. Röhr | 75 | |
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Synthesis and Crystal Structure of a
Novel Neutral Polymeric
Lead(II)-thiosemicarbazonato Complex
Key words: Polymeric Lead(II) Complex, 2-Acetylpyridine-4N-methylthiosemicarbazone, X-Ray Data A. Castiñeiras, R. Domínguez, L. Bresolin, A. J. Bortoluzzi, R. A. Burrow, M. Hörner | 81 | |
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Studies of Polyhalides, 33.
Polyiodides of the Nickel Hexammine Complex:
Nickelhexammine Bistriiodide [Ni(NH3)6](I3)2 and
Nickelhexammine Bispentaiodide [Ni(NH3)6](I5)2
(In German)
Key words: Polyiodide, Triiodide, Pentaiodide, Nickel Hexammine Complex, Crystal Structure K.-F. Tebbe, T. Gilles, B. Radke | 87 | |
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Crystal Structure, 195Pt NMR Chemical Shifts, Vibrational Spectra, and
Normal
Coordinate Analyses of trans-Dihalogeno-bis(oxalato)platinates(IV),
trans-[PtX2(ox)2]2-, X = Cl, Br, I
(In German)
Key words: trans-Dichloro-bis(oxalato)platinate(IV), trans-Dibromo-bis(oxalato)platinate(IV), trans-Diiodo-bis(oxalato)platinate(IV), Crystal Structure, Vibrational Spectra W. Preetz, J.-G. Uttecht | 93 | |
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Transition Metal Complexes of Nitroxide Radicals. Palladium, Platinum,
Pentamethylcyclopentadienyl
Rhodium and Iridium Complexes, and
a-Aminocarboxylate
Complexes with Derivatives of
2,5-Dihydroimidazole-1-oxyls
(In German)
Key words: Nitroxide Radicals, 2,5-Dihydroimidazole-1-oxyls, Transition Metal Complexes F. Hintermaier, S. Helding, L. B. Volodarsky, K. Sünkel, K. Polborn, W. Beck | 101 | |
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On the System Sr/Mo/O: Phase Diagram, Synthesis and Characterization
of Ternary Compounds
(In German)
Key words: Strontium Molybdate, Phase Diagram, Synthesis, Thermochemical Data, Electric Properties U. Steiner, W. Reichelt | 110 | |
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Synthesis of Alkaline Earth Metallocenes from Alkaline Earth Metal
Bis[bis(trimethylsilyl)amide] and 6-Methyl-6-phenylfulvene
(In German)
Key words: Calcocene, Strontocene, Barocene, Bis(trimethylsilyl)amide, Alkaline Earth Metallocene M. Westerhausen, M. Hartmann, N. Makropoulos, B. Wieneke, M. Wieneke, W. Schwarz, D. Stalke | 117 | |
| Note | ||
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Enantioselective Catalysis, 122. Synthesis of New Optically Active
3,5-Dinitrosalicycloxazolines
Key words: 3,5-Dinitrosalicycloxazolines, Enantioselectivity, Catalysis, Cyclopropanations H. Brunner, B. Haßler | 126 | |
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Erratum
V. U. Ahmad, M. S. Ali, K. Usmanghani | 129 | |
| N u m b e r 2 | ||
| Original Communications | ||
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Crystal Structure of MgSO3·H2O
(In German)
Key words: X-Ray, Sulfites, Hydrates, Magnesium, Pseudosymmetry W. Buchmeier, B. Engelen, H. Müller | 131 | |
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Synthesis of Novel Lithium Salts with Doubly Charged Anions
for Secondary Batteries
(In German)
Key words: a,w-Perfluoro Alkanebis(sulfonylfluorides), 19F NMR Data, Bis(trifluoromethylsulfonyl)methane, Lithium Salts, Conductivity R. Jüschke, M. Köckerling, P. Sartori | 135 | |
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Synthesis of Spirocyclic Aminosilanes with Electron
Withdrawing Substituents at Nitrogen
Key words: Spirocyclic Sulfonamidosilanes, 1,2-Phenylene Diamides, Capped Tetrahedron, X-Ray Data, Chelation M. Wollenweber, R. Keese, H. Stoeckli-Evans | 145 | |
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Synthesis and Crystal Structure of the Lanthanum Titanate Tellurate
LaTi(Ti0.25Te0.75)O6 and its Relationship to
PbSb2O6 and Sr(MnTe)O6
(In German)
Key words: Lanthanum, Titanate, Tellurate, Crystal Structure L. Wulff, Hk. Müller-Buschbaum | 149 | |
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Oxochlorination of Transition Metal Complexes with Thionyl Chloride
(In German)
Key words: Thionyl Chloride, Oxochlorination, Metaloxodichloride, X-Ray Data C. Stoll, I.-P. Lorenz, H. Nöth, T. Seifert | 153 | |
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Ag2Cs[B15O24]: An Anhydrous Quaternary Silver(I)-Borate
with a New Helical Borate Anion
(In German)
Key words: Silver, Caesium, Borate, Synthesis, Crystal Structure A. Wiesch, K. Bluhm | 157 | |
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Synthesis and Characterisation of the Fullerene Co-Crystal
C60*SiH(C6H5)3
(In German)
Key words: Fullerene C60, Synthesis, Crystal Structure G. Waidmann, M. Jansen | 161 | |
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Oligomeric Tetrahedral Anions in Borophosphates: Synthesis and Crystal
Structures of
NaFe[BP2O7(OH)3] and
K2Fe2[B2P4O16(OH)2]
(In German)
Key words: Boron, Tetrahedral Anions, Phosphorus I. Boy, G. Cordier, B. Eisenmann, R. Kniep | 165 | |
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(Triphenylarsine)gold(I) Complexes: Synthesis of an Oxonium Salt
and Redistribution of the Arsine Ligands}
Key words: Gold(I) Complexes, Arsine Complexes, Oxonium Salts, Gold Clusters U. M. Tripathi, A. Schier, H. Schmidbaur | 171 | |
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Thermal Decomposition and Solution Calorimetry of Ammonium Neodymium
Chlorides
(In German)
Key words: Ammonium Neodymium Chlorides, Neodymium Chloride, Thermodynamical Data, Solution Calorimetry, Heat of Solution C. Hennig, H. Oppermann | 175 | |
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On the Chemical Transport of Rhenium and Rhenium Oxides
(In German)
Key words: Chemical Transport Reaction, Rhenium Oxides, Thermodynamic Calculation, Mass Spectra J. Feller, H. Oppermann, M. Binnewies, E. Milke | 184 | |
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Metal Complexes of Biologically Important Ligands, XCVIII.
Cyclopalladated Schiff Bases of a-Amino Acid and
Peptide Esters (In German)
Key words: N-Diphenylmethylene a-Amino Acid Esters, Peptide Esters, Ortho Palladation A. Böhm, B. Schreiner, N. Steiner, R. Urban, K. Sünkel, K. Polborn, W. Beck | 191 | |
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Crystal Structures of the Iodized closo-Hexaborates
trans-(Ph4P)2[B6H4I2],
mer-(Ph4P)2[B6H3I3] · 2
CH2Cl2, trans-(Ph4P)2[B6H2I4]
· 2 CH3CN and (CH2Py2)[B6HI5]
(In German)
Key words: Iodized closo-Hexaborates(2-), Crystal Structure D. Sonnak, W. Preetz | 206 | |
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Enantioselective Catalysis, XVIII.
The Influence of Non-Coordinated Stereocenters on the Enantioselective
Hydrogenation
(In German)
Enantioselective Hydrogenation, Chiral Phosphane Oxides,
Z-a-Acetamidocinnamic Acid, Ketones, Rhodium
Catalyst Ulrich Nagel, Christoph Roller | 211 | |
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Photoreactivity of Titanocene Pentasulfide
Key words: Charge Transfer, Titanium Complexes, Sulfide Complexes, Photochemistry H. Kunkely, A. Vogler | 224 | |
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Synthesis and Vibrational Spectra of cis- and
trans-[OsXY(acac)2], X \not= Y = Cl, Br, I, and Normal Coordinate
Analysis of trans-[OsClBr(acac)2]
(In German)
Key words: Dihalogeno-bis(acetylacetonato)osmium(IV), IR Data, Raman Data, Normal Coordinate Analysis, trans Influence K. Dallmann, W. Preetz | 227 | |
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Synthesis, Crystal Structure, Vibrational Spectra, and Normal Coordinate
Analysis of [Os(acac)3]
(In German)
Tris(acetylacetonato)osmium(III), Crystal Structure, IR Data, Raman Data,
Normal Coordinate Analysis
K. Dallmann, W. Preetz | 232 | |
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Synthesis and Crystal Structure of
[H2NMe2]+[(Me2NH)2TiCl4]-}
(In German)
Key words: N-Silyl Amides, Crystal Structure, Titanium R. Bettenhausen, W. Milius, W. Schnick | 239 | |
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18-Crown-6 and Small Carboxylic Acids. Formation and Structure of Binary
Adducts
with Formic and Acetic Acid, as well as Ternary Ones with Acetic
Acid and Water
(In German)
Key words: Acetic Acid, Crown Ether, Formic Acid, Hydrate, Melting Diagram A. Albert, D. Mootz | 242 | |
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The Promotive Properties of Alkali Metals Nitrate Melts for the Partial
Oxidation of Methane to Methanol
Partial Oxidation, Conversion, Selectivity, Molten Salt, Reduced Oxygen Species
B.-J. Lee, S. Kitsukawa, S. Asakura, K. Fukuda | 249 | |
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Interaction of the Vanadyl(IV) Cation with L-Ascorbic Acid and Related Systems
Key words: Vanadyl(IV), Ascorbid Acid, Oxidation Products, Solution Interactions, Solid Complexes E. G. Ferrer, P. A. M. Williams, E. J. Baran | 256 | |
| Note | ||
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Studies on Polyhalides, XXXIV. Cesium(18-crown-6)dichloroiodate,
[Cs(C12H24O6]ICl2
(In German)
Key words: Polyhalogenide, Dichloroiodate, Crown Complex, Cesium Compound, Crystal Structure M. El Essawi, K.-F. Tebbe | 263 | |
| N u m b e r 3 | ||
| Original Communications | ||
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Enantioselective Catalysis, XVII.
Enantioselective Catalytic Hydrogenation of Unfunctionalized Ketones
Key words: Enantioselective Hydrogenation, Unfunctionalized Ketones, Rhodium, Salt Effect, Solvent Effect Ulrich Nagel, Christoph Roller | 267 | |
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Isoselenocyanatoborates - Crystal Structures of
(n-Bu4N)[BH(NCSe)3] and (Ph4P)[B3H7(NCSe)]
(In German)
Key words: Triisoselenocyanatohydroborate(1-), Isoselenocyanato-heptahydrotriborate(1-), Crystal Structure B. Steuer, W. Preetz | 271 | |
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Redox Reactions of Molybdenum Compounds with
Bis(2-salicylidene-aminophenyl)disulfide.
Crystal Structure of
Salicylaldehyde-2-mercaptoanilato(2-)-triphenylphosphaneoxide-dioxomolybdenum(VI)
(In German)
Key words: Molybdenum Chelates, Ligand Exchange Reactions, Bis(2-salicylideneaminophenyl)-disulfide, Salicylaldehyde-2-mercaptoanilato(2-)-triphenylphosphaneoxide-dioxomolybdenum(VI), Crystal Structure W. Banße, J. Fliegner, S. Sawusch, U. Schilde, E. Uhlemann | 275 | |
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Ag+ as Substituent of an Alkaline Metal in Ag2SrMnV2O8
(In German)
Key words: Silver, Strontium, Manganese, Vanadium Oxide R. Rettich, Hk. Müller-Buschbaum | 279 | |
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Kagomé Layers Connected by Isolated Trigonal SrO6 Prisms in the
Strontium Manganate(IV) Tellurate(VI): SrMnTeO6
(In German)
Key words: Strontium, Manganese, Tellurate, Crystal Structure L. Wulff, Hk. Müller-Buschbaum | 283 | |
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Isolated 1¥[TeO5] Chains of Octahedra in the Lead
Tellurate Pb2TeO5
(In German)
Key words: Lead, Tellurate, Crystal Structure B. Wedel, L. Wulff, Hk. Müller-Buschbaum | 287 | |
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On the Crystal Chemistry of the Silver Manganese Oxovanadates
Ag2BaMnV2O8 and (AgCa2)Mn2(VO4)3
(In German)
Key words: Barium, Calcium, Manganese, Vanadium Oxide, Crystal Structure R. Rettich, Hk. Müller-Buschbaum | 291 | |
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Synthesis of Fluoroorganic O-(Trimethylsilyl)cyanhydrines
(In German)
Key words: O-Silylcyanohydrines, O-Trimethylsilylcyanhydrines, Cyanotrimethylsilane M. Sander, W. Sundermeyer | 296 | |
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Synthesis and Reactions with CO and C2H4 of Cobalt(I)
Complexes
Containing Trimethylphosphine and Chelating o-Diphenylphosphanylphenolate
Ligands
Key words: Cobalt, o-Phosphanylphenolate Complexes, Synthesis, Structure, Fluxionality H.-F. Klein, A. Brand, G. Cordier | 307 | |
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Spectrometric pK Determination of Daphnetin, Chlorogenic Acid
and Quercetin
Key words: Daphnetin, Chlorogenic Acid, Quercetin N. Sauerwald, M. Schwenk, J. Polster, E. Bengsch | 315 | |
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Bonding in an Unusual Nickel Carbide
Key words: Carbides, Molecular Orbitals, Electronic Structure, Metal Carbides, Square-Planar Carbon E. F. Merschrod S., Huang Tang, R. Hoffmann} | 322 | |
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Supersilylated Compounds of the Thirteenth Group, IV.
Supersilylelement Halides tBu3SiEX2 and
(tBu3Si)2EX with E = Al, Ga, In:
Syntheses, Properties, Structures
(In German)
Key words: Supersilylaluminum Halides, Supersilylgallium Halides, Supersilylindium Halides, Acid-base Reactions, Redox-Reactions, X-Ray Data N. Wiberg, K. Amelunxen, H.-W. Lerner, H. Nöth, J. Knizek, I. Krossing | 333 | |
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Solventothermal Synthesis of the Lamellar Selenidostannates(IV)
A2Sn4Se9·H2O (A = Rb, Cs)
and Cs2Sn2Se6
Key words: Tin, Selenium, Selenidostannates(IV), Lamellar Structures, Solventothermal Synthesis Anja Loose, William S. Sheldrick | 349 | |
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Cyclodisilazanes in cis Conformation - a Facile Synthesis
(In German)
Key words: Silicon, Lithium, Silylamide, Silaamidide, Cyclodisilazane U. Klingebiel, B. Tecklenburg, M. Noltemeyer, D. Schmidt-Bäse, R. Herbst-Irmer | 355 | |
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Investigations on the Chemical Transport Reaction of YX3 with
AlX3 and on the
Existence of Gaseous and Solid Complexes YAl3
X12 (X = Br, I)
(In German)
Key words: Chemical Transport Reaction, Yttrium Aluminium Halides, Enthalpy of Formation, Standard Entropy, Total Pressure Measurements H. Oppermann, S. Herrera, Dao Quoc Huong | 361 | |
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Synthesis and Mesomorphic Properties of
Polymethylene-a,w-bis
[2-thio-5-(4',4"n-alcoxybenzoyloxy)phenyl]-1,3,4-oxadiazole Key words: Liquid Crystal, Twin Mesogens, Oxadiazole, Mesomorphic Properties C. Aguilera, M. Parra, G. Fuentes | 367 | |
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Syntheses and Structures of Cyclopentadienyl Arsenic (III) Compounds Part
III:Tetraisopropylcyclopentadienyl Arsenic (III) Dibromide and
Tetraisopropylcyclopentadienyl Arsenic (III) Diiodide
(TipCpAsBr)2, (TipCpAsI)2)
Key words: Arsenic, Arsenic Halides, Cyclopentadienyl Arsenic Compounds, Crystal Structure K. Megges, E. V. Avtomonov, R. Becker, J. Lorberth | 371 | |
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Crystal Structure of [Mo(CO)3(NCMe)(StBu)]2
(In German)
Key words: Molybdenum Carbonyl Complex, Thiolato Complex, Crystal Structure M. R. Kopp, B. Neumüller | 378 | |
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The Molecular Structures and Conformational Preferences of
Bis(dimethylstibyl)-Sulfane and -Tellurane, E(SbMe2)2, E = S or Te,
Me = CH3, by Density Functional Theory Calculations and Gas Electron
Diffraction
Key words: Distibylsulfane, Distibyltellurane, Density Functional Theory Calculations, Gas Electron Diffraction A. Haaland, D. J. Shorokhov, H. V. Volden, H. J. Breunig, M. Denker, R. Rösler | 381 | |
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Experimental and Computational Studies on Aminoguanidine Free Base,
Monocation and Dication. Part III Proton Affinities of Guanidine,
Aminoguanidine and Glyoxal Bis(amidinohydrazone)
Key words: Proton Affinity, gas Phase Basicity, Acid Dissociation Constant J. T. Koskinen | 386 | |
| Note | ||
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Reaction of 9-Borabicyclo[3.3.1]nonane with N-Trimethylsilylamines -
Cleavage of the N-Si or N-H Bond
Key words: Aminoborane, Aminosilane, Boron, Pyridine, NMR Data B. Wrackmeyer, G. Kehr, S. Ali | 393 | |
| N u m b e r 4 | ||
| Original Communications | ||
|
Phase Relations and Chemical Transport of the Compounds
in the Ternary System Re/Mo/O
(In German)
Key words: Rhenium Molybdenum Mixed Oxides, Chemical Transport Reaction, Phase Diagram J. Feller, H. Oppermann, R. Kucharkowski, S. Däbritz | 397 | |
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Dimeric and Polymeric Pnictidostannate(IV) Anions - Preparation and
Crystal
Structures of Na2K3[SnP3], Na2Cs3[SnP3] and
Na2K3[SnBi3]
(In German)
Key words: Disodium Tripotassium Triphosphidostannate(IV), Disodium Tricesium Triphosphidostannate(IV), Disodium Tripotassium Tribismutidostannate(IV), Dimeric Tetrahedral Anions, Zweier Single Chains M. Asbrand, B. Eisenmann, H. Engelhardt, U. Rößler | 405 | |
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Some Applications of Ultrahigh Resolution 15N NMR Spectroscopy
Key words: NMR Data, Ultrahigh Resolution B. Wrackmeyer, \-E. Kup\vce | 411 | |
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Coordination Ambidence of the Thiocyanate Anion in
Alkali Trithiocyanatomanganate(II) Hydrates
(In German)
Key words: Alkali Thiocyanatomanganate(II) Hydrates, Crystal Structure, Coordination Ambidence M. Biedermann, H. Hartung, H. Böhland, R. Matthäus | 416 | |
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Charge Transfer Interaction in (Riboflavin)tricarbonylrhenium(I) Chloride
Key words: Charge Transfer, Rhenium Complexes, Riboflavin H. Kunkely, A. Vogler | 423 | |
|
The Low Temperature Crystal Structure of Trimethylsilanol
(In German)
Key words: Trimethylsilanol, Preparation, Crystal Structure R. Minkwitz, S. Schneider | 426 | |
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Synthesis and Structure of Benzyltriethylammonium Trichlorogermanate(II)
Key words: Germanium Dichloride, Trichlorogermanate(II) G. L. Wegner, A. Jockisch, H. Schmidbaur | 430 | |
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An Aluminium-Oxide-Isopropoxide Cluster with Peripheral Ammonia Ligands
Key words: Aluminium Isopropoxide, Aluminium Oxide Isopropoxide, Ammonia Complex, Cluster U. M. Tripathi, A. Schier, H. Schmidbaur | 434 | |
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Studies on Sodium Trifluoromethanesulfonate.
Crystal Structure of Sodium
Trifluoromethanesulfonate-Trifluoromethanesulfonic Acid (1/3)
(In German)
Key words: Sodium Trifluoromethanesulfonate, Sodium Triflate, Trifluoromethanesulfonic Acid, Synthesis, Crystal Structure G. Korus, M. Jansen | 438 | |
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A Further 2l5,4l5-Diphosphapyridine:
2,2,4,4-Tetrakis-(dimethylamino)-6-amino-1-aza-2l5,4l5-diphosphinine (In German)
Key words: l5-Diphosphete, 1-Aza-2l5,4l5-diphosphinine, NMR Spectra, X-Ray Data G. Heckmann, E. Jonas, E. Fluck, B. Neumüller | 443 | |
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Metal Complexes of Biologically Important Ligands, CIV.
ortho-Palladated Complexes
of N,N-Dimethyl-C-phenylglycine-methylester.
Synthesis of a-Amino Acid Derivatives
by Insertion
of Isocyanides, CO, Alkenes, and Alkynes into the Pd-C Bond
(In German)
Key words: Palladium(II) Complexes, ortho-Palladation, N,N-Dimethyl-C-phenylglycine, Insertion Reactions A. Böhm, K. Polborn, K. Sünkel, W. Beck | 448 | |
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New Syntheses with Magnesium Hydride.
Part 3: Preparation of Nanocrystalline or Amorphous Metals by Hydride
Reduction
(In German)
Key words: Nanocrystalline Metals, Amorphous Metals, Hydride Reduction, Magnesium Hydride W. Knott, G. Frommeyer, A. Klapdor, D. Windbiel | 459 | |
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Structure of the Short-Lived Intermediate Formed during the Metal
Substitution Reaction of the Mercury(II) Porphyrin Complex with
Cobalt(II) Ion in Aqueous Solution Determined by the Stopped-Flow
EXAFS Method
Key words: Structure of Short-Lived Intermediate, Stopped-Flow EXAFS, Metal Substitution Reaction, Cobalt(II) Porphyrin Complexes, Cobalt(III) Porphyrin Complex K. Ozutsumi, S. Ohnishi, H. Ohtaki, M. Tabata | 469 | |
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Enantioselective Catalysis, 120.
New Optically Active Pyrrole-oxazolines
Key words: Pyrrole-oxazolines, Enantioselectivity, Catalysis, Cyclopropanations H. Brunner, B. Haßler | 476 | |
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Carbacylamidophosphates: Synthesis, Properties, and Structure of
Dimorfolido-N-trichloroacetylphosphorylamide
Key words: Carbacylamidophosphates, IR Data, X-Ray Data V. A. Ovchynnikov, V. M. Amirkhanov, T. P. Timoshenko, T. Glowiak, H. Kozlowski | 481 | |
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Absolute Configuration of Chiral
1,3,4,5-Tetrahydro-2H-1,5-benzodiazepin-2-ones
Key words: Chiral 1,5-Benzodiazepin-2-ones, Crystal Structure, Absolute Configuration M. Hasan, T. A. Nizami, A. Malik, C. Ohlendorf, W. Hiller, W. Voelter | 485 | |
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Utility of Cyano Acid Hydrazide in Heterocyclic Chemistry: A New Route for
the Synthesis of New 1,2,4-Triazolo[1,5-a]pyridines and
1,2,4-Triazolo[1,5-a]isoquinolines
Key words: 1,2,4-Triazolo[1,5-a]pyridines, 1,2,4-Triazolo[1,5-a]isoquinolines A. H. M. Hussein | 488 | |
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CT Complexes Derived from Verdazyl Radicals
Key words: Verdazyl Radical, Stable Radical, CT Complex, Magnetic Property, X-Ray Data S. Nakatsuji, A. Kitamura, A. Takai, K. Nishikawa, Y. Morimoto, N. Yasuoka, H. Kawamura, H. Anzai | 495 | |
| Note | ||
|
The Crystal Structures of MesSn(Cl)Me2 and MesSnCl2
(In German)
Key words: Mesitylin Compounds, Chloro Compounds, Crystal Structure T. Kräuter, B. Neumüller | 503 | |
| N u m b e r 5/6 | ||
| Original Communications | ||
|
Preparation and Structure of
NaCa3Mn(V2O7)(V3O10)
(In German)
Key words: Sodium, Calcium, Manganese, Vanadium Oxide, Crystal Structure R. Rettich, Hk. Müller-Buschbaum | 507 | |
|
Ba4Mn2Ag2O(AsO4)4, a Barium Manganese
Oxide-Arsenate Showing
Nonlinear O-Ag-O Dumbbells
(In German)
Key words: Barium, Manganese, Silver, Oxide-Arsenate, Crystal Structure M. Staack, Hk. Müller-Buschbaum | 512 | |
|
Partial Tetrahedral Oxygen Coordination of Indium in
BaIn2Zn3O7.
A Consideration of the
Ba2Ln2Zn8O13/BaLnAlZn3O7 Type
(In German)
Key words: Barium, Indium, Zinc, Oxide, Crystal Structure O. Sfreddo, Hk. Müller-Buschbaum | 517 | |
|
On an Vanadyl Oxocuprate Phosphate CaCu(VO)(PO4)2 Containing
Cu2+ at Positions
of VO2+ Ions and a Copper
Rich Phase CaCu1.13(VO)0.87(PO4)2
(In German)
Key words: Calcium, Copper, Vanadyl-Phosphate, Crystal Structure S. Meyer, Hk. Müller-Buschbaum | 521 | |
|
Connection of (TeO6)6 and (TeO6)3(NiO6)3
Hexagons by
TeNiO9 Octahedra Double in Pb3Ni4,5Te2,5O15}
(In German)
Key words: Lead, Nickel, Tellurium Oxide, Crystal Structure B. Wedel, K. Sugiyama, Hk. Müller-Buschbaum | 527 | |
|
Preparation and X-Ray Structure of
3,5-Dimethyl-1,4-dichloro-1,2,6-thiadiazine-1-oxide
Key words: Crystal Structure, 1,2,6-Thiadiazines, Sulfanuric Chloride T. Chivers, Xiaorong Li, M. Parvez | 532 | |
|
Pentafluoro[(4-methyl-1,4-bisazoniacyclohex-1-yl)methyl]germanate
Hydrate: Synthesis and Crystal Structure of a Zwitterionic
l6Ge-Germanate with a
GeF5C Framework
Key words: Hexacoordinate Germanium, Zwitterion, Preparation, Crystal Structure R. Tacke, J. Heermann, M. Pülm | 535 | |
|
Mesitylene Osmium(II) Complexes Containing the Functional Phosphane
tBuP(CH2CO2Me)2 and Anionic Species Derived Thereof
as Bi- and
Tridentate Ligands
Key words: Osmium, Halfsandwich Complexes, Chelate Complexes, Phosphanediyldiester G. Henig, H. Werner | 540 | |
|
Benzylgallium Compounds. The Crystal Structures of
[Mg3Br2,4Cl1,6(OEt2)6][Ga(CH2Ph)4]2
· 0.5 Toluene and
[(3,5-Me2C6H3CH2)2GaBr]2
(In German)
Key words: Gallium Compounds, Magnesium Compound, Crystal Structures} M. R. Kopp, B. Neumüller | 545 | |
|
Crystal Structure of [Me3PN(H)PMe3]4I28, a Polyiodide
with I3-, I82-, and I144- Ions
(In German)
Key words: Polyiodide, Synthesis, Crystal Structure T. Gröb, F., K. Dehnicke | 552 | |
|
In situ Neutron Diffraction on DxNb2O5
Key words: Neutron Diffraction, Electrochemical Cell, Niobium-(V)-oxide, Niobium Hydrogen Bronze, Hydrogen Distribution T. Unruh, G. Schwitzgebel, C. Ritter | 557 | |
|
The First Hydrogen Containing (Polyfluorocycloalken-1-yl)xenon(II) Salts
Key words: Xenon Difluoride, Fluorinated Alkenylxenon(II) Salts, Fluorinated Arylxenon(II) Salts, Oxidative Fluorination H.-J. Frohn, V. V. Bardin | 562 | |
|
Crystal Structure of
1,1'-Dimethyl-4,4'-bipyridinium-octachlorodiantimonate(III)
(In German)
Key words: Crystal Structure, 1,1'-Dimethyl-4,4'-bipyridinium-octachlorodiantimonate(III) B. Jaschinski, R. Blachnik, H. Reuter | 565 | |
|
Crystal Structure of the Double Complex Salt
trans-(py2CH2)[Pt(OH)2(ox)2]
·
trans-(py2CH2)[Pt(OH)(ox)2(H2O)]2·4H2O
(In German)
Key words: trans-Dihydroxobis(oxalato)platinate(IV), trans-Hydroxobis(oxalato)aquaplatinate(IV), Crystal Structure, Hydrogen Bonding J.-G. Uttecht, W. Preetz | 569 | |
|
Tetrakis(sulfurdiimido)silane, -germane and -stannane
Key words: Silicon, Germanium, Tin, Sulfur Diimides, Heterocycles, NMR Data M. Herberhold, S. Gerstmann, B. Wrackmeyer | 573 | |
|
Synthesis and Characterization of Amino Acid Complexes of Platinum(IV)
Stabilized by Crown Ethers
(In German)
Key words: Platinum(IV) Complexes, Crown Ethers, Amino Acids, Crystal Structure D. Steinborn, O. Gravenhorst, H. Junicke, F. W. Heinemann | 581 | |
|
Hydrido(acylphenolato)cobalt(III) Compounds Containing
Trimethylphosphane Ligands
(In German)
Key words: Acylcobalt(III) Complexes, Reactions, Structure, Hard-Soft Chelating Ligands H.-F. Klein, S. Haller, H. Sun, X. Li, T. Jung, C. Röhr, U. Flörke, H.-J. Haupt | 587 | |
|
Onio-Assisted SN2-Reactions: General Access to Symmetrical and
Unsymmetrical Geminally Bisonio Substituted Methane Derivatives
(In German)
Key words: Geminal Bisonium Salts, SN-Reactions, Electrostatic Effects, Synthesis, X-Ray Data R. Weiss, M. Handke, S. Reichel, F. Hampel | 599 | |
|
Anodic Methoxylation of Isatin
Key words: Indole, Isatin, Electrochemistry, Anodic Methoxylation A. Nied\'zwiecka-Korna\'s, E. Bojarska, J. Kami\'nski, Z. Kazimierczuk | 620 | |
| Notes | ||
|
Novel Synthesis and Molecular Structure of Benzyl Potassium
(thf)[KCH2C6H5]2
(In German)
Key words: Potassium, Bezyl Potassium, X-Ray Data M. Westerhausen, W. Schwarz | 625 | |
|
Further Compounds of the Ba6Nd2Al4O15 Type:
Ba4Nd4Zn3PtO15 and
Ba4Eu4Zn3PtO15
(In German)
Key words: Barium, Rare Earth Metals, Zinc, Oxide, Crystal Structure O. Sfreddo, Hk. Mller-Buschbaum | 628 | |
|
Fe[B2P2O7(OH)5:
A New Borophosphate Containing Non-Branched Tetrahedral Vierer-Einfach Chains
(In German)
Key words: Boron, Iron, Phosphorus, Tetrahedral Chains, Borophosphates I. Boy, C. Hauf, R. Kiep | 631 | |
|
Polysulfonylamines, CIII. A Hydroxylymine with a Remarkably Short O-N Bond:
Crystal and Molecular Structure of MeO-N(SO2Me)2
(In German)
Key words: O-Methyl-N,N-di(methanesulfonyl)hydroxylamine, Crystal Structure M. Näveke, A. Blachette, P. G. Jones | 634 | |
|
3,10,17,24-Tetra(1-methylethyl)-[29H,31H-tetrapyrido[2,3-b:2',3'-g:2''-3''-
I:2''',3'''-q]porphyrazinato-(2-)N29,N30,N31,N32]-nickel-Eu(fod)3]4
- A Souble Pyridoporphyrazine
(In German)
Key words: Pridoporphyrazines, Coordination Compound, High Solubility A::K. Eichinger, C. Brunmair, M. Bucher | 637 | |
| N u m b e r 7 | ||
| Original Communications | ||
|
Studies on Polyhalides, XXXVI.
On the Octaiodide Ion I82-:
Preparation and Crystal Structure of
[(Crypt-2.2.2)H2]I8,
of [Ni(phen)3]I8·2CHCl3
and of the (N-alkylurotropinium)octaiodides (UrR)2I8
with R = methyl and ethyl
(In German)
Key words: Cryptate, N-Alkyl-Urotropinium Cation, Tris(1,10-phenanthroline)nickel(II), Octaiodide, Crystal Structure Arista Gräfe-Kavoosian, Shida Nafepour, Klaus Nagel, Karl-Friedrich Tebbe | 641 | |
|
Gold(I) Complexes with Amine Ligands, II.
Methylpyridine Complexes of Gold(I)
(In German)
Key words: Gold(I), Pyridine, Amine Complexes, X-Ray Data P. G. Jones, B. Ahrens | 653 | |
|
Reactions of Lithium Hydridosilylamides with Carbonyl Compounds and
Mixtures of Carbonyl Compounds and Chlorotrimethylsilane
(In German)
Key words: Hydridosilylamides, Reaction Behaviour, Imines, Hydrosilylation Jan Schneider, Eckhard Popowski, Hans Fuhrmann | 663 | |
|
Ternary Intermetallic Compounds LnMn2Al10 (Ln = Y, La-Nd, Sm,
Gd-Dy)
and LnRe2Al10 (Ln = Ce, Pr, Sm) with
CaCr2Al10-Type Structure
Key words: Intermetallic Compounds, Crystal Structure, X-Ray Data V. M. T. Thiede, W. Jeitschko | 673 | |
|
The Partial Oxidation of Methane to Methanol
with Nitrite and Nitrate Melts
Key words: Superoxide Ion, Nitrite, Nitrate, Partial Oxidation, Methanol B.-J. Lee, S. Kitsukawa, H. Nakagawa, S. Asakura, K. Fukuda | 679 | |
|
Crystal Engineering towards Design of Macrocyclic Coordination
Compounds:
Crystal Structure of Rubidium Tetrachloro- and
Tetracyanoaurate(III) Complexes with 18-Crown-6
Key words: 18-Crown-6, Rubidium Macrocyclic Complexes, Gold(III), Crystal Structure J. A. Manskaya, K. V. Domasevitch, V. V. Ponomareva, J. Sieler, V. N. Kokozay | 683 | |
|
Dioxomolybdenum(VI) Complexes with Tridentate Diacidic Ligands
(In German)
Key words: Ligand Exchange Reactions, Dioxomolybdenum(VI) Complexes, Tridentate Diacidic Ligands, Crystal Structure W. Banße, J. Fliegner, S. Sawusch, U. Schilde, E. Uhlemann | 689 | |
|
Structure Analysis of Dihalogeno(diphosphine)nickel Complexes
in Solution
with Differential Puls Polarography
(In German)
Key words: Dihalogeno(diphosphine)nickel Complexes, NMR Data M. Mutz, H. P. Latscha | 694 | |
|
Synthesis, Spectroscopic Studies, and Crystal Structure of
Diethylchlorotin Dimethylphosphinate Et2ClSnO2PMe2
Key words: Crystal Structure, IR Data, Mass Spectroscopic Data, Diethylchlorotin Dimethylphosphinate A.-F. Shihada, F. Weller | 699 | |
|
Studies on Tetramethylammonium Selenate(VI) and Chromate(VI)
Key words: Tetramethylammonium Selenate(VI), Tetramethylammonium Chromate(VI), Crystal Structure, Vibrational Spectra, Thermal Analysis M. Malchus, M. Jansen | 704 | |
|
Francoanellite K3Al5(HPO4)6(PO4)2
· 12 H2O: Structure and Synthesis by
Topochemical Dehydration of Taranakite
(In German)
Key words: Crystal Structure, Neutron Scattering, Francoanellite, Taranakite, Topochemical Reaction S. Dick, T. Zeiske | 711 | |
|
Stable Carbene Adducts of Chlorine
(In German)
Key words: Carbene, Chlorine, X-Ray Data N. Kuhn, J. Fahl, R. Fawzi, C. Maichle-Mößmer, M. Steimann | 720 | |
|
Complexation of Beryllium(II) by Maleic and Succinic Acid
Key words: Beryllium(II), Maleic Acid, Succinic Acid, X-Ray Data M. Schmidt, A. Bauer, A. Schier, H. Schmidbaur | 727 | |
|
Polysulfonylamines, CV. The First N,NDisulfonylated Sulfinic Amides:
Synthesis and Crysal Structures of RS(O)-N(SO2Me)2 (R = Me,
CCl3)
(In German)
Key words: N,N-Bis(organosulfonyl)sulfinamides, Synthesis, Crystal Structure, Long S(O)-N Bonds M. Näveke, A. Blaschette, P. G. Jones | 734 | |
|
1,2,3,4-Tetrahydroquinolines as Substrates for Mannich Compounds
(In German)
Key words: Aminals, Iminium Salts, C- and N-Aminomethylations, Naphthols H. Möhrle, E. Tot, S. Rüdiger | 742 | |
|
Solid Phase Synthesis of Muramyl Dipetides on Isomeric Trialkoxybenzylamine
Resins
(In German)
Key words: Muramyl Peptides, Solid Phase Glycopeptide Synthesis, Peptide Amide Synthesis, Glycopeptides H.-J. Kohlbau, J. Tschakert, R. A. Al-Qawasmeh, T. A. Nizami, A. Malik, W. Voelter | 753 | |
|
Oxidation-Induced Acyl Group Transfer from Hydroquinone Esters to
Nucleophiles
Key words: Acyl Group Transfer, Hydroquinone Esters, Oxidation, Dipeptides, Active Esters G. Reischl, M. El-Mobayed, R. Beiáwenger, K. Regier, C. Maichle-Mössmer, A. Rieker | 765 | |
| Notes | ||
|
Synthesis and Crystal Structure of [Cu2(OAc)4(NCMe)2] ·
2MeCN
Key words: Copper Compound, Acetato Complex, Crystal Structure M. Ghassemzadeh, K. Aghapoor, B. Neumüller | 774 | |
|
On the Preparation and Spectroscopic Characterization of
(Me3SiO)3PH+I-
(In German)
Key words: Tris(trimethylsiloxy)phosphonium Iodide, Vibration Spectra, NMR Data R. Minkwitz, S. Schneider | 777 | |
| N u m b e r 8 | ||
| Original Communications | ||
|
Variations in the Chain Structure of Cationic (Phosphine)gold(I)
Dialkyldithiophosphate Complexes
Key words: Gold Complexes, Phosphinates, Thiophosphinates, Dithiophosphinates M. Preisenberger, A. Schier, H. Schmidbaur | 781 | |
|
The Solution and Solid State Structure of L-Carnitine L-Tartrate
Key words: Carnitine, Tartrate, Hydrogen Bonds H. Schmidbaur, A. Schier, A. Bayler | 788 | |
|
Interactions in Molecular Crystals, 143.
ortho-Benzene Derivatives with Meshed
Cogwheel Chloromethyl and Methylamino Substituents: Structures and Rotation
Enthalpy Hypersurfaces
(In German)
Key words: ortho-Benzene Derivatives, Meshed Cogwheel Substituents, Crystal Structure, Rotation Enthalpy Hypersurfaces H. Bock, N. Nagel | 792 | |
|
Interactions in Molecular Crystals, 144.
ortho-Benzene Derivatives with Meshed Cogwheel
Trimethylsilyl
Substituents: Structural
Comparison with Benzene-1,2-disulfonate Salts and
Rotation Enthalpy Hypersurfaces
(In German)
Key words: ortho-Benzene Derivatives, Meshed Cogwheel Substituents, Crystal Structure, Rotation Enthalpy Hypersurfaces H. Bock, N. Nagel | 805 | |
|
Crystal Structure of Cs2[B6H5(SCN)]
(In German)
Key words: Thiocyanato-pentahydro-closo-hexaborate(2-), Crystal Structure W. Preetz, S. Zander, C. Bruhn | 816 | |
|
Synthesis, Spectroscopic Characterization and Crystal Structure of
Dicyclopentadienylcobalt-hexahydro-closo-hexaborate
[(C5H5)Co(C5H4)B6H5Hfac]}
(In German)
Key words: Dicyclopentadienylcobalt-hexahydro-closo-hexaborate, Crystal Structure, 11B NMR T. Schaper, W. Preetz | 819 | |
|
Crystal Structures, Vibrational Spectra and Normal Coordinate Analyses
of trans-[OsO2(ox)2]2- and
trans-[OsO2(mal)2]2-
(In German)
Key words: trans-Dioxo-bisoxalatoosmate(VI), trans-Dioxo-bismalonatoosmate(VI), Crystal Structure, Vibrational Spectra, Normal Coordinate Analysis A. Strueß, W. Preetz | 823 | |
|
Synthesis, 11B and 19F NMR Spectra of the
Monofluoropentaiodo-closo-hexaborate
Anion and the Crystal Structure
of (CH2Py2)[B6FI5]
(In German)
Key words: Monofluoropentaiodo-closo-hexaborate(2-), Crystal Structure, 11B and 19F NMR Spectra H. Thomsen, W. Preetz | 829 | |
|
Synthesis and X-Ray Structure of 1,3,5-Tri(phenylethynyl)benzene
Key words: Ethynylbenzene, X-Ray Data M. N. Bochkarev, M. A. Katkova, E. A. Fedorova, N. P. Makarenko, H. Schumann, F. Girgsdies | 833 | |
|
Synthesis, IR and X-Ray Studies of
Tetra(N,N'-tetraethyl-N"-benzoylphosphorictriamide)-tetra(m-3-methoxo)-tetra(methanol) tetra-Nickel(II)
Key words: Nickel (II), Carbacylamidophosphates, X-Ray Data V. A. Ovchynnikov, V. M. Amirkhanov, A. A. Kapshuk, T. Y. Sliva, T. Glowiak, H. Kozlowski | 836 | |
|
A New Synthesis of
Tetrakis(C-methyl)octakis(hydroxyethyl)calix[4]resorcinarene via an
Ethoxy-Tethered Trimethylsiloxy Precursor
Key words: Calix[4]resorcinarenes, Conformational Isomers, Spacer Groups, X-Ray Data I. Neda, T. Siedentop, A. Vollbrecht, H. Thönnessen, P. G. Jones, R. Schmutzler | 841 | |
|
The Bis(trimethylsilyl)ester of Carbonic Acid: Spectroscopic Characterization
and Improved Preparation
(In German)
Key words: Bis(trimethylsilyl)ester of Carbonic Acid, Vibrational Spectra, NMR Data R. Minkwitz, S. Schneider | 849 | |
|
Photooxidation of Dicyanoaurate(I) Induced by Metal-to-Ligand Charge
Transfer Excitation
Key words: Photochemistry, Charge Transfer, Gold Complexes, Cyanide Complexes H. Kunkely, A. Vogler | 853 | |
|
Halogeno(acylphenolato)cobalt(III) Compounds Containing
Trimethylphosphane Ligands
(In German)
Key words: Acylcobalt(III) Complexes, Reactions, Structure, Hard-Soft Chelating Ligands H.-F. Klein, S. Haller, H. Sun, X. Li, T. Jung, C. Röhr, U. Flörke, H.-J. Haupt | 856 | |
|
Reaction of [Co(But2PH)2I2] with
[Ru3(CO)12]: Synthesis and X-Ray Crystal Structure
of [Ru3(CO)6(m-H)(m-I)2(m-PBut2)(But2PH)] (In German)
Key words: Cobalt, Ruthenium, Cluster, Phosphido-Bridged, Crystal Structure M. Graf, K. Merzweiler, C. Bruhn, H.-C. Böttcher | 865 | |
|
Crystal Structure and Spectroscopic Behaviour of a
Binuclear
Copper(II) Complex of Mefenamic Acid and Dimethylsulfoxide
Key words: Copper(II), Mefenamic Acid, Crystal Structure, Spectral Data G. Facchin, M. H. Torre, E. Kremer, O. E. Piro, E. J. Baran | 871 | |
|
Electrochemical Study of
Tricarbonyl(h6-cyclooctatetraene)metal(0)
Complexes of the Group 6 Elements
Key words: Carbonyl, Chromium, Molybdenum, Tungsten, Cyclic Voltammetry G. A. Yilmaz, A. M. Önal, S. Özkar | 875 | |
|
On the Reaction of 2,3-Dihydroimidazol-2-ylidenes with
Pentafluoropyridine:
Carbenes as Reactants in Nucleophilic Aromatic
Substitution
(In German)
Key words: Carbenes, Imidazoles, Pyridines, Nucleophilic Aromatic Substitution, Hydrogen Bonds N. Kuhn, J. Fahl, R. Boese, G. Henkel | 881 | |
|
On the Reaction of Bis(t-butylamino)dimethylsilane with Titanium
Tetrachloride. Crystal Structures of the Imido Complex
[TiCl2(N-CMe3)(H2N-CMe3)(CH3CN)]2
and of the
Ketimido Complex [TiCl3{NC(Me)N(H)CMe3}(CH3CN)2]
(In German)
Key words: Titanium, Imido Complex, Ketimido Complex, Crystal Structure A. Mommertz, R. Leo, W. Massa, K. Dehnicke | 887 | |
|
Tuning the Steric and Electronic Properties of Chiral Rhenium Thiolate
Complexes
Key words: Rhenium Complexes, Thiolate Ligands, Structure N. Burzlaff, M. Hagel, W. A. Schenk | 893 | |
|
On the Crystal Structure of Ho2Se3
(In German)
Key words: Holmium Sesquiselenide, Chemical Transport, Crystal Structure W. Urland, H. Person | 900 | |
|
Metal Ion-Binding Properties in Aqueous Solution of the Nucleoside Analogue,
5,6-Dichloro-1-(b-D-ribofuranosyl)benzimidazole (DRB)
Key words: Acidity Constants, Benzimidazole Type Ligands, Imidazole Type Ligands, Metal Ion Complexes, Steric Inhibition L. E. Kapinos, B. Song, H. Sigel | 903 | |
|
Synthesis of Some Chromanone Derivatives and the Use of DNA in Evaluation of
their Biological Activity
Key words: Chromanone, Visnagin, Dibenzopyranone, Benzimidazole, Furochromone E-S I. El-Desoka, E. M. El-Telbani, M. A. Hammad, F. A. Badria, A-R. H. Abded-Rahman | 909 | |
|
[R2S-CH2-OTf]+OTf- as a Reagent with an Optionally Mono-
or Biselectrophilic Csp3 Center
Key words: Geminal Bisonium Salts, SN-Reaction, Synthesis, Regioselectivity, X-Ray Data R. Weiss, M. Handke, F. Hampel | 916 | |
| Note | ||
|
Preparation, Structures and Optical Properties of
[H3N(CH2)6NH3]BiX5 (X = I, Cl) and
[H3N(CH2)6NH3]SbX5 (X = I, Br)
Key words: Alkylammonium Halogenobismuthates and Antimonates, Excitonic Spectra, Dielectric Properties G. A. Mousdis, G. C. Papavassiliou, A. Terzis, C. P. Raptopoulou | 927 | |
| N u m b e r 9 | ||
| Original Communications | ||
|
Thermochromic Chloro- and Bromocuprates:
[C(NH2)3]2CuBr4,
(H3CC2N2SNH3)2[Cu2Br6],
(C7N3H14)2[CuCl4],
(C7N3H14)2[CuBr4],
[(Cl, Br)C3N2H6][CuCl3OH2] and
(BrC3N2H6)2[CuBr4]
(In German)
Key words: Chloro Cuprates, Bromo Cuprates, Crystal Structures, Thermochromism I. Díaz, V. Fernández, J. L. Martínez, L. Beyer, A. Pilz, U. Müller | 933 | |
|
The Trichlorogermanite(II) Anion and its Gold(I) Complexes
Key words: Germanium(II), Trichlorogermanite(II), Gold-Germanium Compounds, Arsine Complexes, Germylene Insertion U. M. Tripathi, G. L. Wegner, A. Schier, A. Jockisch, H. Schmidbaur | 939 | |
|
Pyridine-Derived Tetrapodal Ligands with NO4 and NN4 Donor Sets
Key words: Template Reaction, Tetrapodal Pentadentate Ligand, Pentaamine, Hydrobromide S. Schmidt, L. Omnès, F. W. Heinemann, J. Kuhnigk, C. Krüger, A. Grohmann | 946 | |
|
Controlled Crystallization of the Gadolinium(III) Complex of
Diethylenetriamine-Pentaacetate: Monomeric and Dimeric Structure
(In German)
Key words: Gadolinium(III) Chelates, Diethylenetriamine-Pentaacetate Complexes, Coordinated Water, Solid State Structures, Magnetic Resonance Imaging R. Ruloff, T. Gelbrich, E. Hoyer, J. Sieler, L. Beyer | 955 | |
|
2-Bromo-5-iodo-hydroquinone and its Symmetrical and Unsymmetrical
Dialkylethers
Key words: Hydroquinones, Building Blocks for Nanostructures, Halogenation, Ipso Substitution S. Höger, Klaus Bonrad, G. Schäfer, V. Enkelmann | 960 | |
|
Metal Complexes of Biologically Important Ligands CVI.
Metal Complexes of Donor Substituted Oxazolones and of Bis(oxazolones)
(In German)
Key words: Oxazolones, Nickel, Palladium, Platinum, Copper, Ruthenium M. Prem, W. Bauer, K. Polborn, W. Beck | 965 | |
|
Synthesis and Crystal Structure of a Novel Germatrane:
1-Bis(trimethylsilyl)aminogermatrane
Key words: Hydroxy Germatrane, Bis(amino)stannylene, Amino Germatrane, X-Ray Data S. N. Nikolaeva, K. Megges, J. Lorberth, V. S. Petrosyan | 973 | |
|
Crystal Structures of Me2Si[N(SiMe3)2]2 and
[Me2Si(NPh)(NHPh)Li · OEt2]2
(In German)
Key words: Silylamine, Lithium Amide, Crystal Structure A. Mommertz, G. Geiseler, K. Harms, K. Dehnicke | 977 | |
|
N-Benzoylthiocarbamoyl Amino Acid Ethyl Esters as Chelate Ligands
for Transition Metal Ions
Key words: Thioureas, Amino Acid Ethyl Esters, Chelates, NMR Data, Crystal Structure F. Leßmann, L. Beyer, R. Richter, R. Meusinger | 981 | |
|
Theoretical and Experimental Investigations on the Protonation of
Substituted closo-Hexaborates - [B6H5HfacF]- and
[B6H5HfacCH3]-}
(In German)
Key words: Fluoro-hexahydro-closo-hexaborate(1-), Methyl-hexahydro-closo-hexaborate(1-), Protonation, NMR Data, Vibrational Spectra B. Steuer, G. Peters, W. Preetz | 991 | |
|
1,2-Bis(1',3'-dimethylimidazolin-2'-iminato)ethane - a Novel
Chelating Ligand
(In German)
Key words: Imines, Palladium, Chelates, Ligand Effects, X-Ray Data N. Kuhn, M. Grathwohl, M. Steimann, G. Henkel | 997 | |
|
Supersilyl Compounds of Phosphorus, V.
Preparation, Structure and Reactivity of the Pentaphosphide
(tBu3Si)3P5Na2
and the Pentaphosphane (tBu3Si)3P5
(In German)
Key words: Silicon, Phosphorus, Supersilyl, Oligophosphides and -phosphanes, NMR Data, X-Ray Data N. Wiberg, A. Wörner, H.-W. Lerner, K. Karaghiosoff, H. Nöth | 1004 | |
|
Benzo[b]fluorenes Formed in the Thermal Cyclization of 3-Ene-1,6-diynes
Key words: Enediyne, Cyclization, X-Ray Data, Biradical M. Schmittel, M. Strittmatter, W. A. Schenk, M. Hagel | 1015 | |
|
Electron Donor-Acceptor Compounds. Synthesis and Structure of
5-(1,4-Benzoquinone-2-yl)-10,15,20-trialkylporphyrins
Key words: Porphyrins, Quinones, Electron Transfer Compounds, Crystal Structure, Conformation S. Runge, M. O. Senge | 1021 | |
|
Liquid Crystals in the Series of 2,3,6,7-Tetraalkoxytriphenylenes
(In German)
Key words: Triphenylenes, Photoconductivity, Discotic Mesogens, Push-Pull Substitution B. Rose, H. Meier | 1031 | |
|
Axial Chirality in Squre-Planar Metal Complexes
Key words: Axial Chirality, Nomenclature, Square-Planar Complexes, Carbene Complexes, Nucleophilic Carbenes D. Enders, H. Gielen, K. Breuer | 1035 | |
|
Cobalt(II) Derivatives of Cyclic Phosphazenes: Synthesis, Characterization
and Fungicidal Behaviour
Key words: Cobalt(II) Derivatives, Cyclic Phosphazenes, IR Spectra B. P. Baranwal ; S. S. Das, P. Singh | 1039 | |
|
Octacidomycins, IV: A New Total Synthesis of rac-Octacidomycin and
Structurally Related Oligocarboxylic Acids (In German)
Key words: Antibiotics, Octacidomycins, Oligocarboxylic Acids, Synthesis, NMR Data A. Krause, H. Lackner | 1043 | |
|
Optimized Automated Solid Phase Synthesis of Oligonucleotides and
Derivatives
Key words: Oligonucleotides, Thio-Oligonucleotides, 5'- and 3'-Derivatisation of Oligonucleotides, Automatic Oligonucleotide Synthesis, Gene Assembly G. Alvarado Urbina, G. Grübler, A. Weiler, H. Echner, S. Stoeva, J. Schernthaner, W. Gross, W. Voelter | 1051 | |
|
Generation of Nonaphene and Dithianonaphene Derivatives - Model Compounds
for Bent Molecular Ribbons (In German)
Key words: Cycloaddition, Dienes, Bisdienophiles, Heterocycles, Molecular Ribbons H. Meier, B. Rose | 1069 | |
| Note | ||
|
Crystal Structure of ClPb[N(SiMe3)2]3
(In German)
Key words: Lead(IV), Amido Complex, Crystal Structure D. M. Smith, B. Neumüller, K. Dehnicke | 1074 | |
| N u m b e r 10 | ||
| Original Communications | ||
|
Transition Metal Substituted Phosphanes, Arsanes and Stibanes, LIX.
An Adduct of the Me3P-Substituted Ferrio-diphenylphosphane
Cp(OC)(Me3P)Fe-PPh2 and Methylisothiocyanate: Synthesis,
Protonation, and Methylation
(In German)
Key words: Ferrio-phosphanes, Organoisothiocyanates, Adduct Formation, Cationic Phosphane Iron Complexes Wolfgang Malisch, André Spörl, Katharina Thirase, Oliver Fey | 1077 | |
|
Transition Metal Substituted Phosphanes, Arsanes and Stibanes, LX.
Ferrio-(thiocarbamoyl)phosphanes Cp(OC)2Fe-P(Mes)[C(=S)-N(R)H] (R=
Me, Et, t-Bu):
Build-up from the Ferrio-mesitylphosphane Cp(OC)2Fe-P(Mes)H and
Organoisothiocyanates,
Quaternization with Alkyl Halides and Oxidation with Sulfur
(In German)
Key words: Metallo-Phosphanes, Insertion, Quaternization, Oxidation W. Malisch, K. Thirase, J. Reising | 1084 | |
|
Phosphenium Complexes, 43.
Ring-Opening Reactions of the Three-Membered
Phosphametallacycles
Cp(OC)2\cyc{W-P(R)2-Se}
{PR2 = P(o-Tol)2, P(Ph)(o-Tol),
P(Mes)[C(S)N(H)Et], P(t-Bu)[C(O)N(H)Et}
(In German)
Key words: Phosphametallacycles, Ring Opening, Metallo-phosphanes, Metallo-selenophosphoranes, Functionalized Phosphane Complexes W. Malisch, C. Abd El Baky, K. Grün | 1092 | |
|
Magnesium Bis[D(-)-Mandelate] Dihydrate and Other Alkaline Earth,
Alkali, and Zinc Salts of Mandelic Acid
Key words: Mandelic Acid, Magnesium Mandelate, Alkaline Earth Mandelates, Alkali Mandelates, Zinc Mandelate M. Schmidt, A. Schier, H. Schmidbaur | 1098 | |
|
The Basicity of Silylamines and Alkylamines:
An Equilibrium Study of
the Competitive Borane Adduct Formation
Key words: Silylamines, Alkylamines, Borane Adducts, Amineboranes, Basicity Studies G. Huber, H. Schmidbaur | 1103 | |
|
Crystal Chemical Relations of
Co6O2[TeO4(CoAsO5)2] to the Rocksalt Structure
of CoO and a Contribution on Magnetic Measurements of
Co6O2[TeO4(CoAsO5)2]
(In German)
Key words: Cobalt, Tellur, Oxide-Arsenate, Magnetism, Structure Relations M. Staack, Hk. Müller-Buschbaum | 1109 | |
|
Synthesis, Crystal Structure, and Properties of Triguanidinium
Tri-m-imidocyclotriphosphate Monohydrate and Tetraguanidinium
Tetra-m-imidocyclotetraphosphate Tetrahydrate,
[C(NH2)3]3(PO2NH)3 · H2O and
[C(NH2)3]4(PO2NH)4 · 4 H2O
(In German)
Key words: Trimetaphosphimate, Tetrametaphosphimate, Crystal Structure, Thermal Properties, IR Data N. Stock, B. Jürgens, W. Schnick | 1115 | |
|
Studies of Polyhalides, XXXVII.
Heptaiodides(3-) of Ammine Complexes of
Chromium and Cobalt:
Hexamminechromium(III) heptaiodide [Cr(NH3)6](I3)(I4)
and the Tri-m-hydroxo-bis[metal(III)-triammine] heptaiodides
[(NH3)3M(OH)3M(NH3)3](I3)2I with M = Co, Cr
(In German)
Key words: Triiodide(1-), Tetraiodide(2-), Heptaiodide(3-), Hexammine and Tri-m-hydroxo-bis[metal-triammine] Complexes of Chromium and Cobalt, Crystal Structure K.-F. Tebbe, T. Gilles | 1127 | |
|
Functionalized 1,1-Ethene Dithiolates as Ligands, V.
Synthesis and Crystal Structure of Palladium(II) and Platinum(II)
Complexes
with Dithioylidene Barbituric Acid Ligands. Molecular Structure
of a 2,6-Diaminopyridine-Platinum(II) Barbiturate Complex
Key words: Intermolecular Hydrogen-Bonding, Supramolecular Self-Assembly, Dithioylidene Barbituric Acid, Palladium Complex, Platinum complexes W. Weigand, V. Plener, H. Nöth, I. Krossing, J. Knizek, M. Schmidt | 1135 | |
|
Solvothermal Synthesis and Crystal Structure Determination of
Tris(ethyleneamine-ammonium) Tetraselenoantimonat: Non-Centrosymmetry
Mediated by an Extended Unusual N-H···N
Hydrogen Bonded Network?
Key words: Selenoantimonates, Solvothermal Synthesis, Crystal Structure, Hydrogen Bonding F. Wendland, C. Näther, M. Schur, W. Bensch | 1144 | |
|
Investigations on Systems of the Type PCl3/MCl3/Arene (M = Al,
Ga), I. Reactions with Monohalobenzenes; Multinuclear NMR Spectroscopic
Characterization of Aryldichlorohydrogenphosphonium Salts; Crystal
Structure of para-Fluorophenyldichlorophosphonium Tetrachloroaluminate
(In German)
Key words: Arylhalophosphonium Ions, Tetrachloroaluminates, Tetrachlorogallates, Crystal Structure, ab initio Calculations W. Frank, B. Gelhausen, G. J. Reiß, R. Salzer | 1149 | |
|
Thermal Decomposition and Solution Calorimetry of Ammonium Europium
Chlorides
(In German)
Key words: Ammonium Europium Chlorides, Europium Chloride, Thermal Decomposition, Standard Enthalpy of Formation, Standard Entropy C. Hennig, H. Oppermann, A. Blonska | 1169 | |
|
Photochemical Reductive Elimination of Nitrogen from
Triazidogallium(III).
Generation of Luminescent Gallium(I)
Key words: Photochemistry, Charge Transfer, Gallium Complexes, Azide Complexes Horst Kunkely, Arnd Vogler | 1180 | |
|
EPR Evidence of [ReNCl4-nFn]- (n = 1 - 3)
Nitridorhenate(VI) Mixed-Ligand Complexes
(In German)
Key words: Rhenium Complexes, Nitrido Complexes, Mixed-Ligand Complexes, EPR Data A. Voigt, U. Abram, R. Kirmse | 1183 | |
|
Synthesis and Crystal Structure of
N-[(1S,4R)-2-Oxo-pinanyl]-b-alanine Methylester
Key words: N-[(1S,4R)-2-Oxo-pinanyl]-b-alanine Methylester, Chiral b-Alanine Equivalent, Crystal Structure, Hydrogen Bond, Electrochemical Modification B. Albert, M. Jansen, J. Jakobi, E. Steckhan | 1188 | |
|
Synthesis and Conformation of Nucleoside 5'-S-Thiosulfates
Key words: Nucleoside 5'-S-Thiosulfates, Bunte Salts, 1H NMR Data A. Orzeszko, A. Nied\'zwiecka-Korna\'s, R. Stolarski, Z. Kazimierczuk | 1191 | |
|
Lower Hydrates of Aliphatic Primary Amines.
New Studies of Formation and Structure
(In German)
Key words: Amine Hydrates, Hydrates, Melting Diagram, Crystal Structure, Hydrogen Bonding S. Janeda, D. Mootz | 1197 | |
|
Synthesis and Dimroth Rearrangement of
6-Cyano-1,2,3-tiazolo-[4,3-a]pyrimidin-5- and 7-ones. A Novel Alkylation
with Orthoesters and a New Participation of the Cyano Group in the
Rearrangement
Key words: Dimroth Rearrangement, Alkylation with Orthoesters, Cyano Group, Pyrimidine, Triazolopyrimidine E. S. H. El Ashry, Y. El Kilany, N. Rashed, A. Mousaad, H. Assafir | 1203 | |
|
Synthesis and Thermal Properties of Twin Compounds, Alkanediacids
4-(4'-Cyano)-biphenyl Diesters
Key words: Alkanediacids 4-(4'-Cyano)-biphenyl Diesters, Twin Mesogens Bia\/lecka-Flrja\'nczyk. E. Wolarz, D. Bauman | 1213 | |
|
Synthesis of Pyrrolo-, Thienopyrrolo-, Benothienopyrroloquinolines as well
as Triazoloindole Derivates
Key words: Pyrroloquinoline, Triazoloindole, NMR Data, IR Data, MS Data S. I. El-Desoky, E. M. Kandeel, A. H. Abd el-Rahman, R. R. Shmidt | 1216 | |
|
Ab initio MO Optimizations of Osmiumtetracarbonyldihydride and
Metallacyclophanes with two Osmium Atoms and their Molecular Complexes with
Different Guests
Key words: Geometry Optimizations, Osmiumtetracarbonyldihydride, Bis-Osmium-Metallacyclophanes, Host-Guest Complexes, Tetrafluoroethene I. Warttmann, G. Häfelinger | 1223 | |
| Notes | ||
|
Preparation and Crystal Structure of Cs4Nb2S11
Key words: Chalcogenide, Thioniobate, Polysulfide, Niobium, Cesium K. O. Klepp, G. Gabl | 1236 | |
|
On the Metalation of 2,6-Dimethyl-4-tert-butyl-thiophenol
Key words: Metalation, 2,6-Dimethyl-4-tert-butyl-thiophenol, Lithium, Sulfur B. Kersting, G. Steinfeld | 1239 | |
|
Crystal Structure of the Oxo-Acetate Complex
[Co7(m4-O)2(O2CCH3)10(OPEt3)2]
(In German)
Key words: Cobalt, Oxo-Acetate Complex, Crystal Structure H. Ackermann, R. Leo, W. Massa, K. Dehnicke | 1241 | |
|
Phenol Catalyzed Claisen otho Ester Rearrangement of Allylic Alcohols
with Trimethyl-b-(methoxy) ortho Propionate
Key words: E-Alkylidene Cycloalkanes, Claisen otho Ester Rearrangement, Trimethyl-b-(methoxy) ortho Propionate F. Iqbal, H. S. Ateeq, A. Malik, Ze. Ali, Zu. Ali | 1244 | |
| N u m b e r 11 | ||
| Original Communications | ||
|
9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)germatranes.
Synthesis, Characterisation, and Crystal Structures
Key words: Germanium, Germatrane, Organotin Reagents, X-Ray Data, NMR Data G. S. Zaitseva, S. S. Karlov, B. A. Siggelkow, E. V. Avtomonov, A. V. Churakov, J. A. K. Howard, J. Lorberth | 1247 | |
|
Synthesis and Characterization of 1-Allyl-3,7,10-trimethylgermatrane
and 1-Allylazagermatranes
Key words: Germanium, Germatrane, Azagermatranes G. S. Zaitseva, B. A. Siggelkow, S. S. Karlov, G. V. Pen'kovoy, J. Lorberth | 1255 | |
|
Solventothermal Synthesis and Structure of the Polymeric
Thioarsenates(III)
(Et4N)2As6S10 and
(Et4N)2As8S13
Key words: Arsenic, Sulphur, Thioarsenates(III), Solventothermal Synthesis, Chain Structures V. Vater, W. S. Sheldrick | 1259 | |
|
Cleavage and Formation of P-C Bonds During an Unusual
Kinnear-Perren Reaction
Key words: Kinnear-Perren Reaction, Triphenylmethyl V. Plack, J. R. Goerlich, R. Schmutzler | 1265 | |
|
Mechanistic Studies towards the Reversible Equilibrium between Metal
Organic Triple Decker and Sandwich Complexes
[Bis{(h5-CpR)Co}-m-{h4:h4-arene}]
and [(h5-CpR)Co(h6-arene)]
(In German)
Key words: Organometallic Chemistry, Tripledecker Complexes, Sandwich Complexes, Arene Exchange J. J. Schneider, D. Wolf | 1267 | |
|
Synthesis and Molecular Structure of a Superbulky Tertiary Phosphine:
Bis[2-phenyl-1,2-dicarba-closo-dodecaboran-1-yl(12)]phenylphosphine
Key words: Synthesis, Molecular Structure, X-Ray Data, NMR Data, Phosphine V. P. Balema, S. Blaurock, E. Hey-Hawkins | 1273 | |
|
Synthesis of Glycosyl Cyanides by the Reaction
of 1-S-Phosphorothioates of Carbohydrates with Trimethylsilyl Cyanide
Key words: S-Glycosylphosphorothioates, Glycosyl Cyanides, Synthesis W. Kudelska | 1277 | |
|
Structure and Magnetic Properties of an Oxalic Acid Bridged
Dinuclear Copper(II) Complex
Key words: Oxalic Acid Bridge, Dimeric Complex, X-Ray Data, Antiferromagnetic Coupling M. K. Saha, S. Sen, P. Kundu, T. Gupta, V. Gramlich, S. Mitra | 1281 | |
|
Skeletal Rearrangements of an Ylidediylphosphane Tetramer
(In German)
Key words: Phosphonium Ylides, Halophosphanes, Chloride Abstraction, Skeletal Rearrangement, Tetraphospha-bicyclooctanes H.-P. Schrödel, A. Schmidpeter, H. Nöth | 1285 | |
|
Ligand Redistribution Equilibria in Aqueous Fluoroberyllate Solutions
Key words: Fluoroberyllates, Beryllium Fluoride, Ligand Redistribution, NMR Data M. Schmidt, H. Schmidbaur | 1294 | |
|
Lewis Acid Catalyzed Z to E Isomerization of 1,2-Bis(diphenylphosphino)ethene
Key words: Z/E Isomerization, Phosphino-Ethenes, Lewis Acid Catalysis, Gallium Halides, Aluminium Halides, Indium Halides M. Sigl, A. Schier, H. Schmidbaur | 1301 | |
|
2-Diphenylphosphino-phenol as a Ligand for Mono- and Poly-Nuclear
Complexes of Manganese, Cobalt, Nickel, Zinc, and Cadmium
Key words: Phosphino-phenolate Ligands, Phenolate Ligands, Zinc Complex, Manganese Complex, Nickel Complex D. Weiß, Annette Schier, H. Schmidbaur | 1307 | |
|
Isolation and Structural Characterisation of Monoprotonated
1,2-Bis(diphenylphosphino)benzene in its Tetrabromogallate(III) Salt
Key words: 1,2-Bis(diphenylphosphino)benzene, Tertiary Phosphonium Cation, Crystal Structure, Tetrabromogallate(III) M. Sigl, A. Schier, H. Schmidbaur | 1313 | |
|
Organometalloidal Compounds with o-Phenylene Substituents,
Part XXXI.
Charge-transfer Complexes of 2,3,7,8-Tetrakis(methylthio)chalkogenanthrenes
with 7,7,8,8-Tetracyanoquinodimethane and Tetracyanoethene
(In German)
Key words: 2,3,7,8-Tetrakis(methylthio)thianthrene and -selenanthrene / 7,7,8,8-Tetracyanoquinodimethane, 2:1 Charge-Transfer Complexes, Donor/Acceptor/Donor Units; 2,3,7,8-Tetrakis(methylthio)thianthrene / Tetracyanoethene, 2:1 Charge-Transfer Complex, Columnar Structure; MNDO Calculations M. Dötze, H. Czepat, J. Kudnig, G. Klar | 1316 | |
|
Crystal Structure of Pyridinium Periodate
Key words: Pyridinium Periodate, Crystal Structure G. Dutkiewicz, Z. Paj\cak | 1323 | |
|
254:
Synthesis and Crystal Structure of
Bis(triphenylphosphine)-decahydro-hypho-hexaborane
[(PPh3)2B6H10]·CH2Cl2
(In German)
Key words: Bis(triphenylphosphine)-decahydro-hypho-hexaborane, Crystal Structure T. Schaper, W. Preetz | 1326 | |
|
Crystal Structures, Vibrational Spectra and Normal Coordinate Analysis of
cis-[ReCl4X2]2-, X = NCS, NCSe
(In German)
Key words: cis-Tetrachlorodi[thiocyanato(N)]-rhenate(IV), cis-Tetrachlorodi[selenocyanato(N)]-rhenate(IV), Crystal Structure, Vibrational Spectra, Normal Coordinate Analysis L. Homolya, S. Strueß, W. Preetz | 1329 | |
|
Synthesis and Crystal Structure of mer-[Os(NCS)3Py3]
(In German)
Key words: mer-Triisothiocyanato-tris(pyridine)osmium(III), Crystal Structure S. Kolf, W. Preetz | 1335 | |
|
Synthesis, Crystal Structure, Vibrational Spectra, and Normal Coordinate
Analysis
of trans-[OsO2(N2H2C2O2)2]2-
(In German)
Key words: trans-Dioxo-bis(oxamido)osmate(VI), Synthesis, Crystal Structure, Vibrational Spectra, Normal Coordinate Analysis A. Strueß, W. Preetz | 1338 | |
|
Thermochemical and Calorical Behaviour of NdAl3Cl12
(In German)
Key words: Aluminium Neodymium Chloride, Decomposition, Thermochemical Data, Enthalpy, Entropy H. Oppermann, M. Zhang, C. Hennig | 1343 | |
|
Investigation of the Thermochemical Behaviour of Osmium Oxides
(In German)
Key words: Osmium Oxides, Chemical Transport Reactions, Total Pressure Measurements, Enthalpy of Formation, Standard Entropy H. Oppermann, B. Marklein | 1352 | |
|
Metal Complexes of Biologically Important Ligands, CVII.
Formation of
Tris(pentamethylcyclopentadienyl-m-L-prolinato-iridium)
Tris(trifluoromethanesulfonate) with Chiral Self Recognition
Key words: Pentamethylcyclopentadienyl, Iridium, Prolinate K. Sünkel, W. Hoffmüller, W. Beck | 1365 | |
|
Neighbourgroup Participation with the Dehydrogenation of Cyclic Amines of
the o-Substituted Aniline Type
(In German)
Key words: Lactam, Hemiaminal, Aminoaldehyde, Ring-Chain Isomerism, Aminoalkylation H. Möhrle, J. Mehrens | 1369 | |
|
Nickel Complexes of N-Alkylated Derivatives of
2,6-Bis(aminomethyl)-4-tert-butyl-thiophenol
Key words: Mononuclear Complexes, Nickel, Amine-Thiolate Ligands, Solid-State Structures, Solution-State Structures B. Kersting | 1379 | |
| Note | ||
|
The Molecular Structure of Tris(dimethylstibino)amine
Key words: Tris(stibino)amine, Aminostibine, Nitrogen Configuration, Planarity of Nitrogen A. Jockisch, H. Schmidbaur | 1386 | |
| N u m b e r 12 | ||
| Original Communications | ||
|
Interactions in Molecular Crystals, 146.
The Crystal Structure of N,N'-Ditosyl-p-phenylenediamine, Density
Functional Theory
Calculations of Conformations and Hydrogen Bond Motifs in Sulfonamides
(In German)
Key words: Sulfonamides, Crystal Structure, N,N'-Ditosyl-p-phenylendiamine, Density Functional Theory Calculations H. Bock, N. Nagel, C. Näther | 1389 | |
|
Interactions in Molecular Crystals, 147.
Isostructural Host/Guest-Inclusion Compounds of
N,N'-Ditosyl-p-phenylenediamine with Acetone, Cyclopentanone,
Cyclopent-2-ene-1-one, 1,3-Dioxolane, Tetrahydrofurane, and 2,5-Dihydrofurane
(In German)
Key words: N,N'-Ditosyl-p-phenylenediamine, Inclusion Compounds, Crystal Growth, Structures, Host/Guest-Relations H. Bock, N. Nagel, C. Näther | 1401 | |
|
Interactions in Molecular Crystals, 148.
Host/Guest-Inclusion Compounds of N,N'-Ditosyl-p-phenylenediamine with
Furane, Benzene and Dioxane
(In German)
Key words: N,N'-Ditosyl-p-phenylenediamine, Inclusion Compounds, Crystal Growth, Structures, Host/Guest-Relations H. Bock, N. Nagel, C. Näther | 1413 | |
|
Interactions in Molecular Crystals, 149.
Host/Guest-Inclusion Compounds of N,N'-Ditosyl-p-phenylenediamine:
The Hydrogen Bonded Adducts with Morpholine,
Pyridine, N,N-Dimethylformamide, and Dimethylsulfoxide
(In German)
Key words: N,N'-Ditosyl-p-phenylenediamine, Inclusion Compounds, Hydrogen Acceptor and Donor Guest Molecules, Crystal Growth, Structures H. Bock, N. Nagel, C. Näther | 1425 | |
|
Oligomeric Tetrahedral Anions in Borophosphates:
Six-Membered Rings with Open and Cyclic Phosphate Branchings in the Crystal
Structure of K6Cu2[B4P8O28(OH)6]
(In German)
Key words: Boron, Phosphorus, Tetrahedral Anions I. Boy, G. Cordier, R. Kniep | 1440 | |
|
Four Novel N3O4 Donor Macrocycles and their Lanthanide(III)
Complexes
Key words: Template Synthesis, Lanthanide(III) Complexes, Oxaazamacrocycle, Schiff-Base, Ion Selectivity E. Bértolo, R. Bastida, A. de Blas, D. E. Fenton, A. Macías, A. Rodríguez, T. Rodríguez-Blas, A. Villar | 1445 | |
|
Reactions of Donor-Free (CF3)2Cd with Phosphorus(V) Halides:
Insertion of Difluorocarbene and Direct Synthesis of (CF3)3PF2
(In German)
Key words: Phosphoranes, Trifluoromethyl Compounds, Difluorocarbene, Cadmium, NMR Data R. Eujen, R. Haiges | 1455 | |
|
Transition Metal Complexes with Sulfur Ligands, CXXXIII.
Synthesis, Structure, and Properties of New FeII Complexes with
[FeN2S2] Cores
(In German)
Key words: Iron Sulfur Complexes, Amine Ligands, Phosphane Ligands, X-Ray Data, Cyclic Voltammetry D. Sellmann, S. Emig, F. W. Heinemann, F. Knoch | 1461 | |
|
Arsenic(III), Antimony(III) and Bismuth(III) Thiobenzoates: Crystal and
Molecular Structures of M(SOCR)3 and PhSb(SOCPh)2
Key words: Tris-thiobenzoates, Arsenic, Antimony, Bismuth P. Singh, S. Singh, V. D. Gupta, H. Nöth | 1475 | |
|
BaCu6Ge2S8 - A Thiogermanate as a Variant of the
Li3Bi Structure
(In German)
Key words: Chalcogenides, Germanium, Copper, Preparation, Crystal Structure M. Tampier, D. Johrendt | 1483 | |
|
Tetratin(II) and Barium Tritin(II)
Tetrakis[m3-tri-tert-butylsilylphosphandiide] Compounds
with a Tetrametallatetraphosphacubane Core
(In German)
Key words: Arene Complexes, Barium, Heterocubanes, Phosphorus, Tin M. Westerhausen, M. Krofta, N. Wiberg, J. Knizek, H. Nöth, A. Pfitzner | 1489 | |
|
Determination of Coupling Signs 1J(119Sn, 15N) and
2J(119Sn, 117Sn) in Trimethylstannylamines
Key words: Tin, Amines, NMR Data, Ultrahigh Resolution, Coupling Sign Determination B. Wrackmeyer, J. Weidinger, H. Nöth, W. Storch, T. Seifert, M. Vosteen | 1494 | |
|
Metal Complexes with Biologically Important Ligands, CIX.
Organometallic Compounds of Platinum(II), Ruthenium(II), Rhodium(III),
and Iridium(III) with Oxocarbonyl-N-protected a-Amino Acids and
L-Methionylglycinate
(In German)
Key words: Platinum, Ruthenium, Rhodium, Iridium Complexes, L-Methionylglycine M. Prem, K. Polborn, W. Beck | 1501 | |
|
Phosphenium Complexes, XXIX.
[4+2]-Cycloaddition of Phosphenium Complexes of the Type
Cp(OC)2W=PR2 (R = Alkyl, Aryl) with 2,3-Dimethylbutadiene
(In German)
Key words: Phosphenium Complexes, 1,3-Dienes, [4+2]-Cycloaddition, Phosphametallacyclohexenes W. Malisch, K. Grün, A. Fried, W. Reich, M. Schmeußer, U. Weis, C. Abd El Baky, C. Krüger | 1506 | |
|
Molecular Recognition Analyzed by Observing Intramolecular
Interconversion with EPR Spectroscopy
Key words: Rock-Key-Equilibria, Spin Labeling, Molecular Dynamics M. Jäger, P. Schuler, H. B. Stegmann, A. Rockenbauer | 1511 | |
|
Synthesis of the Stereoisomers of b-Hydroxyhistidine and their
Analytical Identification in Hydrolysates of Bacterial Peptides
Key words: b-Hydroxyhistidine, Stereospecific Synthesis K. Taraz, M. Weber, H. Budzikiewicz | 1520 | |
| Notes | ||
|
The Stucture of Lithiumiodide 3-Tetrahydrofuran
Key words: Lithiumiodide, THF Solvate, X-Ray Data H. Nöth, R. Waldhör | 1525 | |
|
Benzo-18-crown-6-Acetonitrile(1/2): Crystallization and Low-Temperature
X-Ray Analysis (In German)
Key words: Benzo-18-crown-6-Acetonitrile(1/2), Crystal Stucture K. Wijaya, O. Moers, A. Blaschette, P. G. Jones | 1528 |